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Keywords = uniaxial loading experiment

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29 pages, 9027 KB  
Article
Microstructural Mechanisms of Concrete Degradation Under Different Coal Gangue Sand Replacement Ratios
by Yukai Cai, Wenhua Zha, Tao Xu, Chao Ji and Yaozong Li
Materials 2025, 18(20), 4787; https://doi.org/10.3390/ma18204787 - 20 Oct 2025
Viewed by 220
Abstract
Coal gangue manufactured sand (CGS), a sustainable substitute for natural sand, offers both resource and environmental benefits; however, the micro-mechanisms underlying performance deterioration at different replacement levels remain unclear. In this study, cube specimens with 25%, 50%, 75%, and 100% CGS were tested [...] Read more.
Coal gangue manufactured sand (CGS), a sustainable substitute for natural sand, offers both resource and environmental benefits; however, the micro-mechanisms underlying performance deterioration at different replacement levels remain unclear. In this study, cube specimens with 25%, 50%, 75%, and 100% CGS were tested in uniaxial compression, and the results were integrated with PFC2D discrete-element simulations and SEM observations to establish an energy–force-chain–crack coupling framework. Experiments and simulations showed close agreement in peak stress, peak strain, and overall curve shape (errors generally <5%). With increasing replacement, the interfacial transition zone (ITZ) evolves from a dense three-phase ITZ (NS–CGS–CA; natural sand–CGS–coarse aggregate) to a degraded two-phase ITZ (CGS–CA), accompanied by more pores and microcracks; the proportion of Adhesive cracks decreases while Cohesive (intra-particle) cracks increase. Concurrently, continuous force-chain networks deteriorate into localized short-chain clusters; the peak and fraction of strain-energy decrease, whereas frictional/damping dissipation rises—together driving a macroscopic transition from ductile to brittle behavior. At 28 d, SEM images and DEM evolution of cracks/force chains/energy exhibit strong consistency, further confirming that low replacement (25% and 50%) favors stable load-transfer paths and suppresses early cracking, whereas high replacement (75% and 100%)—through ITZ degradation and force-chain instability—induces more concentrated cracking and higher energy dissipation, thereby diminishing mechanical performance. Full article
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17 pages, 3942 KB  
Article
Transparent Elastic Wound Dressing Gel Supporting Drug Release: Synergistic Effects of Poly(Vinyl Alcohol)/Chitosan Hybrid Matrix
by Lifei Chen, Ningning Yuan, Zhenjiang Tan, Jianwei Zhang, Lishi Zhang, Wenwei Tang, Cheng Chen and Donghai Lin
Gels 2025, 11(10), 771; https://doi.org/10.3390/gels11100771 - 25 Sep 2025
Viewed by 358
Abstract
Wound infection is one of the most critical factors affecting the healing process. Therefore, the development of wound dressings with excellent antibacterial effects has become a research hotspot in the current academic field. We prepared AgNPs (silver nanoparticles) via a redox method, combined [...] Read more.
Wound infection is one of the most critical factors affecting the healing process. Therefore, the development of wound dressings with excellent antibacterial effects has become a research hotspot in the current academic field. We prepared AgNPs (silver nanoparticles) via a redox method, combined them with Poly(vinyl alcohol)/chitosan (PVA/CS), and dried the mixture into a film to fabricate a silver-loaded hydrogel film dressing with excellent antibacterial properties. Uniaxial tensile tests on the samples revealed that the prepared film dressings exhibited good mechanical properties, preventing fracture caused by external forces. Protein adsorption experiments indicated their favorable protein adsorption performance, which can adsorb microorganisms on the external surface of the dressing. By leveraging the bactericidal mechanism of AgNPs, the dressing achieves efficient antibacterial effects. Additionally, the dressing prepared by this method features good transparency, facilitating routine observation of the wound area without removing the dressing and maintaining a sterile environment for an extended period. Finally, we verified the drug loading and drug release capabilities of the dressing, and found that it has good drug loading capacity and drug release effect. This preliminarily proves its effectiveness and provides more possibilities for subsequent research on composite drugs. This study provides new insights for exploring the clinical application of multifunctional silver-loaded wound dressings. Full article
(This article belongs to the Special Issue Designing Gels for Wound Dressing (2nd Edition))
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21 pages, 2858 KB  
Article
Study on the Mechanical Properties and Fracture Mechanisms of Anchor Cable Specimen Materials
by Chenfei Wang, Guangming Fan, Kai Zhang, Yajun Zhang, Junyin Lian, Wenkai Huang, Shuqin Shi and Mincheng Zhang
J. Compos. Sci. 2025, 9(9), 508; https://doi.org/10.3390/jcs9090508 - 19 Sep 2025
Viewed by 450
Abstract
This study investigated the tensile behaviors of 12.70 mm and 15.20 mm diameter anchor cable specimens with ultimate tensile strengths of 1860 MPa and their material specimens through experiments and finite element (FE) simulations. Material specimens and anchor cable specimen tensile samples were [...] Read more.
