Search Results (270)

This study explores the application of low-power vibrothermography (LVT) for detecting barely visible impact damage (BVID) in carbon fibre-reinforced polymer (CFRP) laminates. Composite specimens with varying impact energies (2.5–20 J) were excited using a single piezoelectric transducer with a nominal centre frequency of 28 kHz, operated at a fixed excitation frequency of 28 kHz. Thermal data were captured using an infrared camera. To enhance defect visibility and suppress background noise, the raw thermal sequences were processed using principal component analysis (PCA) and robust principal component analysis (RPCA). In LVT, RPCA and PCA provided comparable signal-to-noise ratios (SNR), with no consistent advantage for either method across all cases. In contrast, for pulsed thermography (PT) data, RPCA consistently resulted in higher SNR values, except for one sample. The LVT results were further validated by comparison with PT and phased array ultrasonic testing (PAUT) data to confirm the location and shape of detected damage. These findings demonstrate that LVT, when combined with PCA or RPCA, offers a reliable method for identifying BVID and can support safer, more efficient structural health monitoring of composite materials. Full article

There has been a growing interest in polymer-based materials in recent years, and current research is focused on reducing fossil-derived epoxy compounds. This review examines the potential of epoxidised vegetable oils (EVOs) as sustainable alternatives to these systems. Epoxidation processes have been systematically analysed and their influence on chemical, thermal, and mechanical properties has been assessed. Results indicate that basic, low-toxicity epoxidation methods resulted in resins with comparable performance to those obtained through more complex common/commercial procedures. In total, 5–7% oxirane oxygen content (OOC) was found to be optimal to achieve a balanced crosslink density, thus enhancing tensile strength. Furthermore, mechanical properties have been insufficiently studied, as less than half of the studies were conducted at least tensile or flexural strength. Reinforcement strategies were also explored, with nano-reinforcing carbon nanotubes (CBNTs) showing the best mechanical and thermal results. Natural fibres reported better mechanical performance when mixed with EVOs than conventional systems. On the other hand, one of the main constraints observed is the lack of consistency in reporting key chemical and mechanical parameters across studies. Environmental properties and end-of-life use are significant challenges to be addressed in future studies, as there remains a significant gap in understanding the end-of-life of these materials. Future research should focus on the exploration of eco-friendly epoxidation reagents and standardise protocols to compare and measure oil properties before and after being epoxidised. Full article

In this study, a new fibre combination for an interlayer hybrid fibre-reinforced polymer laminate was investigated to achieve pseudo-ductile behaviour in tensile tests. The chosen high-strain fibre for this purpose was S-Glass, and the low-strain fibre was flax. These materials were chosen because of their relatively low environmental impact compared to carbon/carbon and carbon/glass hybrids. An analytical model was used to find an ideal combination of the two materials. With that model, the expected stress–strain relation could also be predicted analytically. The modelling was based on preliminary tensile tests of the two basic components investigated in this research: unidirectional laminates reinforced with either flax fibres or S-Glass fibres. Hybrid specimens were then designed, produced in a heat-assisted pressing process, and subjected to tensile tests. The strain measurement was performed using distributed fibre optic sensing. Ultimately, it was possible to obtain repeatable pseudo-ductile stress–strain behaviour with the chosen hybrid when the specimens were subjected to quasi-static uniaxial tension in the direction of the fibres. The intended damage-mode, consisting of a controlled delamination at the flax-fibre/glass-fibre interface after the flax fibres failed, followed by a load transfer to the glass fibre layers, was successfully achieved. The pseudo-ductile strain averaged 0.52% with a standard deviation of 0.09%, and the average load reserve after delamination was 145.5 MPa with a standard deviation of 48.5 MPa. The integrated fibre optic sensors allowed us to monitor and verify the damage process with increasing strain and load. Finally, the analytical model was compared to the measurements and was partially modified by neglecting the Weibull strength distribution of the high-strain material. Full article

