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Keywords = magnetostrictive powders

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11 pages, 1624 KiB  
Article
Microstructure and Magnetic Properties of Nanocrystalline Fe60−xCo25Ni15Six Alloy Elaborated by High-Energy Mechanical Milling
by Nawel Khitouni, Béchir Hammami, Núria Llorca-Isern, Wael Ben Mbarek, Joan-Josep Suñol and Mohamed Khitouni
Materials 2022, 15(18), 6483; https://doi.org/10.3390/ma15186483 - 19 Sep 2022
Cited by 7 | Viewed by 2389
Abstract
In the present work, the effect of Si addition on the magnetic properties of Fe60−xCo25Ni15Six (x = 0, 5, 10, 20, and 30 at%) alloys prepared by mechanical alloying was analyzed by X-ray diffraction and magnetic [...] Read more.
In the present work, the effect of Si addition on the magnetic properties of Fe60−xCo25Ni15Six (x = 0, 5, 10, 20, and 30 at%) alloys prepared by mechanical alloying was analyzed by X-ray diffraction and magnetic vibrating sample magnetometry and SQUID. The crystallographic parameters of the bcc-solid solutions were calculated by Rietveld refinement of the X-ray diffraction patterns with Maud software. Scanning electron microscopy (SEM) was used to determine the morphology of the powdered alloys as a function of milling time. It was found that the Si addition has an important role in the increase of structural hardening and brittleness of the particles (favoring the more pronounced refinement of crystallites). The resulting nanostructure is highlighted in accordance with the concept of the structure of defects. Magnetic properties were related to the metalloid addition, formed phases, and chemical compositions. All processed samples showed a soft ferromagnetic behavior (Hc ≤ 100 Oe). The inhomogeneous evolution of the magnetization saturation as a function of milling time is explained by the magnetostriction effective anisotropy and stress induced during mechanical alloying. Full article
(This article belongs to the Special Issue Novel Materials Synthesis by Mechanical Alloying/Milling (Volume II))
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12 pages, 4478 KiB  
Article
Static and Dynamic Magneto-Elastic Sensing Properties of Fe-Al Alloy Powder-Epoxy Composite Patches
by Suok-Min Na, Byungseok Yoo, Darryll J. Pines, Jin-Hyeong Yoo and Nicholas J. Jones
Magnetism 2022, 2(2), 105-116; https://doi.org/10.3390/magnetism2020008 - 1 Apr 2022
Cited by 1 | Viewed by 2451
Abstract
By combining the two types of magnetoelastic and magnetochromatic materials in an epoxy, we can make a hybrid system that exhibits an optical response due to an elastic strain. It could be used in structural health monitoring, for real-time monitoring of crack propagation [...] Read more.
By combining the two types of magnetoelastic and magnetochromatic materials in an epoxy, we can make a hybrid system that exhibits an optical response due to an elastic strain. It could be used in structural health monitoring, for real-time monitoring of crack propagation or general evaluation of the condition of a structure, both visualized by a change in color. In this study, magnetostrictive polymer composites (MPCs) with Fe81Al19 (Alfenol) alloy particles are evaluated to determine magneto-elastic properties in composite patches attached to a surface, prior to understanding the full hybrid magneto–elasto–optical interactions. To measure static magneto-elastic performance, a tension apparatus within a solenoid was fabricated to apply uniform strain to the MPC patch on an aluminum dog-bone substrate. It was demonstrated that, for epoxies with an elastic modulus higher than ~0.1 GPa, a tensile strain/stress applied to the composite improved magneto-elastic coupling, resulting in increased permeability values, at least up to strains of 0.1%. Composites were fabricated with both spherical and flake-shaped powders, with flake-shaped powders exhibiting better magnetic responses than those with spherical morphology. Alfenol MPCs were also measured dynamically at ultrasonic frequencies, exhibiting comparable dynamic sensing performance to Galfenol at 120 kHz using ultrasonic guided wave techniques. Full article
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24 pages, 6611 KiB  
Review
Laser Additive Manufacturing of Fe-Based Magnetic Amorphous Alloys
by Merve G. Ozden and Nicola A. Morley
Magnetochemistry 2021, 7(2), 20; https://doi.org/10.3390/magnetochemistry7020020 - 29 Jan 2021
Cited by 35 | Viewed by 6629
Abstract
Fe-based amorphous materials offer new opportunities for magnetic sensors, actuators, and magnetostrictive transducers due to their high saturation magnetostriction (λs = 20–40 ppm) and low coercive field compared with polycrystalline Fe-based alloys, which have high magnetostriction but large coercive fields and [...] Read more.
