Search Results (154)

Cemented paste backfill (CPB) plays an important role in sustainable mining by providing structural support and reducing surface subsidence. While traditional destructive testing methods such as unconfined compressive strength (UCS) tests offer valuable understanding of material strength, they require a lot of resources, are time-consuming, and environmentally unfriendly. However, non-destructive testing (NDT) techniques such as ultrasonic pulse velocity (UPV), electrical resistivity (ER), and acoustic emission (AE) provide sustainable alternatives by preserving sample integrity, minimizing waste, and enabling real-time monitoring. This study systematically reviews and quantitatively compares the effectiveness of UPV, ER, and AE in predicting the strength of CPB. Meta-analysis of 30 peer-reviewed studies reveals that UPV and AE provide the most consistent and reliable correlations with UCS, with R² values of 0.895 and 0.896, respectively, while ER shows more variability due to its sensitivity to environmental factors. Additionally, a synthetic model combining UPV, AE and ER demonstrates improved accuracy in predicting strength. This hybrid approach enhances predictions of material performance while supporting sustainability in mining and construction. Our research advocates for better testing practices and presents a promising direction for future infrastructure projects, where real-time, non-invasive monitoring can enhance material performance evaluation and optimize resource use. Full article

Red mud (RM) is a strongly alkaline waste residue produced during alumina production, and its high alkali and fine particle characteristics are prone to cause soil, water, and air pollution. Phosphogypsum (PG), as a by-product of the wet process phosphoric acid industry, poses a significant risk of fluorine leaching and threatens the ecological environment and human health due to its high fluorine content and strong acidic properties. In this study, RM-based cemented paste backfill (RCPB) based on the synergistic curing of PG and ordinary Portland cement (OPC) was proposed, aiming to achieve a synergistic enhancement of the material’s mechanical properties and fluorine fixation efficacy by optimizing the slurry concentration (63–69%). Experimental results demonstrated that increasing slurry concentration significantly improved unconfined compressive strength (UCS). The 67% concentration group achieved a UCS of 3.60 MPa after 28 days, while the 63%, 65%, and 69% groups reached 2.50 MPa, 3.20 MPa, and 3.40 MPa, respectively. Fluoride leaching concentrations for all groups were below the Class I groundwater standard (≤1.0 mg/L), with the 67% concentration exhibiting the lowest leaching value (0.6076 mg/L). The dual immobilization mechanism of fluoride ions was revealed by XRD, TGA, and SEM-EDS characterization: (1) Ca²⁺ and F⁻ to generate CaF₂ precipitation; (2) hydration products (C-S-H gel and calixarenes) immobilized F⁻ by physical adsorption and chemical bonding, where the alkaline component of the RM (Na₂O) further promotes the formation of sodium hexafluoroaluminate (Na₃AlF₆) precipitation. The system pH stabilized at 9.0 ± 0.3 after 28 days, mitigating alkalinity risks. High slurry concentrations (67–69%) reduced material porosity by 40–60%, enhancing mechanical performance. It was confirmed that the synergistic effect of RM and PG in the RCPB system could effectively neutralize the alkaline environment and optimize the hydration environment, and, at the same time, form CaF₂ as well as complexes encapsulating and adsorbing fluoride ions, thus significantly reducing the risk of fluorine migration. The aim is to improve the mechanical properties of materials and the fluorine-fixing efficiency by optimizing the slurry concentration (63–69%). The results provide a theoretical basis for the efficient resource utilization of PG and RM and open up a new way for the development of environmentally friendly building materials. Full article