This study presents a novel methodology for the real-time characterisation and quantitative assessment of damage in fibre-reinforced polymers (FRPs) using acoustic emission (AE) techniques. While FRPs offer superior mechanical properties for structural applications, their anisotropic nature introduces complex damage mechanisms that are challenging to detect with conventional inspection methods. Our approach advances beyond traditional peak frequency analysis by implementing a multi-variant frequency assessment that can detect and evaluate simultaneously occurring damage modes. By applying the fast Fourier transform and examining multiple frequency peaks within AE signals, we successfully identified five distinct damage mechanisms in carbon fibre composites: matrix cracking (100–200 kHz), delamination (205–265 kHz), debonding (270–320 kHz), fibre fracture (330–385 kHz), and fibre pullout (395–490 kHz). A comparative analysis with wavelet transform methods demonstrated that our approach provides earlier detection of critical damage events, with delamination identified approximately 28 s sooner than with conventional techniques. The proposed methodology enables a more accurate quantitative assessment of structural health, facilitating timely maintenance interventions for large-scale FRP structures, such as wind turbine blades, thereby enhancing reliability while reducing operational downtime and maintenance costs. Full article

The increasing demand for lightweight, high-performance materials in marine and offshore engineering has driven the development of hybrid solutions combining metals and composites. This study investigates the stress corrosion cracking (SCC) and tribocorrosion behaviour of a novel hybrid wire consisting of a superaustenitic stainless steel (6Mo) outer shell and a carbon fibre-reinforced polymer (CFRP) core. Microstructural analysis, residual stress measurement, and corrosion testing were performed to assess the integrity of the welded structure under harsh conditions. The results revealed that residual stresses and interdendritic segregation in the weld zone significantly contribute to SCC susceptibility, while the 6Mo steel showed improved corrosion resistance over 316L under tribocorrosion conditions but was more sensitive to the sliding frequency. These findings provide critical insights into the degradation mechanisms of metal composite hybrid wires and support the future design of corrosion-resistant components for offshore and structural applications. Full article

The use of composite materials within extreme environments is an exciting frontier in which a wealth of cutting-edge developments have taken place recently. Although there is vast knowledge of composites’ behaviour in standard room temperature and humidity, there is a great need to understand their performance in ‘hot/wet’ conditions, as these are the conditions of their envisaged applications. One of the key failure mechanisms within composites is interlaminar fracture, commonly referred to as delamination. The environmental effects of moisture and elevated temperatures on interlaminar fracture toughness are therefore essential design considerations for laminated aerospace-grade composite materials. IM7/8552, a toughened epoxy/carbon fibre reinforced polymer, was experimentally characterised in both ‘Dry’ and ‘Wet’ conditions at 23 °C and 90 °C. A moisture uptake study was conducted during the ‘Wet’ conditioning of the material in a 70 °C/85% relative humidity environment. Dynamic mechanical thermal analysis was carried out to determine the effect of moisture on the glass transition temperature of the material. Mode I initiation and propagation fracture properties were determined using double cantilevered beam specimens and Mode II initiation fracture properties were deduced using end-notched flexure specimens. The effects of precracking and the methodology of high-temperature testing are discussed in this report. Mode I interlaminar fracture toughness, $G_{IC}$, was found to increase with elevated temperatures and moisture content, with $G_{IC}=0.205{\mathrm{kJ}/\mathrm{m}}^2$ in ‘Dry 23 °C’ conditions increasing by 26% to $G_{IC}=0.259{\mathrm{kJ}/\mathrm{m}}^2$ in ‘Wet 90 °C’ conditions, demonstrating that the material exhibited its toughest behaviour in ‘hot/wet’ conditions. Increased ductility due to matrix softening and fibre bridging caused by temperature and moisture were key contributors to the elevated $G_{IC}$ values. Mode II interlaminar fracture toughness, $G_{IIC}$, was observed to decrease most significantly when moisture or elevated temperature was applied individually, with the combination of ‘hot/wet’ conditions resulting in an 8% drop in $G_{IIC}$, with $G_{IIC}=0.586{\mathrm{kJ}/\mathrm{m}}^2$ in ‘Dry 23 °C’ conditions and $G_{IIC}=0.541{\mathrm{kJ}/\mathrm{m}}^2$ in ‘Wet 90 °C’ conditions. The coupled effect of fibre-matrix interface degradation and increased plasticity due to moisture resulted in a relatively small knockdown on $G_{IIC}$ compared to $G_{IC}$ in ‘hot/wet’ conditions. Fractographic studies of the tested specimens were conducted using scanning electron microscopy. Noteworthy surface topography features were observed on specimens of different fracture modes, moisture saturation levels, and test temperature conditions, including scarps, cusps, broken fibres and river markings. The qualitative features identified during microscopy are critically examined to extrapolate the differences in quantitative results in the various environmental conditions. Full article

