Search Results (44)

With advances in scientific foundations and engineering practice, segmented mirrors—a key architecture for realizing extremely large apertures and high-resolution imaging—have become foundational across space astronomy, ground-based telescopes, and advanced manufacturing. In recent years, interferometry, which leverages optical coherence and phase sensitivity, has become a powerful tool for inter-segment co-phasing. Its capabilities have advanced markedly owing to developments in multi-wavelength techniques, high-speed high-dynamic-range detectors, and instantaneous phase-shifting methods. Relative to non-interferometric sensing, interferometry directly encodes and unwraps phase. This enables a unified framework that combines millimeter-scale dynamic range with nanometer-level resolution throughout coarse acquisition, fine phasing, and in situ maintenance. This paper first outlines the degrees of freedom and error sources in segmented mirrors. It then reviews the configurations and acquisition strategies of shearing, Mach–Zehnder, Michelson, Fizeau, and PISTIL interferometers, and systematizes interferogram processing methods—such as phase-shifting, synthetic-wavelength techniques, and digital holography—for retrieving piston and tip/tilt. Accuracy of piston is λ/50–λ/100, and tip/tilt accuracy can reach the arcsecond level, with resolution at the nanometer scale. Finally, we discuss pathways to extend interferometric metrology from segmented mirrors to other discontinuous surfaces (e.g., segmented detectors, segmented gratings, microlens arrays) and outlines future research directions. Full article

We present some numerical results on piston and tilt detection by using the Young experiment with Genetic Algorithms (GAs). We have simulated the cophasing of a flat surface by following the experimental setup and the mathematical model for Optical Path Difference (OPD) in the Young experiment to characterize piston and tip–tilt misalignment images in the order of a few nanometers, considering diffraction effects and random noise of 5%. Thus, the best fitness obtained by the genetic algorithm is considered as a determining factor to decide a complete error measurement because the proposed algorithm is capable of extracting the values of piston and tilt separately, regardless of which error is present or both. As a result, we have developed a study on piston detection from (0.001, 10) mm with a tilt present in the same pattern from (0, $\lambda /2$) by using GAs embedded in a computational application. Full article

In the current highly industrialized living environment, air quality has become an increasing public health concern. Natural environments like forests have excellent air quality due to high concentrations of negative oxygen ions originating from low-voltage ionization, without harmful ozone. Traditional negative oxygen ion generators require high voltage for corona discharge to produce ions. However, high voltage can increase electron collisions and excitations, leading to more dissociation and recombination of oxygen molecules and consequently higher ozone production. To address the challenge of generating negative oxygen ions without accompanying ozone production, this study designed and constructed a low-voltage negative oxygen ion generator based on nanometer-tip carbon fiber electrodes. The advantage of this device lies in the high curvature radius of carbon fibers, which provides high local electric field strength. This allows for efficient production of negative oxygen ions at low operating voltages without generating ozone. Experiments demonstrated that the device can efficiently generate negative oxygen ions at a working voltage as low as 2.16 kV, 28% lower than the lowest voltage reported in similar studies. The purification device manufactured in this study had a total decay constant for PM_2.5 purification of 0.8967 min⁻¹ within five minutes, compared to a natural decay constant of only 0.0438 min⁻¹, resulting in a calculated Clean Air Delivery Rate (CADR) of 0.1535 m³/min. Within half an hour, concentrations of PM_2.5, PM₁, PM₁₀, formaldehyde, and TVOC were reduced by 99.09%, 99.40%, 99.37%, 94.39%, and 99.35%, respectively, demonstrating good decay constants and CADR. These findings confirm its effectiveness in improving indoor air quality, highlighting its significant application value in air purification. Full article

Millimeter-scale biopsy tools combined with an endoscope instrument have been widely used for minimal invasive surgery and medical diagnosis. Recently, a capsule-type endoscope was developed, which requires micromachining to fabricate micro-scale biopsy tools that have a sharp tip and other complex features, e.g., nanometer-scale end-tip sharpness and a complex scalpel design. However, conventional machining approaches are not cost-effective for mass production and cannot fabricate the micrometer-scale features needed for biopsy tools. Here, we demonstrate an electroplated nickel micro-biopsy tool which features a planar shape and is suitable to be equipped with a capsule-type endoscope. Planar-type micro-biopsy tools are designed, fabricated, and evaluated through in vitro tissue dissection experiments. Various micro-biopsy tools with a long shaft and sharp tip can be easily fabricated using a thick photoresist (SU8) mold via a simple one-step lithography and nickel electroplating process. The characteristics of various micro-biopsy tool design features, including a tip taper angle, different tool geometries, and a cutting scalpel, are evaluated for efficient tissue extraction from mice intestine. These fabricated biopsy tools have shown appropriate strength and sharpness with a sufficient amount of tissue extraction for clinical applications, e.g., cancer tissue biopsy. These micro-scale biopsy tools could be easily integrated with a capsule-type endoscope and conventional forceps. Full article

