Search Results (45)

The main aim of this research is to investigate the possibilities and challenges involved in the electric arc welding of solid-state-recycled EN AW 6082 aluminum alloy. Lately, solid-state recycling has gained increased attention as a more sustainable and efficient aluminum recycling method, whereby only about 30% of the energy of conventional recycling is used. This method is based on the deformation of small-sized metal waste into solid recycled specimens without a remelting step. For the welding of solid-state-recycled specimens, both metal inert gas welding and tungsten inert gas welding methods are used. To evaluate the weldability of solid-state-recycled material, welded specimens are compared with welded, commercially produced EN AW 6082 aluminum alloy sheets. The welding is performed using the same processes, parameters, and conditions. To evaluate the welding potential of solid-state-recycled alloy, tensile tests, microhardness tests, optical metallography, and scanning electron microscopy, accompanied by energy-dispersive spectroscopy analysis, are performed. Full article

This paper describes a study of the microstructure and mechanical properties of a titanium–gallium (Ti-8 wt.% Ga) alloy using X-ray diffraction, optical metallography, micro-hardness measurements, compression and tensile testing, nanoindentation and ultrasonic velocity measurements. X-ray diffraction has shown the alloy to be wholly α Ti with no other phases present. A comparison of the hardness and elastic modulus values of the Ti-8Ga alloy with those of Ti-6Al-4V showed the former to have a significantly higher hardness, although the elastic moduli of the two alloys were broadly comparable. The study also indicated reasonable agreement between the elastic moduli obtained by nanoindentation, ultrasonic velocity measurements and tensile testing. Under compressive loading, the mean 0.2% proof stress values of the Ti-8Ga alloy were between 1066 MPa and 1083 MPa. However, under tensile conditions, the mean tensile strength was found to be only 427 MPa, and the alloy exhibited highly brittle behaviour, with specimens failing before they had undergone any appreciable plasticity. The cause of this was ascribed to high oxygen and nitrogen levels. Full article

To investigate the mechanical properties and microstructure evolution of P92 steel during long-term service, the operated P92 main steam pipes from the first ultra-supercritical units in China were sectioned into samples representing various service durations and stresses (0# (as-received state, 1# (82,000 h, 67.3 MPa), 2# (85,000 h, 78.0 MPa), and 3# (100,000 h, 80.3 MPa)). Thereafter, a comprehensive assessment of their mechanical properties, including tensile strength, impact, hardness, and creep resistance, as well as a detailed microstructure analysis, was carried out. The effect of stress on the aging of material properties during operation is discussed. The results show that the circumferential stress caused by the increase in the internal steam pressure can significantly promote the creep life consumption of P92 steel, resulting in the degradation of mechanical properties and the expedited aging of the microstructure. The R_p0.2 and R_m of the P92 main steam pipe at room temperature and 605 °C decreased with the service time increase, reflecting the influence of stress in operation, which is expected to be used for the residual life evaluation of P92 steel. The relationship between the impact absorption energy (FATT50), Brinell hardness, and the operating time of P92 operating pipes is non-monotonic, indicating that these parameters are not sensitive indicators of material aging due to stress. The evaluation of performance degradation in P92 operating pipes due to stress-induced aging is not reliably discernible through optical metallography alone. To achieve a thorough assessment, the use of transmission electron microscopy (TEM) is essential. Full article

This study developed a new metallography–property relationship neural network (MPR-Net) to predict the relationship between the microstructure and mechanical properties of 316L stainless steel built by laser powder bed fusion (LPBF). The accuracy R² of MPR-Net was 0.96 and 0.91 for tensile strength and Vickers hardness predictions, respectively, based on optical metallurgy images. Feature visualisation methods, such as gradient-weighted class activation mapping (Grad-CAM) and clustering, were employed to interpret the abstract features within the MPR-Net, providing insights into the molten pool morphology and grain formation mechanisms during the LPBF process. Experimental results showed that the optimal process parameters—190 W laser power and 700 mm/s scanning speed—yielded a maximum tensile strength of 762.83 MPa and a Vickers hardness of 253.07 HV_0.2 with nearly full densification (99.97%). The study marks the first application of a convolutional neural network (MPR-Net) to predict the mechanical properties of 316L stainless steel samples manufactured through laser powder bed fusion (LPBF) based on metallography. It innovatively employs techniques such as gradient-weighted class activation mapping (Grad-CAM), spatial coherence testing, and clustering to provide deeper insights into the workings of the machine learning model, enhancing the interpretability of complex neural network decisions in material science. Full article