This study investigated the tensile behaviors of 12.70 mm and 15.20 mm diameter anchor cable specimens with ultimate tensile strengths of 1860 MPa and their material specimens through experiments and finite element (FE) simulations. Material specimens and anchor cable specimen tensile samples were prepared, and the complete engineering stress–strain curves were obtained via uniaxial tensile tests. FE analysis was used to simulate the uniaxial tensile tests, and the applicability of different constitutive models for describing the true stress–strain relationships was evaluated by comparing the simulated and experimental engineering stress–strain curves. The results showed that the Ludwik, Hollomon, and Swift models, fitted using the pre-necking hardening stage, overestimated the post-necking true stress, while the Voce model underestimated it. In contrast, the Ling and Swift + Voce models provided accurate post-necking true stress predictions. Based on the Ling model and the Rice and Tracey fracture criterion, the load–displacement relationship and fracture behavior of the 12.7 mm anchor cable specimen were best described with W = −0.1 and a = 2, whereas W = −0.1 and a = 3 yielded optimal predictions for the 15.2 mm anchor cable specimen. Full article
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15 pages, 6499 KB  
Article
The Effect of Interrupted Loading on the Lüder Phenomena in AISI 1524 Steel Alloy
by Mohamed Almatroushi, Salman Pervaiz and Wael A. Samad
Alloys 2025, 4(3), 19; https://doi.org/10.3390/alloys4030019 - 17 Sep 2025
Viewed by 471
Abstract
Under specific temperature and strain rate conditions, certain materials, such as low-carbon steels and select magnesium and aluminum alloys, experience a localized deformation phenomenon known as the Lüders effect. This behavior manifests as a well-defined yield point, after which the stress–strain response transitions [...] Read more.
Under specific temperature and strain rate conditions, certain materials, such as low-carbon steels and select magnesium and aluminum alloys, experience a localized deformation phenomenon known as the Lüders effect. This behavior manifests as a well-defined yield point, after which the stress–strain response transitions into a plateau phase. Experimentally observed through full-field tests, the Lüders effect appears in the form of a band(s). This manuscript presents, for the first time, a systematic study of interrupted loading on the Lüders phenomenon in AISI 1524 hot-rolled steel, using uniaxial tensile testing combined with digital image correlation (DIC). While similar approaches have been applied to other alloys, no prior work has reported on AISI 1524 steel under unloading–reloading cycles during the Lüders plateau. Interruptions in loading involved unloading at 25%, 50%, and 75% of the total plateau region independently until stress approached zero, followed by reloading at the same rate until failure. Each unloading case was subjected to two tests, alongside two additional control tests where loading proceeded without interruption. Based on the findings of this study, it can be inferred that the Lüders phenomenon in AISI 1524 steel exhibits a decrease in strain intensity upon unloading, along with an extension of the Lüders plateau when interrupted loading occurs up to halfway through the plateau region. However, implementing an interrupted loading regime at three-quarters of the plateau had minimal to no discernible effect on the phenomenon. The majority of samples displayed two Lüders bands, a few exhibited either a single band or three bands, suggesting a complex relationship with material heterogeneity and specific impurities present in each sample. The novelty of this work lies in showing how controlled unloading–reloading cycles alter both the propagation and characteristics of Lüders bands in AISI 1524 steel. Full article
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21 pages, 8478 KB  
Article
Research on Strength Degradation and Crack Development in Defective Concrete
by Qiwei Lin, Yujing Jiang and Satoshi Sugimoto
GeoHazards 2025, 6(3), 50; https://doi.org/10.3390/geohazards6030050 - 1 Sep 2025
Viewed by 591
Abstract
Tunnel linings play a vital role in underground infrastructure, yet their performance can be severely affected by pre-existing cracks. This study investigates the mechanical behavior and failure mechanisms of C30 concrete with artificial cracks under uniaxial compression, simulating various crack conditions observed in [...] Read more.