Utilizing potassium salt aggregates and waste brine to produce underground cemented filling materials can address the waste storage issue. However, it is essential for the backfill materials to meet specific transport characteristics. This paper examines the transportation characteristics of lime-cemented mine backfill for a potash mine. The parameters were optimized for the cemented backfill process of potash mines through loop experiments and model simulations. Results indicate that the slump and fluidity of the backfill slurry diminished with increasing lime content and solid concentration. Additionally, the growth rate of pressure loss at the bent pipe and the pressure loss per unit distance in a horizontal pipe increased rapidly over transportation time, indicating a decline in the flowability of the backfill slurry. The lime dosage and solid concentration must align with the backfill requirements. When the lime dosage is 0.5%, the solid content is 70–75%; conversely, with a lime dosage of 0.7% and solid content of 65%, the maximum pumpable time extends to 1 h. The compressive strength of the cured backfill material after 28 days exceeds 1.01 MPa, meeting the transportation requirements for 300 m vertical pipes and 5000 m horizontal pipes. In the case study, the actual flow rate of backfill slurry surpasses the calculated critical flow rate. The estimated and measured values of on-site pressure loss per unit distance in a horizontal pipe exhibit a strong correlation. As the pressure loss per unit distance in a horizontal pipe rises, the discrepancy between the calculated and measured values also increases. When the solid content exceeds 65%, the loop test slightly enhances the compressive strength of the lime-cemented backfill. The findings from this article can aid in determining the on-site backfill process parameters with lime as a binder. Full article

Cemented paste backfill with mine tailings provides a desirable solution for maximally utilizing mine tailings. Ordinary Portland cement (OPC) is the most widely used binder for cemented tailings backfills; however, the serious environmental problems resulting from OPC production and the drawbacks of OPC in cementing fine tailings motivate the investigation of novel binders characterized by environmental friendliness, cost-effectiveness, and efficiency. We previously synthesized solid-waste-based cementitious materials (SWCMs) for cementing fine tailings. In this study, CaCl₂ was added as an accelerator to further enhance the cementing performance of SWCMs for fine tailings. Adding a small amount of CaCl₂ accelerated the hydration of raw materials and prompted the formation of larger amounts of hydration products. As a result, the cementing performance of SWCMs for fine tailings was significantly enhanced through the combined effect of C-S-H gel and ettringite. The cemented fine tailings backfill can be hardened only after curing for ~36 h, with a 50% decrease in hardening duration compared to the control sample without CaCl₂. The optimal amount of CaCl₂ was controlled at 1.5 wt.%, and the sample strength reached 0.21 MPa at 36 h, even at a low binder-to-tailings ratio of 1:8, meeting the requirement of early strength of common cemented tailings backfills. The rapid hardening of cemented fine tailings backfills has significant implications for accelerating ore mining speed, improving mining production capacity, ensuring the safe environment of underground mining sites, and preventing the movement of surface masses in the terrain where mining production takes place. Full article

This study developed a one-part alkali-activated slag/wood biomass fly ash (WBFA) binder (AAS) for preparing cemented paste backfill (CPB) as an alternative to traditional cement. Through multi-scale characterizations (XRD, FTIR, TGA, rheological testing, and MIP) and performance analyses, the regulation mechanisms of slag/WBFA ratios on hydration behavior, microstructure, and mechanical properties were systematically revealed. Results demonstrate that high slag proportions significantly enhance slurry rheology and mechanical strength, primarily through slag hydration generating dense gel networks of hydration products and promoting particle aggregation via reduced zeta potential. Although inert components in WBFA inhibit early hydration, the long-term reactivity of slag effectively counteracts these negative effects, achieving comparable 28-day compressive strength between slag/WBFA-based CPB (4.11 MPa) and cement-based CPB (4.16 MPa). Microstructural analyses indicate that the disordered gels in AAS systems exhibit silicon–oxygen bond polymerization degrees (950 cm⁻¹) comparable to cement, while WBFA regulates Ca/Si ratios to induce bridging site formation (900 cm⁻¹), significantly reducing porosity and enhancing structural compactness. This research provides theoretical support and process optimization strategies for developing low-cost, high-performance mine filling materials using industrial solid wastes, advancing sustainable green mining practices. Full article