The fatigue performance of laser powder bed fusion-fabricated Ti-6Al-4V alloy was investigated using four-point bending testing. Specifically, the effects of keyhole and lack-of-fusion porosities along with various surface roughness parameters, were evaluated in the context of pore circularity and size using 2D optical metallography. Surface roughness of S_a = 15 to 7 microns was examined by SEM, and the corresponding fatigue performance was found to vary by 10² cycles to failure. The S–N curves for the various defects were also correlated with process window examination in laser beam power–velocity (P–V) space. Basquin’s stress-life relation was well fitted to the experimental S–N curves for various process parameters except keyhole porosity, indicating reduced importance for LPBF-fabricated Ti-6Al-4V alloy components. Full article

The main aim of this research was to investigate the aluminum AlSi9Cu3(Fe) machining chips recycling possibility utilizing a direct hot extrusion process and thixoforming. The thixo feedstock was prepared directly from the aluminum alloy AlSi9Cu3(Fe) machining chips waste without any remelting step. The machining chips were compacted, and direct hot extruded to create the solid samples and thixo feedstock. The aluminum alloy AlSi9Cu3(Fe) machining chips had a high degree of plastic deformation and after extrusion and heating in the semisolid temperature range, the suitable globular microstructure was achieved, which is a precondition for a successful thixoforming process. This approach can be characterized as a semisolid recycling process with a lower energy consumption, a higher material yield, and reduced greenhouse gas emissions into the atmosphere compared with conventional casting and recycling. Optical metallography, scanning electron microscopy accompanied with energy dispersive spectroscopy, electrical conductivity, and mechanical properties investigation were performed on the reference casted sample with a dendritic microstructure, the extruded sample with a severely deformed microstructure, and finally the thixoformed samples with a globular microstructure produced with different parameters, according to the Taguchi L4 (2³) experimental plan. Full article

Four ferrous objects, a winch, a heart-shaped shackle, a deadeye strap with a futtock plate, and a stud-link chain controller, that were retrieved from the Akko Tower shipwreck were studied by different methods, including conventional metallography, light microscopy, scanning electron microscopy with energy-dispersive spectroscopy, optical emission spectroscopy, microhardness measurements, and the novel field multi-focal metallography (FMM), in order to determine their composition, microstructure, and manufacturing methods. The results of FMM agree well with conventional destructive metallography. The winch drum was made of grey cast iron and its shaft was wrought iron; the heart-shaped shackle and the deadeye strap with a futtock plate were wrought iron; and the stud-link chain controller was grey cast iron similar in composition and microstructure to the winch. All the wrought iron items revealed a similar composition and microstructure. Based on the composition, microstructure, and manufacturing processes of the four items, it is suggested that they were manufactured in the mid-nineteenth century. The high quality of these items indicates that they were produced using controlled processes, probably in the same workshop. Full article

Pure titanium is limited to be used in biomedical applications due to its lower mechanical strength compared to its alloy counterpart. To enhance its properties and improve medical implants feasibility, advancements in titanium processing technologies are necessary. One such technique is equal-channel angular pressing (ECAP) for its severe plastic deformation (SPD). This study aims to surface modify commercially pure titanium using micro-arc oxidation (MAO) or plasma electrolytic oxidation (PEO) technologies, and mineral solutions containing Ca and P. The composition, metallography, and shape of the changed surface were characterized using X-ray diffraction (XRD), digital optical microscopy (OM), and scanning electron microscope (SEM), respectively. A microhardness test is conducted to assess each sample’s mechanical strength. The weight % of Ca and P in the coating was determined using energy dispersive spectroscopy (EDS), and the corrosion resistance was evaluated through potentiodynamic measurement. The behavior of human dental pulp cell and periodontal cell behavior was also studied through a biomedical experiment over a period of 1-, 3-, and 7-days using culture medium, and the cell death and viability can be inferred with the help of enzyme-linked immunosorbent assay (ELISA) since it can detect proteins or biomarkers secreted by cells undergoing apoptosis or necrosis. This study shows that the mechanical grain refinement method and surface modification might improve the mechanical and biomechanical properties of commercially pure (CP) titanium. According to the results of the corrosion loss measurements, 2PassMAO had the lowest corrosion rate, which is determined to be 0.495 mmpy. The electrode potentials for the 1-pass and 2-pass coated samples are 1.44 V and 1.47 V, respectively. This suggests that the coating is highly effective in reducing the corrosion rate of the metallic CP Ti sample. Changes in the grain size and the presence of a high number of grain boundaries have a significant impact on the corrosion resistance of CP Ti. For ECAPED and surface-modified titanium samples in a 3.6% NaCl electrolyte solution, electrochemical impedance spectroscopy (EIS) properties are similar to Nyquist and Bode plot fitting. In light of ISO 10993-5 guidelines for assessing in vitro cytotoxicity, this study contributes valuable insights into pulp and periodontal cell behavior, focusing specifically on material cytotoxicity, a critical factor determined by a 30% decrease in cell viability. Full article