Tunnel linings play a vital role in underground infrastructure, yet their performance can be severely affected by pre-existing cracks. This study investigates the mechanical behavior and failure mechanisms of C30 concrete with artificial cracks under uniaxial compression, simulating various crack conditions observed in tunnel linings. Specimens were designed with varying crack lengths and orientations. Acoustic emission (AE) monitoring was employed to capture the evolution of internal damage and micro-cracking activity during loading. Fractal dimension analysis was performed on post-test crack patterns to quantitatively evaluate the complexity and branching characteristics of crack propagation. The AE results showed clear correlations between amplitude characteristics and macroscopic crack growth, while fractal analysis provided an effective metric for assessing the extent of damage. To complement the experiments, discrete element modeling (DEM) using PFC3D was applied to simulate crack initiation and propagation, with results compared against experimental data for validation. The study demonstrates the effectiveness of DEM in modeling cracked concrete and highlights the critical role of crack orientation and size in strength degradation. These findings provide a theoretical and numerical foundation for assessing tunnel lining defects and support the development of preventive and reinforcement strategies in tunnel engineering. Full article
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17 pages, 3279 KB  
Article
Rapid Assessment of Ti-6Al-4V Fatigue Limit via Infrared Thermography
by Chiara Colombo, Antonio Salerno, Arthur Teyssiéras and Carlo Alberto Biffi
Metals 2025, 15(8), 825; https://doi.org/10.3390/met15080825 - 23 Jul 2025
Cited by 1 | Viewed by 632
Abstract
The experimental tests needed for the estimation of the fatigue limit generally require extensive time and many specimens. A valid but not standardized alternative is the thermographic analysis of the self-heating phenomenon. The present work is aimed at using Infrared thermography to determine [...] Read more.
The experimental tests needed for the estimation of the fatigue limit generally require extensive time and many specimens. A valid but not standardized alternative is the thermographic analysis of the self-heating phenomenon. The present work is aimed at using Infrared thermography to determine the fatigue limit in two kinds of Ti-6Al-4V samples obtained by hot rolling: (1) with the standard dog-bone shape (unnotched specimen) and (2) with two opposed semicircular notches at the sides (notched specimen). Uniaxial tensile experiments are performed on unnotched samples, and the surface temperature variation during loading is monitored. The stress corresponding to the end of the thermoelastic stage gives a rough indication of the fatigue limit. Then, fatigue tests at different sinusoidal loads are performed, and the thermographic signal is monitored and processed. The results obtained using lock-in thermography in dissipative mode, e.g., analyzing the second harmonic, showed a sudden change in slope when the applied stress exceeded a certain limit. This slope change is related to the fatigue limit. In addition, the ratio between the fatigue limits obtained for notched and unnotched specimens, e.g., the fatigue strength reduction factor, is consistent with literature values based on the selected geometry. Full article
(This article belongs to the Special Issue Fracture Mechanics of Metals (2nd Edition))
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22 pages, 13284 KB  
Article
Mechanical Properties of CuZr Amorphous Metallic Nanofoam at Various Temperatures Investigated by Molecular Dynamics Simulation
by Yuhang Zhang, Hongjian Zhou and Xiuming Liu
Materials 2025, 18(14), 3423; https://doi.org/10.3390/ma18143423 - 21 Jul 2025
Viewed by 710
Abstract
Metallic nanofoams with amorphous structures demonstrate exceptional properties and significant potential for diverse applications. However, their mechanical properties at different temperatures are still unclear. By using molecular dynamics simulation, this study investigates the mechanical responses of representative CuZr amorphous metallic nanofoam (AMNF) under [...] Read more.