There is currently no research examining the rheological properties of cementitious paste backfill (CPB) materials containing aluminium oxide nanoparticles (nAlO). Knowing the yield stress and viscosity of CPB containing nAlO is crucial, especially when applying nano-CPB technology in underground mines. The purpose of this work is to thoroughly examine how nAlO affects the rheological characteristics of CPB and how those characteristics change over time. Yield stress and viscosity measurements are performed on CPB samples with different compositions (e.g., nAlO content, binder type, and superplasticizer content) at intervals of 0 min, 20 min, 1 h, 2 h, and 4 h. The study also includes measurements of the pH and zeta potential of the materials, microstructural studies (TG/DTG and XRD), and electrical conductivity (EC). The findings show that adding nAlO to CPB significantly changes its rheological properties, which in turn affects flowability. The yield stress and viscosity of CPB samples are greatly increased by the incorporation of nAlO, with the degree of influence varying based on variables including water content, curing duration, and type of binder. Because of the nAlO-induced microstructural changes in the CPB material, the interaction of nAlO and a larger fraction of nAlO, along with an increase in curing time, raises rheological characteristics and decreases paste flowability. The results of EC, DTG, and XRD, which show that binder hydration improves with nAlO dosage, corroborate this. Moreover, as nAlO content increases, the zeta potential decreases in magnitude, resulting in stronger repulsion forces and reduced flowability. However, EC, XRD, and DTG analyses suggest that the addition of 0.125% superplasticizer counteracts the flowability reduction caused by nAlO, as the superplasticizer slows down the cement hydration rate at very early curing stages. Moreover, the increase in the slag percentage from 0% to 50% and 75% of the binder content slightly decreases viscosity but greatly increases yield stress. The study’s fresh perspectives contribute to the advancement of nano-CPB technology and have important ramifications for the practical use of this technology in underground mine backfill operations. Full article

In cemented paste backfill (CPB), fly ash (FA) can reduce cement costs. However, the chemical compositions of FA and tailings used in the CPB can vary significantly, affecting the strength values of CPBs, which can be determined through laboratory tests and play a crucial role in design operations. Therefore, developing a predictive model would be advantageous in terms of time and cost. The most critical aspect of this study is that machine learning (ML) models demonstrate high accuracy in the performance of strength prediction in experimental studies, especially in nonlinear and complex data structures, and even in the presence of uncertainty in geochemical and geophysical parameters. Among the ML algorithms, random forest (RF), artificial neural network (ANN), linear regression (LR), voting, and extreme gradient boosting (XGBoost) algorithms were used in this study. According to the results obtained, the XGBoost model exhibited the most robust predictive performance, evidenced by the highest correlation coefficient (R) (0.922) and the lowest mean absolute error (0.666). XGBoost also demonstrated its durability and stability by achieving the lowest relative absolute error (18.81%) and root mean square error (41.10%). Therefore, it has been understood that significant time and resource savings can be achieved in important projects by eliminating the need for experimental tests. Full article

Cemented paste backfill (CPB) improves underground stability by filling mine voids, but the high cost of cement presents economic challenges for miners. While alternative binders and admixtures have been explored, the combined impact of slag substitution and alkali-free (AF) accelerators on CPB performance is not yet fully understood. This study investigates the influences of slag substitution and AF accelerators on the performance of CPB through a comprehensive experimental approach. CPB samples were prepared with slag substitution ratios of 25%, 50%, and 75%, maintaining a fixed AF accelerator content of 0.4%. Various test techniques, including unconfined comprehensive strength (UCS), mercury intrusion porosimetry (MIP), X-ray diffraction (XRD), and thermal analysis (TG/DTA), were employed to study their mechanical and microstructural properties. Monitoring tests were also conducted to thoroughly assess the performance of CPB, including suction (self-desiccation), electrical conductivity (EC), and volumetric water content (VWC) tests. The results showed that the PCI50–SL50–0.4AF sample exhibited 2.3 times higher strength than the control sample for 28 days, with this improvement attributed to enhanced pozzolanic reactions contributing to better microstructural compactness. Monitoring tests revealed accelerated hydration kinetics and reduced water content in slag-reinforced CPB, highlighting the significant role of AF accelerator in facilitating rapid setting and improving early-age mechanical strength. Microstructural findings revealed that porosity decreased and C–S–H gel formation increased in the specimen containing slag and AF accelerators, contributing to increased strength and durability. These findings highlight the potential usage of slag and AF accelerators to enhance CPB’s mechanical, microstructural, and hydration properties, offering significant benefits for mining operations by improving backfill performance, while contributing to environmental sustainability through reduced cement consumption and associated CO₂ emissions. Full article