The porosity of die-cast aluminum alloys is a determining factor for the quality of the product. In this paper, we studied the porosity of a selected part of a die-cast AlSi9Cu3(Fe) compressor part by computer tomography and metallography. In the case of this part, the achievable resolution by CT, a non-destructive testing method, was 30 μm—this method could not detect smaller cavities. Based on metallographic analysis, the percentage of defects larger than 30 μm ranges from 10 to 30% of the total number of defects, which represents 75–95% of the defective area (area ratio). Impregnation with methacrylate resin (used to seal cavities to prevent leakage) can be detected with UV-illuminated optical microscopic examination on metallographically prepared specimens. As confirmed by scanning electron microscopy, partial filling and partial impregnation can occur in a system of shrinkage cavities. Full article

This paper aims to improve the mechanical properties and fatigue life of AISI/SAE 4140 alloy steel connecting rods (CRs). Conventional CRs are typically manufactured through open die forging/hammering, blocking, and hot forging processes. In the present work, a modification to the process route has been proposed such that the open die forging/hammering was completely replaced with a multistep asymmetrical reducer rolling technique. Four rolling passes were introduced to achieve the desired preform shape and size. The effect of each rolling pass on grain size, mechanical properties, and fatigue life was investigated. Samples from each multistep rolling, blocking, and forging stage were subjected to impact, hardness, tensile, and fatigue testing. Metallography using optical and scanning electron microscopes was also conducted to reveal metallurgical changes. Fatigue testing and fractography were performed using the R.R. Moore Rotating-Beam Fatigue testing machine and scanning electron microscope, respectively, to evaluate the fatigue life and the fracture behavior of both the conventional and multistep rolled forged CRs. It was observed that, unlike the conventional forging process, multistep asymmetrical rolling gradually reduces grain size as the rolling progresses and improves yield, tensile, and impact strengths, hardness, and ductility. In comparison to conventional forging, multistep rolling led to an almost 33% and 29% increase in yield and tensile strengths, respectively. Moreover, the fatigue life of multistep rolled CR increased by more than five times compared to conventional CR. Full article

The thin-wall heat pipe is an efficient heat transfer component that has been widely used in the field of heat dissipation of high-power electronic equipment in recent years. In this study, the orange peel morphology defect of thin-wall heat pipes after bending deformation was analyzed both for the macro-3D profile and for the micro-formation mechanism. The morphology and crystal orientations of the grains and annealing twins were carefully characterized utilizing optical metallography and the electron backscatter diffraction technique. The results show that after high-temperature sintering treatment, the matrix grains of the heat pipe are seriously coarsened and form a strong Goss texture, while certain annealing twins with the unique copper orientation are retained. The distribution of the Schmid factor value subjected to the uniaxial stress indicates that inhomogeneity in the intergranular deformation exists among the annealing twins and matrix grains. The annealing twin exhibits a “hard-oriented” component during the deformation; thus, it plays a role as a barrier and hinders the slipping of dislocation. As the strain accumulates, part of the annealing twins may protrude from the surface of the heat pipe, forming a large-scale fluctuation of the surface as the so-called “orange peel” morphology. The 3D profile shows the bulged twins mostly perpendicular to the drawing direction, about 200–300 in width and 10–20 μm in height. Full article

