Quantitative Microstructure Characterization in Additively Manufactured Nickel Alloy 625 Using Image Segmentation and Deep Learning
Abstract
1. Introduction
2. Materials and Methods
2.1. PBF-LB/M of Nickel Alloy 625
2.2. Characterization of Test Coupons for Relative Density and Melt Pool Size
2.3. Microstructural Characterization of Test Coupons for Grain Size
2.4. Microstructural Characterization of Test Coupons for Porosity
2.5. Deep Learning-Based Characterization of Microstructure
2.5.1. Dependencies and Required Libraries
2.5.2. Training Process
2.5.3. Melt Pool Dataset and Methodology
3. Results
3.1. Effects of Process Parameters and Energy Density on Relative Density and Melt Pool Size
3.2. Effects of Process Parameters and Energy Density on Grain Size and Porosity
3.3. Results on Automatically Characterized Melt Pool Regions and Types
3.3.1. Melt Pool Dataset and Approach
3.3.2. DNN Model Execution
3.3.3. Stage 1—Region Proposal Network
3.3.4. Stage 2—Proposal Classification
3.3.5. Stage 3—Generating Masks
3.3.6. Performance Comparison with Confusion Matrices
4. Discussions
5. Conclusions
Author Contributions
Funding
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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| Laser Power, P [W] | Scan Velocity, vs [mm/s] | Hatch Distance, h [mm] | Energy Density, Ed [J/mm3] | Coupon No. | Relative Density (SSR = 67°), ρrel [%] | Coupon No. | Relative Density (SSR = 90°), ρrel [%] |
|---|---|---|---|---|---|---|---|
| 169 | 875 | 0.10 | 96.57 | #11 | 95.23 | #1 | 96.00 |
| 195 | 875 | 0.10 | 111.43 | #19 | 98.30 | #4 | 98.70 |
| 182 | 875 | 0.09 | 115.56 | #26 | 97.03 | #6 | 97.40 |
| 182 | 725 | 0.11 | 114.11 | #10 | 95.97 | #8 | 96.17 |
| 195 | 800 | 0.11 | 110.80 | #25 | 98.47 | #9 | 98.52 |
| 182 | 725 | 0.09 | 139.46 | #27 | 97.14 | #12 | 97.29 |
| 182 | 800 | 0.10 | 113.75 | #7 | 98.10 | #14 | 98.21 |
| 182 | 800 | 0.10 | 113.75 | #22 | 98.05 | #15 | 98.19 |
| 195 | 725 | 0.10 | 134.48 | #3 | 97.50 | #16 | 97.74 |
| 182 | 800 | 0.10 | 113.75 | #24 | 98.13 | #17 | 98.30 |
| 182 | 875 | 0.11 | 94.55 | #28 | 96.50 | #18 | 96.75 |
| 169 | 725 | 0.10 | 116.55 | #2 | 96.38 | #20 | 96.52 |
| 169 | 800 | 0.09 | 117.36 | #5 | 97.50 | #21 | 97.91 |
| 169 | 800 | 0.11 | 96.02 | #30 | 96.60 | #23 | 96.78 |
| 195 | 800 | 0.09 | 135.42 | #13 | 99.01 | #29 | 99.23 |
| 195 | 800 | 0.10 | 121.88 | #31 | 98.64 | #34 | 98.86 |
| 195 | 800 | 0.10 | 121.88 | #32 | 98.53 | #35 | 98.75 |
| 195 | 800 | 0.10 | 121.88 | #33 | 98.69 | #36 | 98.81 |
| MP Width Avg [μm] | MP Width Std Dev. [μm] | MP Depth Avg [μm] | MP Depth St. Dev. [μm] | |||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|
| Coupon No. | Type I | Type II | Total | Type I | Type II | Total | Type I | Type II | Total | Type I | Type II | Total |
| 01 | 134 | 92 | 113 | 12 | 9 | 24 | 35 | 31 | 33 | 6 | 5 | 6 |
| 04 | 170 | 111 | 135 | 25 | 7 | 34 | 49 | 46 | 47 | 7 | 8 | 7 |
| 06 | 149 | 101 | 128 | 17 | 16 | 30 | 45 | 38 | 42 | 7 | 5 | 7 |