Springs are widely used in industries such as aerospace and automotive. As the demand for emission reduction grows, the research on lightweight spring performance is becoming increasingly important. This study analyses the mechanical performance of triple-layer braided composite helical springs (TCHS) under various loads and compression angles. Firstly, the optimal high-temperature curing condition of the epoxy resin was determined through tensile and three-point bending analysis. Then, TCHS were fabricated based on optimal epoxy curing conditions, and multi-angle compression tests under different loads were carried out. Simultaneously, strain gauges were installed at various positions and orientations on the inner and outer sides of the spring wire to reveal strain patterns during the compression. The test results indicate that stiffness decreases with increasing compression angle. Additionally, the strain in the inner and outer positions in different directions of the same region increased with the rise in compression force and angle, and strains in the helical direction were the largest. Subsequently, strain in the helical direction across different regions further showed that maximum strain occurred in the centre coil (region 2), with inner and outer helical direction strains reaching −5116.89 με and 5700.15 με, respectively, which are 71.3% and 90.4% higher than those in region 1 and 73.2% and 92.9% higher than those in region 3. As the compression load increased, cracks appeared on the outer side of the centre coil. In addition, the crack was perpendicular to the helical direction, further confirming that the highest strain occurred in the helical direction. This study provides an in-depth analysis of the impact of angle-specific loads on TCHS, offering valuable insights for the design and optimisation of composite helical springs and laying a theoretical foundation for their future development. Full article

In drilling Carbon-Fibre-Reinforced Polymers (CFRP)/Al stacks, adaptive drilling facilitates the optimisation of cutting parameters for each constituent stack layer and tool wear, thus enhancing cutting efficiency and borehole quality. This study proposed a knot–Temporal Pyramid Pooling (TPP) model aimed at monitoring both process incidences and tool wear in the drilling of hybrid stacks, which subsequently informs the machine tool to adjust cutting parameters or, if necessary, replaces the tool. TPP is introduced to remove the restriction of input dimensions, allowing for the acceptance of inputs with arbitrary shapes. On the other hand, a knot structure has been proposed to incorporate the classification of process incidences into the tool wear analysis, thereby enhancing prediction accuracy. The proposed model achieves a process incidence identification accuracy of 99.19% and a Mean Absolute Error (MAE) of 10 μm in tool wear prediction, demonstrating robust performance across a wide range of sampling conditions. This achievement facilitates decision-making and optimisation relating to cutting parameters and tool replacement in the context of adaptive drilling of aerospace materials. Full article

The development of lightweight construction is of crucial importance for the development of sustainable technologies and for the reduction in carbon dioxide emissions, especially in the automotive industry. This study aims to address the challenges associated with manufacturing plant fibre-based polymer composites. The investigation focused on two novel formulations of bio-based unsaturated polyester resins, assessing their viability as a matrix in plant fibre-reinforced composites within the context of automotive applications. The study addresses the challenges related to the preparation and processing of the system, leading to the necessity of diluting the resin with (hydroxymethyl)methacrylate (HEMA) to achieve an applicable viscosity. Two different flax fibre textiles, in the form of a short fibre mat and a woven fabric, were used as reinforcement. The composite panels were manufactured using the vacuum-assisted resin infusion (VARI) process. The most efficacious material combination, comprising Bcomp^® ampliTex™ 5040 and STRUKTOL^® POLYVERTEC^® 3831, with viscosity modified by 39% HEMA, exhibited a consistent fibre volume fraction of 40% and a glass transition temperature of 70 °C. In addition, the mechanical behaviour in the 0°-direction demonstrated tensile strength and modulus values of approximately 99 MPa and 9 GPa, respectively, accompanied by an elongation at break of 2%. The flexural modulus was found to be 7 GPa, and the flexural strength 94 MPa. Full article