Metallic nanofoams with amorphous structures demonstrate exceptional properties and significant potential for diverse applications. However, their mechanical properties at different temperatures are still unclear. By using molecular dynamics simulation, this study investigates the mechanical responses of representative CuZr amorphous metallic nanofoam (AMNF) under uniaxial tension and compression at various temperatures. Our results reveal that the mechanical properties, such as Young’s modulus, yield stress, and maximum stress, exhibit notable temperature sensitivity and tension–compression asymmetry. Under tensile loading, the Young’s modulus, yield strength, and peak stress exhibit significant reductions of approximately 30.5%, 33.3%, and 32.9%, respectively, as the temperature increases from 100 K to 600 K. Similarly, under compressive loading, these mechanical properties experience even greater declines, with the Young’s modulus, yield strength, and peak stress decreasing by about 34.5%, 38.0%, and 41.7% over the same temperature range. The tension–compression asymmetry in yield strength is temperature independent. Interestingly, the tension–compression asymmetry in elastic modulus becomes more pronounced at elevated temperatures, which is attributed to the influence of surface energy effects. This phenomenon is further amplified by the increased disparity in surface-area-to-volume ratio variations between tensile and compressive loading at higher temperatures. Additionally, as the temperature rises, despite material softening, the structural resistance under large tensile strains improves due to delayed ligament degradation and more uniform deformation distribution, delaying global failure. Full article
(This article belongs to the Section Mechanics of Materials)
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29 pages, 21376 KB  
Article
Numerical Simulation of Fracture Failure Propagation in Water-Saturated Sandstone with Pore Defects Under Non-Uniform Loading Effects
by Gang Liu, Yonglong Zan, Dongwei Wang, Shengxuan Wang, Zhitao Yang, Yao Zeng, Guoqing Wei and Xiang Shi
Water 2025, 17(12), 1725; https://doi.org/10.3390/w17121725 - 7 Jun 2025
Cited by 1 | Viewed by 725
Abstract
The instability of mine roadways is significantly influenced by the coupled effects of groundwater seepage and non-uniform loading. These interactions often induce localized plastic deformation and progressive failure, particularly in the roof and sidewall regions. Seepage elevates pore water pressure and deteriorates the [...] Read more.
The instability of mine roadways is significantly influenced by the coupled effects of groundwater seepage and non-uniform loading. These interactions often induce localized plastic deformation and progressive failure, particularly in the roof and sidewall regions. Seepage elevates pore water pressure and deteriorates the mechanical properties of the rock mass, while non-uniform loading leads to stress concentration. The combined effect facilitates the propagation of microcracks and the formation of shear zones, ultimately resulting in localized instability. This initial damage disrupts the mechanical equilibrium and can evolve into severe geohazards, including roof collapse, water inrush, and rockburst. Therefore, understanding the damage and failure mechanisms of mine roadways at the mesoscale, under the combined influence of stress heterogeneity and hydraulic weakening, is of critical importance based on laboratory experiments and numerical simulations. However, the large scale of in situ roadway structures imposes significant constraints on full-scale physical modeling due to limitations in laboratory space and loading capacity. To address these challenges, a straight-wall circular arch roadway was adopted as the geometric prototype, with a total height of 4 m (2 m for the straight wall and 2 m for the arch), a base width of 4 m, and an arch radius of 2 m. Scaled physical models were fabricated based on geometric similarity principles, using defect-bearing sandstone specimens with dimensions of 100 mm × 30 mm × 100 mm (length × width × height) and pore-type defects measuring 40 mm × 20 mm × 20 mm (base × wall height × arch radius), to replicate the stress distribution and deformation behavior of the prototype. Uniaxial compression tests on water-saturated sandstone specimens were performed using a TAW-2000 electro-hydraulic servo testing system. The failure process was continuously monitored through acoustic emission (AE) techniques and static strain acquisition systems. Concurrently, FLAC3D 6.0 numerical simulations were employed