This study examines the electrical properties and layer quality of field emission microtriodes that have planar electrode geometry and are based on tungsten (W) and silicon dioxide (SiO₂). Two types of microtriodes were analyzed: one with a multi-tip cathode fabricated using photolithography (PL) and the other with a single-tip cathode fabricated using a focused ion beam (FIB). Atomic force microscopy (AFM) analysis revealed surface roughness of the W layer in the order of several nanometers (Ra = 3.8 ± 0.5 nm). The work function values of the Si substrate, SiO₂ layer, and W layer were estimated using low-energy ultraviolet photoelectron emission (PE) spectroscopy and were 4.71 eV, 4.85 eV, and 4.67 eV, respectively. The homogeneity of the W layer and the absence of oxygen and silicon impurities were confirmed via X-ray photoelectron spectroscopy (XPS). The PL microtriode and the FIB microtriode exhibited turn-on voltages of 110 V and 50 V, respectively, both demonstrating a field emission current of 0.4 nA. The FIB microtriode showed significantly improved field emission efficiency compared to the PL microtriode, attributed to a higher local electric field near the cathode. Full article

We report the microfabrication and characterization of concentric gold nanoring electrodes (Au NREs), which were fabricated by patterning two gold nanoelectrodes on the same silicon (Si) micropillar tip. Au NREs of 165 ± 10 nm in width were micropatterned on a 6.5 ± 0.2 µm diameter 80 ± 0.5 µm height Si micropillar with an intervening ~ 100 nm thick hafnium oxide insulating layer between the two nanoelectrodes. Excellent cylindricality of the micropillar with vertical sidewalls as well as a completely intact layer of a concentric Au NRE including the entire micropillar perimeter has been achieved as observed via scanning electron microscopy and energy dispersive spectroscopy data. The electrochemical behavior of the Au NREs was characterized by steady-state cyclic voltammetry and electrochemical impedance spectroscopy. The applicability of Au NREs to electrochemical sensing was demonstrated by redox cycling with the ferro/ferricyanide redox couple. The redox cycling amplified the currents by 1.63-fold with a collection efficiency of > 90% on a single collection cycle. The proposed micro-nanofabrication approach with further optimization studies shows great promise for the creation and expansion of concentric 3D NRE arrays with controllable width and nanometer spacing for electroanalytical research and applications such as single-cell analysis and advanced biological and neurochemical sensing. Full article

We demonstrate a highly sensitive acoustic vibration sensor based on a tapered-tip optical fiber acting as a microcantilever. The tapered-tip fiber has a unique output profile that exhibits a circular fringe pattern, whose distribution is highly sensitive to the vibration of the fiber tip. A piezo transducer is used for the acoustic excitation of the fiber microcantilever, which results in a periodic bending of the tip and thereby a significant output power modulation. Using a multimode readout fiber connected to an electric spectrum analyzer, we measured the amplitude of these power modulations over the 10–50 kHz range and observed resonances over certain frequency ranges. Two types of tapered-tip fibers were fabricated with diameter values of 1.5 µm and 1.8 µm and their frequency responses were compared with a non-tapered fiber tip. Thanks to the resonance effect as well as the sensitive fringe pattern of the tapered-tip fibers, the limit of detection and the sensitivity of the fiber sensor were obtained as 0.1 nm and 15.7 V/nm, respectively, which were significantly better than the values obtained with the non-tapered fiber tip (i.e., 1.1 nm and 0.12 V/nm, respectively). The sensor is highly sensitive, easy to fabricate, low-cost, and can detect sub-nanometer displacements, which makes it a promising tool for vibration sensing, particularly in the photoacoustic sensing of greenhouse gases. Full article