| 08 | 153 | 107 | 130 | 25 | 12 | 30 | 48 | 39 | 44 | 8 | 9 | 9 |
| 09 | 143 | 109 | 128 | 13 | 9 | 21 | 44 | 42 | 43 | 7 | 7 | 7 |
| 12 | 134 | 113 | 126 | 18 | 11 | 19 | 45 | 36 | 41 | 7 | 10 | 10 |
| 14 | 132 | 109 | 121 | 11 | 10 | 15 | 44 | 38 | 41 | 7 | 6 | 7 |
| 15 | 128 | 105 | 119 | 12 | 11 | 17 | 40 | 33 | 37 | 9 | 6 | 9 |
| 16 | 152 | 114 | 133 | 13 | 11 | 22 | 52 | 42 | 47 | 18 | 10 | 16 |
| 17 | 143 | 112 | 127 | 10 | 7 | 18 | 48 | 38 | 42 | 6 | 7 | 8 |
| 18 | 134 | 110 | 126 | 13 | 15 | 17 | 47 | 32 | 41 | 7 | 7 | 10 |
| 20 | 159 | 106 | 136 | 13 | 8 | 29 | 51 | 42 | 47 | 8 | 6 | 8 |
| 21 | 154 | 107 | 131 | 14 | 9 | 27 | 47 | 45 | 46 | 8 | 9 | 8 |
| 23 | 150 | 96 | 120 | 28 | 11 | 33 | 43 | 33 | 36 | 6 | 6 | 8 |
| 29 | 149 | 103 | 128 | 15 | 16 | 28 | 49 | 39 | 44 | 7 | 12 | 11 |
| 34 | 109 | 86 | 102 | 15 | 11 | 17 | 31 | 21 | 28 | 8 | 6 | 9 |
| 35 | 155 | 112 | 128 | 11 | 15 | 25 | 50 | 41 | 46 | 6 | 7 | 8 |
| 36 | 145 | 109 | 127 | 18 | 11 | 24 | 38 | 30 | 34 | 7 | 8 | 9 |
| MP Width Avg [μm] | MP Width Std Dev. [μm] | MP Depth Avg [μm] | MP Depth St. Dev. [μm] | |||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|
| Coupon No. | Type I | Type II | Total | Type I | Type II | Total | Type I | Type II | Total | Type I | Type II | Total |
| 02 | 129 | 135 | 132 | 5 | 2 | 5 | 65 | 55 | 60 | 11 | 8 | 10 |
| 03 | 134 | 119 | 127 | 9 | 19 | 16 | 51 | 43 | 48 | 8 | 6 | 8 |
| 05 | 157 | 135 | 146 | 37 | 35 | 37 | 49 | 39 | 44 | 13 | 13 | 14 |
| 07 | 151 | 124 | 138 | 24 | 28 | 29 | 45 | 31 | 38 | 11 | 8 | 12 |
| 10 | 132 | 112 | 123 | 14 | 24 | 21 | 44 | 35 | 40 | 9 | 9 | 10 |
| 11 | 122 | 115 | 119 | 13 | 21 | 17 | 40 | 35 | 38 | 8 | 9 | 9 |
| 13 | 131 | 107 | 122 | 17 | 2 | 18 | 49 | 44 | 47 | 9 | 11 | 9 |
| 19 | 128 | 116 | 122 | 13 | 11 | 13 | 53 | 42 | 48 | 5 | 12 | 10 |
| 22 | 135 | 114 | 124 | 14 | 19 | 19 | 52 | 41 | 46 | 9 | 7 | 9 |
| 24 | 144 | 105 | 121 | 34 | 11 | 30 | 52 | 33 | 41 | 22 | 9 | 17 |
| 25 | 108 | 92 | 99 | 11 | 18 | 16 | 41 | 28 | 34 | 8 | 6 | 9 |
| 26 | 129 | 105 | 117 | 16 | 18 | 20 | 49 | 38 | 43 | 11 | 7 | 11 |
| 27 | 129 | 118 | 123 | 10 | 16 | 14 | 40 | 37 | 38 | 7 | 8 | 7 |
| 28 | 140 | 119 | 130 | 25 | 19 | 24 | 46 | 37 | 41 | 6 | 7 | 8 |
| 30 | 125 | 129 | 127 | 10 | 16 | 12 | 47 | 40 | 44 | 12 | 5 | 10 |
| 31 | 139 | 95 | 120 | 12 | 11 | 26 | 48 | 29 | 40 | 6 | 4 | 11 |
| 32 | 162 | 134 | 148 | 19 | 28 | 27 | 66 | 51 | 59 | 14 | 11 | 15 |
| 33 | 144 | 114 | 131 | 16 | 23 | 24 | 52 | 41 | 48 | 11 | 5 | 11 |
| Coupon No. | Mean Grain Radius [μm] | Std. Dev. [μm] | Mean Pore Radius [μm] | Std Dev. [μm] | Porosity, ϕ |
|---|---|---|---|---|---|
| 01 | 2.2794 | 1.5510 | 4.5917 | 3.1961 | 0.7178 |
| 04 | 2.0132 | 1.3418 | 4.0492 | 2.8706 | 0.7147 |
| 06 | 1.8956 | 1.2351 | 4.4277 | 2.9787 | 0.7559 |
| 08 | 2.1505 | 1.4380 | 4.7066 | 3.4561 | 0.7567 |
| 09 | 2.4213 | 1.7668 | 4.1178 | 3.0785 | 0.6699 |
| 12 | 2.1787 | 1.5250 | 4.5536 | 3.3237 | 0.7348 |
| 14 | 2.4601 | 1.8565 | 3.8310 | 2.9046 | 0.6367 |
| 15 | 2.2317 | 1.4896 | 4.0132 | 2.7045 | 0.6829 |