to analyze the evolution of internal stress fields and the spatial distribution of plastic zones in saturated sandstone containing pore defects. Experimental results indicate that under non-uniform loading, the stress–strain curves of saturated sandstone with pore-type defects typically exhibit four distinct deformation stages. The extent of crack initiation, propagation, and coalescence is strongly correlated with the magnitude and heterogeneity of localized stress concentrations. AE parameters, including ringing counts and peak frequencies, reveal pronounced spatial partitioning. The internal stress field exhibits an overall banded pattern, with localized variations induced by stress anisotropy. Numerical simulation results further show that shear failure zones tend to cluster regionally, while tensile failure zones are more evenly distributed. Additionally, the stress field configuration at the specimen crown significantly influences the dispersion characteristics of the stress–strain response. These findings offer valuable theoretical insights and practical guidance for surrounding rock control, early warning systems, and reinforcement strategies in water-infiltrated mine roadways subjected to non-uniform loading conditions. Full article
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19 pages, 3343 KB  
Article
Crystal Plasticity Finite Element Simulation of Tensile Fracture of 316L Stainless Steel Produced by Selective Laser Melting
by Guowei Zeng, Ziyang Huang, Bei Deng and Rui Ge
Metals 2025, 15(5), 567; https://doi.org/10.3390/met15050567 - 21 May 2025
Cited by 3 | Viewed by 1186
Abstract
Selective Laser Melting (SLM) of 316L stainless steel exhibits great potential prospects for engineering applications due to its high strength, high forming freedom, and low material waste. However, due to the unique processing technology of additive manufacturing, challenges related to the microstructure and [...] Read more.
Selective Laser Melting (SLM) of 316L stainless steel exhibits great potential prospects for engineering applications due to its high strength, high forming freedom, and low material waste. However, due to the unique processing technology of additive manufacturing, challenges related to the microstructure and differences in the mechanical properties of the formed parts are inevitable. To investigate the influence of building direction and grain boundary strength on the fracture parameters of SLM 316L stainless steel, electron backscatter diffraction (EBSD) experiments were conducted to characterize the microstructure of SLM 316L stainless-steel specimens. A representative volume element (RVE) model reflecting the microstructure of SLM 316L stainless steel was established based on a combination of the crystal plastic finite element method (CPFEM) and UMAT subroutine technology. The crystal plasticity parameters were determined by comparing the results of tensile tests. Cohesive elements were employed and inserted at the grain boundaries of the polycrystalline RVE to simulate the intergranular fracture behavior of SLM 316L stainless steel under uniaxial tensile loading. The damage and fracture mechanisms of the material at the microscale were analyzed. The simulated tensile stress–strain curves were in good agreement with the experimental results; hence, the combined CPFEM model is suitable for characterizing the mechanical response and fracture behavior of the SLM 316L stainless steel. The results revealed that cracks initiate at stress concentration sites and propagate along grain boundaries with increasing external load, ultimately leading to rupture. Additionally, the building direction influences the location of microcracks and their propagation significantly. Full article
(This article belongs to the Special Issue Multi-scale Simulation of Metallic Materials (2nd Edition))
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19 pages, 25099 KB  
Article
Study on Infrasonic Signal Characteristics and Energy Characterization of Damage and Failure in Red Sandstone Under Uniaxial Cyclic Loading and Unloading Conditions
by Min Zhang, Peng Zeng, Kui Zhao, Zhigang Lu, Xinmu Xu, Yan Yang and Zhouchao Liu
Appl. Sci. 2025, 15(9), 4893; https://doi.org/10.3390/app15094893 - 28 Apr 2025
Viewed by 393
Abstract
The instability and collapse of surrounding rock in mine goaf areas often lead to the destabilization of geological structures, surface subsidence, and mining safety accidents. To investigate the evolutionary mechanisms and precursor characteristics of rock instability and failure processes, uniaxial loading and cyclic [...] Read more.