In recent decades, great efforts have been made to develop innovative, effective, and accurate nanofabrication techniques stimulated by the growing demand for nanostructures. Nowadays, mechanical tip-based emerged as the most promising nanolithography technique, allowing the pattern of nanostructures with a sub-nanometer resolution, high reproducibility, and accuracy. Unfortunately, these nanostructures result in contoured pile-ups that could limit their use and future integration into high-tech devices. The removal of pile-ups is still an open challenge. In this perspective, two different AFM-based approaches, i.e., Force Modulation Mode imaging and force-distance curve analysis, were used to characterize the structure of pile-ups at the edges of nanogrooves patterned on PMMA substrate by means of Pulse-Atomic Force Lithography. Our experimental results showed that the material in pile-ups was less stiff than the pristine polymer. Based on this evidence, we have developed an effective strategy to easily remove pile-ups, preserving the shape and the morphology of nanostructures. Full article

Magnetic Force Microscopy (MFM) is among the best techniques for examining and assessing local magnetic characteristics in surface structures at scales and sizes. It may be viewed as a unique way to operate atomic force microscopy with a ferromagnetic tip. The enhancement of magnetic signal resolution, the utilization of external fields during measurement, and quantitative data analysis are now the main areas of MFM development. We describe a new structure of MFM design based on a cryogen-free superconducting magnet. The piezoelectric tube (PZT) was implemented with a tip-sample coarse approach called SpiderDrive. The technique uses a magnetic tip on the free end of a piezo-resistive cantilever which oscillates at its resonant frequency. We obtained a high-quality image structure of the magnetic domain of commercial videotape under extreme conditions at 5 K, and a high magnetic field up to 11 T. When such a magnetic field was gradually increased, the domain structure of the videotape did not change much, allowing us to maintain the images in the specific regions to exhibit the performance. In addition, it enabled us to locate the sample region in the order of several hundred nanometers. This system has an extensive range of applications in the exploration of anisotropic magnetic phenomena in topological materials and superconductors. Full article

Force mapping of biological tissues via atomic force microscopy (AFM) probes the mechanical properties of samples within a given topography, revealing the interplay between tissue organization and nanometer-level composition. Despite considerable attention to soft biological samples, constructing elasticity maps on hard tissues is not routine for standard AFM equipment due to the difficulty of interpreting nanoindentation data in light of the available models of surface deformation. To tackle this issue, we proposed a protocol to construct elasticity maps of surfaces up to several GPa in moduli by AFM nanoindentation using standard experimental conditions (air operation, nanometrically sharp spherical tips, and cantilever stiffness below 30 N/m). We showed how to process both elastic and inelastic sample deformations simultaneously and independently and quantify the degree of elasticity of the sample to decide which regime is more suitable for moduli calculation. Afterwards, we used the frequency distributions of Young’s moduli to quantitatively assess differences between sample regions different for structure and composition, and to evaluate the presence of mechanical inhomogeneities. We tested our method on histological sections of sheep cortical bone, measuring the mechanical response of different osseous districts, and mapped the surface down to the single collagen fibril level. Full article

The use of focused ion and focused electron beam (FIB/FEB) technology permits the fabrication of micro- and nanometer scale geometries. Therefore, FIB/FEB technology is a favorable technique for preparing TEM lamellae, nanocontacts, or nanowires and repairing electronic circuits. This work investigates FIB/FEB technology as a tool for nanotip fabrication and quantum mechanical tunneling applications at a low tunneling voltage. Using a gas injection system (GIS), the Ga-FIB and FEB technology allows both additive and subtractive fabrication of arbitrary structures. Using energy dispersive X-ray spectroscopy (EDX), resistance measurement (RM), and scanning tunneling microscope (STM)/spectroscopy (STS) methods, the tunneling suitability of the utilized metal–organic material–platinum carbon (PtC) is investigated. Thus, to create electrode tips with radii down to 15 nm, a stable and reproducible process has to be developed. The metal–organic microstructure analysis shows suitable FIB parameters for the tunneling effect at high aperture currents (260 pA, 30 kV). These are required to ensure the suitability of the electrodes for the tunneling effect by an increased platinum content (EDX), a low resistivity (RM), and a small band gap (STM). The STM application allows the imaging of highly oriented pyrolytic graphite (HOPG) layers and demonstrates the tunneling suitability of PtC electrodes based on high FIB aperture currents and a low tunneling voltage. Full article