It is not realistic to optimize the roll pass design of profile rolling mills, which typically roll hundreds of profiles, using physical modelling or operational rolling. The use of reliable models of microstructure evolution is preferable here. Based on the mathematical equations describing the microstructure evolution during hot rolling, a modified microstructure evolution model was presented that better accounts for the influence of strain-induced precipitation (SIP) on the kinetics of static recrystallization. The time required for half of the structure to soften, t_0.5, by static recrystallization was calculated separately for both situations in which strain-induced precipitation occurred or did not occur. On this basis, the resulting model was more sensitive to the description of grain coarsening in the high-rolling-temperature region, which is a consequence of the rapid progress of static recrystallization and the larger interpass times during rolling on cross-country and continuous mills. The modified model was verified using a plain strain compression test (PSCT) simulation of rolling a 100-mm-diameter round bar performed on the Hydrawedge II hot deformation simulator (HDS-20). Four variants of simulations were performed, differing in the rolling temperature in the last four passes. For comparison with the outputs of the modified model, an analysis of the austenite grain size after rolling was performed using optical metallography. For indirect comparison with the model outputs, the SIP initiation time was determined based on the NbX precipitate size distribution obtained by TEM. Using the PSCT and the outputs from the modified microstructure evolution model, it was found that during conventional rolling, strain-induced precipitation occurs after the last pass and thus does not affect the austenite grain size. By lowering the rolling temperature, it was possible to reduce the grain size by up to 56 μm, while increasing the mean flow stress by a maximum of 74%. The resulting grain size for all four modes was consistent with the operating results. Full article

A material strength investigation along with a detailed microfractography analysis of fractures formed during static tensile tests of steel Armstal 550 was performed. The tests in this research were conducted in a temperature range of 298 to 973 K. In addition, during tensile tests at ambient temperature, optical measurements of strain maps and the curvature of the neck were performed. The minimum cross-sectional diameter and the radius of the neck curvature during tensile tests were obtained. The data can be directly used to obtain the true stress–strain curve. The material property analysis confirmed the high strength of the Armstal 550 alloy. The ultimate strength at room temperature equals 2.14 GPa, whereas the yield point equals 1.65 GPa. A decrease in the strength parameters along with an increase in temperature was noted. This is a typical phenomenon related to a change in the density and thermal expansion of steel under the influence of the temperature increase. For example, at a temperature of 500 °C, the ultimate strength is more than 50% less than at room temperature. An in-depth analysis of the metallography and microfractography of fractures resulting from static tensile tests showed the formation of atypical nano- and microstructures with an elongated shape. Local nano- and microstructures were observed at different levels of intensity for different temperatures. The largest clusters of nanoparticles were present on the surfaces of the specimens examined at a temperature of 973 K. Scanning microscopy analysis confirmed the presence of molybdenum oxides. Full article

Laser welding-brazing was used to join cemented carbide WC-Co and steel dissimilar materials. In this study, high-speed welding was adopted. The effect of welding parameters and brazing filler metals on the macrostructure, elemental diffusion, micro hardness and thermomechanical behavior was analyzed using optical metallography, scanning electron microscopy, electron probe micro-analysis, hardness test, and finite element method (FEM) based on thermo-elastic-plastic analysis. The experimental results show that increasing laser power is helpful to the increase of maximum welding speed. However, FEM also shows that increased welding speed leads to residual stress concentration, especial in the vicinity of jig. It is still a challenge to optimize laser power welding speed for a given brazing filler metal. The results show: when using pure copper, silver and nickel (thickness is less than 0.5 mm) as brazing filler metal, the combination, laser power of 1.2 kW and welding speed at 0.1 m/s, leads to complete penetration with good weld formation. However, when using Cu/Invar/Ni as brazing filler metal, laser power should increase to 1.7 kW if we still using a higher welding speed (0.1 m/s). Although a trial of high speed welding in laser welding-brazing exhibits feasibility, as-welded joints still have much more brittle risks due to the higher residual stresses. Full article

This work focused on the effects of laser energy density on the relative density, microstructure, and microhardness of Inconel 718 alloy manufactured by selective laser melting (SLM). The microstructural architectures, element segregation behavior in the interdendritic region and the evolution of laves phases of the as-SLMed IN718 samples were analyzed by optical metallography (OM), scanning electron microscopy (SEM), energy dispersive spectrometer (EDS), and electron probe microanalysis (EPMA). The results show that with an increase in the laser volume energy density, the relative density and the microhardness firstly increased and then decreased slightly. It also facilitates the precipitation of Laves phase. The variation of mechanical properties of the alloy can be related to the densification degree, microstructure uniformity, and precipitation phase content of Inconel 718 alloy. Full article