The instability and collapse of surrounding rock in mine goaf areas often lead to the destabilization of geological structures, surface subsidence, and mining safety accidents. To investigate the evolutionary mechanisms and precursor characteristics of rock instability and failure processes, uniaxial loading and cyclic loading–unloading tests were conducted on red sandstone using a rock mechanics loading system. These experiments aimed to explore the mechanical behavior of the rock and the development process of internal fractures. The characteristics of infrasonic signals generated during red sandstone fracturing and the laws governing damage evolution were analyzed with an infrasonic acquisition system. The research results indicate that the infrasonic signal activity generated by rock under loading conditions can be characterized by three distinct stages, namely the relative stability period, the active period, and the pre-failure precursor period. Prior to peak strength, a substantial number of infrasonic signals are generated in rocks with significant activity; this characteristic is independent of the loading path but dependent on the stress magnitude. The variation in cumulative infrasonic energy reflects the accumulation of damage in rock specimens during the loading process, and as damage accumulates, the stress–strain curve exhibits hysteresis effects and nonlinear increases, accompanied by a rapid rise in infrasonic energy. By analyzing the characteristics of infrasonic parameters and characterizing the damage and its evolutionary features in red sandstone based on infrasonic energy, the internal crack damage evolution process in rocks can be effectively characterized. This approach provides theoretical foundations and technical support for early warning and monitoring prior to rock failure. Full article
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30 pages, 29741 KB  
Article
Evolution Characteristics of Pore–Fractures and Mechanical Response of Dehydrated Lignite Based on In Situ Computed Tomography (CT) Scanning
by Shuai Yan, Lijun Han, Shasha Zhang, Weisheng Zhao and Lingdong Meng
Fractal Fract. 2025, 9(4), 220; https://doi.org/10.3390/fractalfract9040220 - 31 Mar 2025
Viewed by 613
Abstract
Based on the uniaxial compression tests and in situ CT scanning experiments of lignite with different dehydration times and the fractal theory, this paper qualitatively and quantitatively investigated the influence of the dehydration effect on the evolution of pore–fractures and the mechanical behavior [...] Read more.
Based on the uniaxial compression tests and in situ CT scanning experiments of lignite with different dehydration times and the fractal theory, this paper qualitatively and quantitatively investigated the influence of the dehydration effect on the evolution of pore–fractures and the mechanical behavior of lignite under uniaxial compression conditions. The results show that the dehydration effect significantly affects the pre-peak deformation and post-peak failure behavior of lignite but has no significant impact on its peak strength. The pore–fracture parameters, such as the fractal dimension, surface porosity, and fracture volume, of three samples all exhibit an evolutionary pattern of “continuous decrease in the compaction and elastic stages–gradual increase in the plastic stage–sharp growth in the post-peak stage” with the dynamic evolution of the pore–fractures. However, the dehydration effect leads to an increase in the intensity of pore–crack evolution and a nonlinear rise in all the parameters characterizing the pore–crack complexity during uniaxial compression, which, in turn, leads to an increment in the fluctuation of the above evolutionary trends. The mechanism underlying the differential influence of the dehydration effect on the macroscopic mechanical behavior of lignite is follows: The dehydration effect non-linearly and positively affects the initial pore–fracture structure of lignite, thereby non-linearly and positively promoting the evolution of pore–fractures during the loading process. Nevertheless, since it fails to weaken the micro-mechanical properties of lignite and cannot form effective through-going fractures, it has no significant impact on the uniaxial compressive strength of the coal samples. The findings of this study can provide some references for the support design and deformation control of underground lignite roadways. Full article
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22 pages, 17592 KB  
Article
Impact of Feature-Selection in a Data-Driven Method for Flow Curve Identification of Sheet Metal
by Quang Ninh Hoang, Hyungbum Park, Dang Giang Lai, Sy-Ngoc Nguyen, Quoc Tuan Pham and Van Duy Dinh
Metals 2025, 15(4), 392; https://doi.org/10.3390/met15040392 - 31 Mar 2025
Viewed by 963
Abstract
This study presents an innovative data-driven methodology to model the hardening behavior of sheet metals across a broad strain range, crucial for understanding sheet metal mechanics. Conventionally, true stress–strain data from such tests are used to analyze plastic flow within the pre-necking regime, [...] Read more.