This work presents an overview of the latest results and new data on the optical response from spherical CdSe nanocrystals (NCs) obtained using surface-enhanced Raman scattering (SERS) and tip-enhanced Raman scattering (TERS). SERS is based on the enhancement of the phonon response from nanoobjects such as molecules or inorganic nanostructures placed on metal nanostructured substrates with a localized surface plasmon resonance (LSPR). A drastic SERS enhancement for optical phonons in semiconductor nanostructures can be achieved by a proper choice of the plasmonic substrate, for which the LSPR energy coincides with the laser excitation energy. The resonant enhancement of the optical response makes it possible to detect mono- and submonolayer coatings of CdSe NCs. The combination of Raman scattering with atomic force microscopy (AFM) using a metallized probe represents the basis of TERS from semiconductor nanostructures and makes it possible to investigate their phonon properties with nanoscale spatial resolution. Gap-mode TERS provides further enhancement of Raman scattering by optical phonon modes of CdSe NCs with nanometer spatial resolution due to the highly localized electric field in the gap between the metal AFM tip and a plasmonic substrate and opens new pathways for the optical characterization of single semiconductor nanostructures and for revealing details of their phonon spectrum at the nanometer scale. Full article

To realize quantum tunneling applications with movable electrodes, sharp tips with radii down to several tens of nanometers are necessary. The use of a focused ion beam (FIB) and focused electron beam (FEB) with a gas injection system (GIS) allows the integration of geometries in the nanoscale directly into micro and nano systems. However, the implementation of the tunneling effect clearly depends on the material. In this work, a metal-organic precursor is used. The investigation of the prepared tunneling electrodes enables an insight into FIB/FEB parameters for the realization of quantum tunneling applications. For this purpose, a high-resolution transmission electron microscopy (HRTEM) analysis is performed. The results show a dependence of the material nanostructure regarding platinum (Pt) grain size and distribution in an amorphous carbon matrix from the used beam and the FIB currents. The integration of the tips into a polysilicon (PolySi) beam and measuring the current signal by approaching the tips show significant differences in the results. Moreover, the approach of FEB tips shows a non-contact behavior even when the tips are squeezed together. The contact behavior depends on the grain size, proportion of platinum, and the amount of amorphous carbon in the microstructure, especially at the edge area of the tips. This study shows significant differences in the nanostructure between FIB and FEB tips, particularly for the FIB tips: The higher the ion current, the greater the platinum content, the finer the grain size, and the higher the probability of a tunneling current by approaching the tips. Full article

Magnetic force microscopy (MFM) belongs to the methods that enable spatially resolved magnetization measurements on common thin-film samples or magnetic nanostructures. The lateral resolution can be much higher than in Kerr microscopy, another spatially resolved magnetization imaging technique, but since MFM commonly necessitates positioning a cantilever tip typically within a few nanometers from the surface, it is often more complicated than other techniques. Here, we investigate the progresses in MFM on magnetic nanofibers that can be found in the literature during the last years. While MFM measurements on magnetic nanodots or thin-film samples can often be found in the scientific literature, reports on magnetic force microscopy on single nanofibers or chaotic nanofiber mats are scarce. The aim of this review is to show which MFM investigations can be conducted on magnetic nanofibers, where the recent borders are, and which ideas can be transferred from MFM on other rough surfaces towards nanofiber mats. Full article

Gradient nanostructure (GNS) has drawn great attention, owing to the unique deformation and properties that are superior to nanostructure with uniform scale. GNS is commonly fabricated via surface plastic deformation with small tips (of balls or shots) so as to produce high deformation to refine the coarse grains, but unfortunately it suffers from the deterioration of surface quality which is hard to guarantee the reliable service. Although there are mirror-finishing techniques that can greatly enhance the surface quality, the induced slight deformation is commonly unable to produce GNS of reasonable thickness. Here, we propose a method to fabricate a GNS surface layer with a substantially enhanced surface quality via ultra-sonic rolling treatment (USRT), namely, surface rolling with a roller vibrated at a frequency of 20,000 Hz. It is found that 4-pass USRT is able to produce 20–30 µm thick GNS on AISI 304 stainless steel pipe inner surface, wherein the surface quality is enhanced by one order of magnitude from the starting Ra = 3.92 µm to 0.19 µm. Processing by a roller with a high-frequency vibration is necessary for both good surface quality and the effective accumulation of heavy deformation on the surface. The flattening mechanism as well as the microstructural evolution from millimeter- to nanometer-scale for AISI 304 stainless steel is discussed. Full article