This study explores advanced process monitoring for one-shot drilling of aeronautical stacks made of aluminium 2024 and carbon fibre-reinforced polymer (CFRP) laminates using a 4.8 mm diameter drilling tool and unsupervised machine learning techniques. An experimental campaign is conducted to collect thrust force and torque signals at a 10 kHz sampling rate during the drilling process. These signals are employed for real-time process monitoring, focusing on material change detection and anomaly identification, where anomalies are defined as holes that fail to meet predefined quality criteria. An innovative approach based on unsupervised learning is proposed to enable automatic material change identification, signal segmentation, feature extraction, and hole quality assessment. Specifically, a semi-supervised approach based on a Gaussian Mixture Model (GMM) and 1D Convolutional AutoEncoder (1D-CAE) is employed to detect deviations from normal drilling conditions. The proposed method is benchmarked against state-of-the-art supervised techniques, including logistic regression (LR) and Support Vector Machines (SVMs). Results show that these traditional models struggle with class imbalance, leading to overfitting and limited generalisation, as reflected by the F1 scores of 0.78 and 0.75 for LR and SVM, respectively. In contrast, the proposed semi-supervised approach improves anomaly detection, achieving an F1 score of 0.87 by more effectively identifying poor-quality holes. This study demonstrates the potential of deep learning-based semi-supervised methods for intelligent process monitoring, enabling adaptive control in the drilling process of hybrid stacks and detecting anomalous holes. While the proposed approach effectively handles small and imbalanced datasets, further research into the application of generative AI could enhance performance, aiming for F1 scores above 0.90, thereby supporting adaptation in real industrial environments with high performance. Full article

Forming hybrid structures into complex shapes is key to address lightweighting of automotive parts. Recently, an innovative joining technique between aluminium and Carbon Fibre-Reinforced Polymer (CFRP) based on mechanical interlocking through sheet punching has been developed. However, scaling up the solution requires the assessment of challenges, such as multi-material forming and joint integrity, after forming operations. Therefore, this work proves the feasibility of forming aluminium–CFRP prepreg panels into complex omega-shaped profiles following a conventional cold-stamping process. Forming without defects was possible even in specimens featuring mechanical joints generated through punching. The effect of the CFRP position (in the inner or the outer side of the formed profile), the number of mechanical joints, the addition of a Glass Fibre-Reinforced Polymer (GFRP) intermediate layer to prevent galvanic corrosion and adequate lubrication on necking, cracking, springback behaviour and the final geometry after curing were studied. Compression tests were performed to assess the mechanical response of the hybrid profile, and the results showed that the addition of CFRP in the aluminium omega profile changed the buckling behaviour from global bending to axial folding, increasing the maximum compression load. Additionally, the presence of mechanical interlocking joints further improved the mechanical performance and led to a more controlled failure due to buckling localization in the geometric discontinuity. Full article

The production of fibre-reinforced composites for use in applications such as type-4 pressure vessels for hydrogen storage is achieved through the use of a thermoset matrix. However, the recycling of thermosets presents a significant challenge due to the lack of established recycling methods. Epoxy-based vitrimers show thermoset characteristics during the manufacturing and utilisation phases but exhibit thermoplastic behaviour at elevated temperatures of 190 °C. This study investigates the industrial-scale production of carbon fibre reinforced vitrimers via a wet filament winding, as exemplified by a type-4 pressure vessel demonstrator. Processing conditions of industrial processes have yet to be applied to vitrimers; therefore, two vitrimer formulations are compared to a conventional epoxy thermoset. The processability and resulting composite quality of wound composites using these materials as matrices are compared. The mechanical properties of the composites are compared using an interlaminar shear strength test, demonstrating that the vitrimeric matrices exhibit 19.8% (23 °C) and 49.2% (140 °C) improved interlaminar strength. Consequently, the epoxy-based vitrimers investigated in this study can be employed as a direct replacement for the thermoset matrix in industrial-scale applications, with the potential for recycling the composite. To increase composite qualities, the winding process must be adapted for vitrimers, since a pore free composite could not be achieved. Full article