The presence of free muscovite in tailings can negatively affect the mechanical strength and rheological properties of cemented paste backfill, as has been observed for several cementitious materials. The aim of this study is to evaluate the influence of free muscovite content in tailings on the consistency and rheology of cemented paste backfill. For this purpose, cemented paste backfill mixtures were prepared from two different tailings. The mixtures were prepared at solids contents between 70% and 74% and with the addition of 5% GU (general use Portland cement)/slag binder. In addition, the influence of muscovite was studied by varying the muscovite content of the tailings from about 14% to 25%. Abrams cone slump tests and rheological analyses were carried out for each recipe. The results show a decrease in slump height and an increase in yield stress, Herschel–Bulkley flow index, and infinite shear rate Cross viscosity with increasing muscovite content for a given solids content. Therefore, water should be added to maintain the required flowability of cemented paste backfill, which increases the water/binder ratio and may affect the mechanical strength. A method is presented for determining the amount of binder to be incorporated to maintain the water/binder ratio of the original cemented paste backfill recipe. Full article

Understanding the mechanical and physical behavior of aged CPB under cyclic loading is a significant area of research. Many parameters such as cementation (hydration) and the microstructure, which dictate the arrangement of particles and permeability, affect the mechanical features of cemented paste backfill (CPB). The impact of a wide range of external energy sources within the mining environment, such as cyclic loading resulting from long-term blasting, can significantly alter the applied stresses on the backfill mass. This paper aims to delve into this crucial area of research. A series of uniaxial cyclic tests were conducted on CPB, utilizing samples made from tailing materials sourced from a copper mine in South Australia. Different loading levels were applied at various curing times. All samples exhibited cyclic loading hardening behavior for cyclic loading levels between 80% and 93% of monotonic unconfined compressive strength (UCS), and a cyclic loading damage behavior was observed for 96% of UCS loading level for both 14- and 28-day curing periods. To further investigate these findings, scanning electron microscope analysis as well as sonic velocity tests were conducted for capturing microstructural changes in the samples before and after tests. These findings can be used to indicate a safe firing distance to a filled mass. Full article

The backfill binder material is the key to the cost and performance of cemented paste backfill. This study aims to understand the current situation of metal ore backfill binders, identify industry challenges, inspire research ideas, and explore development directions. Current research investigates trends and developments of backfill binders through literature review, experience summary, field research, statistical analysis, and other methods. Firstly, the main backfill binder types are summarized, including cement, metallurgical slag, thermal slag, chemical slag, and tailings binders. Secondly, the research progress regarding reactivity activation, hydration mechanism, harmful ion solidification, energy conservation, and carbon reduction is summarized. Thirdly, three industrial applications of new backfill binders are introduced and summarized. Cement is still the most common, followed by slag powder binder. The cases of steel slag binder and semi-hydrated phosphogypsum backfill have shown significant effects. Solid waste-based backfill binder materials are gradually replacing cement, which is a trend. Finally, further research is discussed, including hydration modeling and simulation, material properties under extreme environments, hardening process control, and technical standards for backfill binders. This work provides a reference and basis for promoting green and efficient paste backfill and sustainable industry development. Full article