This study presents an innovative data-driven methodology to model the hardening behavior of sheet metals across a broad strain range, crucial for understanding sheet metal mechanics. Conventionally, true stress–strain data from such tests are used to analyze plastic flow within the pre-necking regime, often requiring additional experiments to inverse finite element methods, which demand extensive field data for improved accuracy. Although digital image correlation offers precise data, its implementation is costly. To address this, we integrate experimental data from standard tensile tests with a machine-learning approach to estimate the flow curve. Subsequently, we conduct finite element simulations on uniaxial tensile tests, using materials characterized by the Swift constitutive equation to build a comprehensive database. Loading force-gripper displacement curves from these simulations are then transformed into input features for model training. We propose and compare three models—Models A, B, and C—each employing different input feature selections to estimate the flow curve. Experimental validation including uniaxial tensile, plane strain, and simple shear tests on the DP590 and DP780 sheets are then carefully considered. Results demonstrate the effectiveness of our proposed method, with Model C showing the highest efficacy. Full article
(This article belongs to the Special Issue Machine Learning Models in Metals)
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25 pages, 16103 KB  
Article
Compressive Response and Damage Distribution of Fiber-Reinforced Concrete with Various Saturation Degrees
by Lu Feng and Xudong Chen
Materials 2025, 18(7), 1555; https://doi.org/10.3390/ma18071555 - 29 Mar 2025
Viewed by 627
Abstract
Tunnels frequently experience issues such as lining spalling and water leakage, making the stability of tunnel support critical for engineering safety. Given that tunnels are subjected to various ground stress disturbances and groundwater influences, it is essential to investigate the mechanical properties and [...] Read more.
Tunnels frequently experience issues such as lining spalling and water leakage, making the stability of tunnel support critical for engineering safety. Given that tunnels are subjected to various ground stress disturbances and groundwater influences, it is essential to investigate the mechanical properties and damage mechanisms of tunnel support materials under different loading paths and saturation levels. Fiber-reinforced concrete (FRC) is widely used for tunnel support; in this study, uniaxial compression tests were conducted on FRC with different fiber contents (0%, 0.5%, 1.0%) under varying loading paths (monotonic, pre-peak cyclic loading, full cyclic loading). The stress–strain behavior, volumetric strain, and elastic modulus were analyzed. The results indicate that increasing fiber content enhances strength and stiffness, while higher water content leads to a significant water-weakening effect, reducing both parameters. To classify crack types, the logistic regression (LR) algorithm is employed based on the AF-RA features, identifying tensile damage (which accounts for 60–80%) as more dominant than shear damage. Using this classification, AE event distributions reveal the spatial characteristics of internal damage in FRC. Gaussian process regression (GPR) is further applied to predict the AE parameters, enabling the assessment of the tensile and shear damage responses in FRC. The location and magnitude of the predicted wave crest indicate extreme damage levels, which become more pronounced under a higher saturation condition. A damage constitutive model is proposed to characterize the post-peak softening behavior of FRC. The numerical verification demonstrates good agreement with the experimental results, confirming the model’s capability to describe the softening behavior of FRC under various fiber and water contents. Full article
(This article belongs to the Special Issue Advanced Characterization of Fiber-Reinforced Composite Materials)
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31 pages, 10107 KB  
Article
Mechanical Characterization and Feasibility Analysis of PolyJet™ Materials in Tissue-Mimicking Applications
by Yash Soni, Paul Rothweiler and Arthur G. Erdman
Machines 2025, 13(3), 234; https://doi.org/10.3390/machines13030234 - 13 Mar 2025
Viewed by 1967
Abstract
PolyJet™ 3D printing is an additive manufacturing (AM) technology from StratasysTM. It has been used for applications such as tissue mimicking, printing anatomical models, and surgical planning. The materials available from StratasysTM have the inherent capabilities of producing a number [...] Read more.