To achieve the sustainability goals set for the European aviation sector, hydrogen-powered solutions are currently being investigated. Storage solutions are of particular interest, with liquid hydrogen tanks posing numerous challenges with regard to the structural integrity of materials at cryogenic temperatures, as well as safety issues because of the high flammability of hydrogen. In this context and in the scope of the Horizon 2020 Clean Aviation Joint Undertaking (CAJU) project H2ELIOS, the gas permeability behavior of prepreg tape carbon fibre reinforced polymer (CFRP) material was studied. Investigations were performed after thermal shock to 20 K (liquid hydrogen immersion) as well as after a uniaxial stress application at 77 K to identify the shift from Fickian behavior after diverse aging conditions. Helium gas permeation was tested at room temperature (RT), and its representativeness to hydrogen permeation in a range of temperatures was considered in the study. The material’s permeation behavior was compared to ideal Fickian diffusion as a means of identifying related permeation barrier function degradation. Finally, it was possible to identify Fickian, near-Fickian, and non-Fickian behaviors and correlate them with the material’s preconditioning. Full article

Comprehensive analysis of the anisotropic nature of additively manufactured (AM) parts caused by their fabrication method requires attention, as current quasi-static experiments on AM specimens are used to determine strength and stiffness. This study investigates the anisotropic mechanical behaviour of AM polymer composites reinforced with short and continuous carbon fibres, examining various filament orientations, loading directions and strain rates. Utilising the fused deposition modelling (FDM) technique, nylon and carbon fibres were fabricated into composites with controlled orientations. Mechanical tests were conducted in different directions to assess the tensile and compressive properties of these composites, with results showing enhanced tensile strength and stiffness in continuous-fibre (CF) composites compared to short-fibre (SF) ones, particularly in longitudinal orientations. The compressive behaviour revealed complex effects of type and orientation of reinforcing fibres, with CF composites demonstrating superior stiffness but lower strength than SF composites in specific orientations. Strain rate sensitivity analysis for the least anisotropic (quasi-isotropic) cases indicated that tensile strength decreased slightly with the increased strain rate while compressive strength increased. These findings underline the critical effect of fibre orientation and type on mechanical properties and suggest potential applications of AM composites in scenarios demanding tailored anisotropic behaviours, including structural optimisation and numerical modelling for various loading conditions. Full article

Fused deposition modelling (FDM) technology provides a flexible and cost-effective solution for the manufacture of polymer components, enabling the precise design of structures and the incorporation of a variety of composite materials. Its development is confirmed by numerous studies on fibre reinforcements (e.g., GFRP and CF) and thermosetting resin modifications, resulting in improved impact strength and fracture toughness and increased thermal stability of products. The final mechanical properties are significantly influenced by processing parameters (e.g., fill density, layer height, and printing speed) and internal geometry (e.g., lattice structures), which can be further optimised by numerical analyses using constitutive models such as the Johnson–Cook model. The focus of the study presented here is on the fabrication of composites from FDM dies filled with F8 polyurethane resin. Filaments, including PETG carbon and PETG, were tested for potential applications with the resin. A static compression test, supported by numerical analysis using the Johnson–Cook model, was carried out to identify key mechanical characteristics and to predict the material’s behaviour under different loading conditions. The results indicate that these structures exhibit numerous potential delamination planes and voids between filament paths, leading to relatively low maximum stress values (σ_m ≈ 2.5–3 MPa). However, the impregnation with polyurethane resin significantly enhances these properties by bonding the layers and filling the pores, resulting in a more homogeneous and stronger composite. Additionally, numerical simulations effectively captured key aspects of structural behaviour, identifying critical stress concentration areas, particularly along the side walls and in regions forming triangular stress zones. These findings provide valuable insights into the potential of resin-filled FDM structures in engineering applications, demonstrating their improved performance over purely printed samples. Full article