Fe-based amorphous materials offer new opportunities for magnetic sensors, actuators, and magnetostrictive transducers due to their high saturation magnetostriction (λs = 20–40 ppm) and low coercive field compared with polycrystalline Fe-based alloys, which have high magnetostriction but large coercive fields and Co-based amorphous alloys with small magnetostriction (λs = −3 to −5 ppm). Additive layer manufacturing (ALM) offers a new fabrication technique for more complex net-shaping designs. This paper reviews the two different ALM techniques that have been used to fabricate Fe-based amorphous magnetic materials, including the structural and magnetic properties. Selective laser melting (SLM)—a powder-bed fusion technique—and laser-engineered net shaping (LENS)—a directed energy deposition method—have both been utilised to fabricate amorphous alloys, owing to their high availability and low cost within the literature. Two different scanning strategies have been introduced by using the SLM technique. The first strategy is a double-scanning strategy, which gives rise to maximum relative density of 96% and corresponding magnetic saturation of 1.22 T. It also improved the glassy phase content by an order of magnitude of 47%, as well as improving magnetic properties (decreasing coercivity to 1591.5 A/m and increasing magnetic permeability to around 100 at 100 Hz). The second is a novel scanning strategy, which involves two-step melting: preliminary laser melting and short pulse amorphisation. This increased the amorphous phase fraction to a value of up to 89.6%, and relative density up to 94.1%, and lowered coercivity to 238 A/m. On the other hand, the LENS technique has not been utilised as much as SLM in the production of amorphous alloys owing to its lower geometric accuracy (0.25 mm) and lower surface quality, despite its benefits such as providing superior mechanical properties, controlled composition and microstructure. As a result, it has been commonly used for large parts with low complexity and for repairing them, limiting the production of amorphous alloys because of the size limitation. This paper provides a comprehensive review of these techniques for Fe-based amorphous magnetic materials. Full article
(This article belongs to the Special Issue Soft and Hard Magnetic Materials: Latest Advances and Prospects)
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13 pages, 915 KiB  
Article
Large-Scale Shape Transformations of a Sphere Made of a Magnetoactive Elastomer
by Oleg Stolbov and Yuriy Raikher
Polymers 2020, 12(12), 2933; https://doi.org/10.3390/polym12122933 - 8 Dec 2020
Cited by 12 | Viewed by 2497
Abstract
Magnetostriction effect, i.e., deformation under the action of a uniform applied field, is analyzed to detail for a spherical sample of a magnetoactive elastomer (MAE). A close analogy with the field-induced elongation of spherical ferrofluid droplets implies that similar characteristic effects viz. hysteresis [...] Read more.