Fiber-reinforced cemented paste backfill (FR-CPB) has attracted considerable attention in modern mining applications due to its superior mechanical properties and adaptability. Despite its potential, understanding its rheological behavior remains limited, largely because of the absence of quantitative methods for assessing fiber packing behavior within CPB. This study develops a rheology-based approach to determine the maximum packing fraction of polypropylene fibers in fresh CPB, revealing that shorter fibers (3 mm) achieve a maximum packing fraction of 0.661, significantly higher than longer fibers (12 mm) with 0.534. Building on these findings, a quantitative model for the static yield stress of FR-CPB was developed, showing that under a high fiber content (0.9%) and with longer fibers (12 mm), the yield stress reached 274.34 kPa, a 40% increase compared to shorter fibers. Additionally, the study modeled the time-dependent evolution of yield stress, achieving a prediction accuracy with a correlation coefficient of 0.92. These advancements enable the optimization of FR-CPB composition, which can reduce material usage, enhance pipeline transport efficiency, and improve backfill stability in underground voids. By minimizing the risk of structural failure and optimizing resource allocation, this research provides a theoretical foundation for safer and more cost-effective mining operations. Full article

Advancements in mine tailings treatment technology have increased the use of superfine tailings, but their extremely fine particle size and high specific surface area limit the performance of superfine tailings cemented paste backfill (STCPB). This study investigates the effects of using superfine cement as a binder to enhance the fluidity, strength, and pore structure of STCPB. The influence of water film thickness (WFT) on STCPB performance is also examined. The results show that the cement-to-tailings ratio (CTR) and solid content (SC) significantly affect the spread diameter (SD) and unconfined compressive strength (UCS), following distinct linear/logarithmic and exponential trends, respectively. WFT has an exponential impact on SD and a non-linear effect on UCS, enhancing strength at low levels (0 μm < WFT < 0.0071 μm) and balancing hydration and flowability at moderate levels (0.0071 μm < WFT < 0.0193 μm) but reducing strength at high levels (WFT > 0.0193 μm). Additionally, superfine cement significantly improves the pore structure of STCPB by reducing porosity and macropore content. These findings provide valuable insights into optimizing STCPB for enhanced performance and sustainability in mine backfilling applications. Full article

Cemented paste backfill (CPB) is a cemented void filling method gaining popularity over traditional hydraulic or rockfill methods. As mining depth increases, CPB-filled stopes are subjected to higher confining pressures. Due to the soil triaxial apparatus limitations, as the conventional method of triaxial testing on CPB, no confining pressures higher than 5 MPa can be applied to CPB over a range of curing time. This lack of data introduces uncertainty in predicting CPB behavior, potentially leading to an overestimation of the required strength. To address this, this study introduces a new testing method that allows for higher confinement beyond traditional limitations by modifying the Hoek triaxial cell to accommodate low-strength materials. This study then investigates the coupled influence of confining pressure and curing time (hydration) on CPB characteristics, specifically examining the impacts of different curing times and confining pressures on the mechanical and rheological properties of CPB. A total of 75 triaxial tests were conducted using 42 mm cylinder shape samples at five various curing times from 7 to 96 days, and applied at low and high confinement condition levels (0.5 to 30 MPa). The results reveal that hydration and confinement positively impact the CPB strength. The modified structured Cam-Clay model was selected to predict the behavior, and its yield surface was updated using the experimental results. The proposed yield model can be utilized to describe CPB material subjected to various curing and pressure conditions underground. Full article

This study evaluated the properties and processing of cemented paste backfills (CPBs) for potash mining through loop tests. The CPBs were made with steel slags as the binder, granulated potash tailings as the aggregate, and waste brine water as the liquid phase. The effects of solid concentration and steel slag dosage on the transport and mechanical properties of CPBs were assessed. The loop test demonstrated that all CPB slurries performed well, exhibiting strong long-distance pipeline transport capabilities. The 28-day compressive strength of the backfills exceeded 1 MPa, meeting the design requirements for backfill strength. The key rheological parameters, including yield stress (τ₀) and viscosity coefficient (η), were comprehensively and theoretically analyzed based on the variations in pressure loss per unit distance of the filling slurry measured during the loop test. The empirical formulas for CPB pressure loss, accounting for varying flow rates and pipeline diameters, were derived with an error margin under 2%. The response surface analysis showed that the affecting extents of factors on pressure loss in CPB slurry were ranked as follows: solid concentration > cementing agent content > flow rate. This study offered valuable guidance for the processing of potash mine backfill operations. Full article