PolyJet™ 3D printing is an additive manufacturing (AM) technology from StratasysTM. It has been used for applications such as tissue mimicking, printing anatomical models, and surgical planning. The materials available from StratasysTM have the inherent capabilities of producing a number of PolyJet™ materials with a range of physical properties that can be utilized for representing realistic tissue behavior mechanically. The preset materials available in the PolyJet™ printing software version 1.92.17.44384 GrabCADTM Print allow the user to manufacture materials similar to biological tissue, but the combinations of possibilities are limited and might not represent the broad spectrum of all tissue types. The purpose of this study was to determine the combination of PolyJet™ materials that most accurately mimicked a particular biological tissue mechanically. A detailed Design of Experiment (DOE) methodology was used to determine the combination of material mixtures and printing parameters and to analyze their mechanical properties that best matched the biological tissue properties available in the literature of approximately 50 different tissue types. Uniaxial tensile testing was performed according to the ASTM standard D638-14 of samples printed from Stratasys J850 digital anatomy printer to their determined stress–strain properties. The obtained values were subsequently validated by comparing them with the corresponding mechanical properties of biological tissues available in the literature. The resulting model, developed using the DOE approach, successfully produced artificial tissue analogs that span a wide range of mechanical characteristics, from tough, load-bearing tissues to soft, compliant tissues. The validation confirmed the effectiveness of the model in replicating the diverse mechanical behavior of various human tissues. Overall, this paper provides a detailed methodology of how materials and settings were chosen in GrabCADTM Print software and Digital Anatomy CreatorTM (DAC) to achieve an accurate artificial tissue material. Full article
(This article belongs to the Special Issue Recent Advances in 3D Printing in Industry 4.0)
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19 pages, 10999 KB  
Article
A Comprehensive Mechanical Testing of Polyacrylamide Hydrogels: The Impact of Crosslink Density
by Christina G. Antipova, Arthur E. Krupnin, Arthur R. Zakirov, Vsevolod V. Pobezhimov, Daniil A. Romanenko, Dina Yu. Stolyarova, Sergei N. Chvalun and Timofei E. Grigoriev
Polymers 2025, 17(6), 737; https://doi.org/10.3390/polym17060737 - 11 Mar 2025
Cited by 2 | Viewed by 3608
Abstract
Mechanical properties are one of the most important characteristics of biomaterials for many different applications, including biomedicine. Soft biomaterials, such as hydrogels, are difficult to characterize by conventional mechanical testing, because their mechanical properties are much lower than required by conventional testing machines. [...] Read more.
Mechanical properties are one of the most important characteristics of biomaterials for many different applications, including biomedicine. Soft biomaterials, such as hydrogels, are difficult to characterize by conventional mechanical testing, because their mechanical properties are much lower than required by conventional testing machines. In this work, we aimed to systematically study the mechanical behavior of a model soft material, polyacrylamide hydrogels, under different loading modes: tension, torsion, compression, and indentation. This allowed us to develop a comprehensive approach to the mechanical testing of soft materials. To overcome excessive compression and slippage of the hydrogel samples when fixed in the grips during tension, additional 3D-printed grips were designed. Digital image correlation was used to determine the Poisson’s ratio of the hydrogels. The Young’s modulus values obtained from all types of mechanical tests analyzed were highly correlated. However, for hydrogels with a low crosslinker concentration, 1–2%, tension–compression asymmetry was observed. Moreover, the results of the mechanical tests were verified in indentation tests, including analytical estimation, and full-scale and numerical experiments. We also discuss the limits of using a two-parameter Mooney–Rivlin model for fitting hydrogel uniaxial tension deformation curves, which was unstable for the hydrogels with 4 and 9% crosslinker concentration. The implemented approach provided a comprehensive analysis of the mechanical behavior of biomaterials. The elastic moduli for all hydrogels studied were in the range from 20 to 160 kPa, which corresponds well to human soft tissues, making them a promising material for application as tissue-mimicking phantoms. Full article
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