| 16 | 2.3398 | 1.6879 | 4.0830 | 3.2377 | 0.7194 |
| 17 | 2.3136 | 1.6081 | 3.8139 | 2.8470 | 0.6805 |
| 18 | 2.2048 | 1.5835 | 4.2186 | 3.0482 | 0.7107 |
| 20 | 2.1372 | 1.5167 | 4.2465 | 3.1071 | 0.7152 |
| 21 | 2.1384 | 1.4816 | 4.3856 | 3.1742 | 0.7259 |
| 23 | 2.3505 | 1.7118 | 4.3226 | 3.3843 | 0.6998 |
| 29 | 2.5596 | 1.9217 | 4.1221 | 3.1664 | 0.6846 |
| 34 | 1.9908 | 1.2578 | 5.2711 | 3.5520 | 0.8059 |
| 35 | 2.4821 | 1.8590 | 4.7938 | 3.7423 | 0.7289 |
| 36 | 2.0277 | 1.3845 | 4.1613 | 3.0649 | 0.7335 |
| Coupon No. | Mean Grain Radius [μm] | Std. Dev. [μm] | Mean Pore Radius [μm] | Std Dev. [μm] | Porosity, ϕ |
|---|---|---|---|---|---|
| 02 | 2.1483 | 1.5134 | 3.9791 | 2.8600 | 0.6964 |
| 03 | 2.2404 | 1.6166 | 4.4491 | 3.5498 | 0.7396 |
| 05 | 1.8759 | 1.2474 | 4.9503 | 3.2635 | 0.7864 |
| 07 | 2.2666 | 1.6092 | 3.9426 | 2.8498 | 0.6728 |
| 10 | 2.0864 | 1.4825 | 4.3285 | 2.9631 | 0.7162 |
| 11 | 2.2232 | 1.4423 | 5.0286 | 3.6196 | 0.7643 |
| 13 | 2.1129 | 1.4082 | 3.4728 | 2.4835 | 0.6721 |
| 19 | 2.2913 | 1.6313 | 4.3415 | 3.2039 | 0.7012 |
| 22 | 2.0632 | 1.3707 | 4.0125 | 2.7893 | 0.7092 |
| 24 | 2.2458 | 1.7224 | 4.5079 | 3.6708 | 0.7319 |
| 25 | 2.1304 | 1.5404 | 4.6321 | 3.5358 | 0.7560 |
| 26 | 2.1113 | 1.4312 | 4.6661 | 3.5630 | 0.7553 |
| 27 | 2.0532 | 1.4089 | 4.4341 | 3.1009 | 0.7394 |
| 28 | 2.0996 | 1.4459 | 4.2513 | 3.0084 | 0.7227 |
| 30 | 2.1272 | 1.5016 | 4.7930 | 3.3313 | 0.7470 |
| 31 | 2.2121 | 1.5708 | 4.3880 | 3.3125 | 0.7287 |
| 32 | 2.0916 | 1.4588 | 3.5067 | 2.6458 | 0.6775 |
| 33 | 2.2009 | 1.5002 | 3.8782 | 2.8120 | 0.6912 |
| Model Backbone | Melt Pool Class | Mean IoU | Precision | Recall |
|---|---|---|---|---|
| ResNet-50 | Type I | 0.81 | 0.89 | 0.86 |
| ResNet-50 | Type II | 0.78 | 0.87 | 0.83 |
| ResNet-101 | Type I | 0.85 | 0.92 | 0.89 |
| ResNet-101 | Type II | 0.82 | 0.90 | 0.87 |
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Özel, T.; Ding, S.; Ramasubramanian, A.; Pieri, F.; Eskicorapci, D. Quantitative Microstructure Characterization in Additively Manufactured Nickel Alloy 625 Using Image Segmentation and Deep Learning. Machines 2026, 14, 366. https://doi.org/10.3390/machines14040366
Özel T, Ding S, Ramasubramanian A, Pieri F, Eskicorapci D. Quantitative Microstructure Characterization in Additively Manufactured Nickel Alloy 625 Using Image Segmentation and Deep Learning. Machines. 2026; 14(4):366. https://doi.org/10.3390/machines14040366
Chicago/Turabian StyleÖzel, Tuğrul, Sijie Ding, Amit Ramasubramanian, Franco Pieri, and Doruk Eskicorapci. 2026. "Quantitative Microstructure Characterization in Additively Manufactured Nickel Alloy 625 Using Image Segmentation and Deep Learning" Machines 14, no. 4: 366. https://doi.org/10.3390/machines14040366
APA StyleÖzel, T., Ding, S., Ramasubramanian, A., Pieri, F., & Eskicorapci, D. (2026). Quantitative Microstructure Characterization in Additively Manufactured Nickel Alloy 625 Using Image Segmentation and Deep Learning. Machines, 14(4), 366. https://doi.org/10.3390/machines14040366