Magnetostriction effect, i.e., deformation under the action of a uniform applied field, is analyzed to detail for a spherical sample of a magnetoactive elastomer (MAE). A close analogy with the field-induced elongation of spherical ferrofluid droplets implies that similar characteristic effects viz. hysteresis stretching and transfiguration into a distinctively nonellipsoidal bodies, should be inherent to MAE objects as well. The absence until now of such studies seems to be due to very unfavorable conclusions which follow from the theoretical estimates, all of which are based on the assumption that a deformed sphere always retains the geometry of ellipsoid of revolution just changing its aspect ratio under field. Building up an adequate numerical modelling tool, we show that the ‘ellipsoidal’ approximation is misleading beginning right from the case of infinitesimal field strengths and strain increments. The results obtained show that the above-mentioned magnetodeformational effect should distinctively manifest itself in the objects made of quite ordinary MAEs, e.g., composites on the base of silicone cautchouc filled with micron-size carbonyl iron powder. Full article
(This article belongs to the Special Issue Magnetic Polymer Composites: Design and Application)
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12 pages, 4716 KiB  
Article
A Low-Cost Current Sensor Based on Semi-Cylindrical Magnetostrictive Composite
by Shaoyi Xu, Qiang Peng, Fangfang Xing, Hongyu Xue, Junwen Sun, Lei Ma and Ming Li
Electronics 2020, 9(11), 1833; https://doi.org/10.3390/electronics9111833 - 3 Nov 2020
Cited by 9 | Viewed by 2219
Abstract
This paper presents the design, fabrication, and characterization of a compact current sensor based on magnetostrictive composites and resistance strain gauges. Firstly, we designed three kinds of current sensors with different structures, in which the shape of the giant magnetostrictive material (GMM) was [...] Read more.
This paper presents the design, fabrication, and characterization of a compact current sensor based on magnetostrictive composites and resistance strain gauges. Firstly, we designed three kinds of current sensors with different structures, in which the shape of the giant magnetostrictive material (GMM) was cuboid, cylindrical, and semi-cylindrical. A set of finite element method (FEM) simulations were performed to qualitatively guide the design of three prototypes of the current sensor. It was determined that the most ideal shape of the GMM was semi-cylindrical. Secondly, Terfenol-D (TD) powder and epoxy resin were mixed to prepare magnetostrictive composites. In this paper, magnetostrictive composites with different particle size ranges and mass ratio were prepared and tested. The results show that the magnetostrictive composites had the best performance when the particle size range was 149–500 μm and the mass ratio of epoxy resin to TD powder was 1:5. Finally, this paper tested the performance of the sensor. The sensitivity, repeatability, and linear working range of the sensor reached 0.104 με/A, 2.51%, and 100–900 A respectively, when only 0.31 g of TD powder was employed. This means that current measurement with low cost, high sensitivity, and wide range was realized. Full article
(This article belongs to the Section Systems & Control Engineering)
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16 pages, 7256 KiB  
Article
Glass-Forming Ability and Soft Magnetic Properties of (Co75Ti25)100−xFex (x; 0–20 at.%) Systems Fabricated by SPS of Mechanically Alloyed Nanopowders
by Mohamed Sherif El-Eskandarany, Naser Ali and Maryam Saeed
Nanomaterials 2020, 10(5), 849; https://doi.org/10.3390/nano10050849 - 28 Apr 2020
Cited by 13 | Viewed by 3349
Abstract
Due to their outstanding mechanical properties and soft magnetic characteristics, cobalt-based metallic glassy alloys have stimulated much interesting research. These metastable ferromagnetic materials possess very small magnetocrystalline anisotropy, and almost zero magnetostriction. They reveal low coercivity, extremely low core loss, moderate saturation polarization, [...] Read more.
Due to their outstanding mechanical properties and soft magnetic characteristics, cobalt-based metallic glassy alloys have stimulated much interesting research. These metastable ferromagnetic materials possess very small magnetocrystalline anisotropy, and almost zero magnetostriction. They reveal low coercivity, extremely low core loss, moderate saturation polarization, and very high magnetism. Despite these attractive physical behaviors, Co-based metallic glasses are difficult to obtain by the melting/casting and conventional rapid solidification techniques due to their poor glass-forming ability. In the present study, we succeed in preparing (Co75Ti25)100−xFex (x; 0–20 at.%) metallic glassy powders, using a mechanical alloying approach. The end product of the as-prepared powders was consolidated into full dense cylinders with large-diameter and thickness (2 × 2 cm), using spark plasma sintering technique. The results have shown that the consolidation step did not lead to any undesired crystallizations or phase transformations, and the as-consolidated buttons maintained their unique short-range order structure. These bulk metallic glassy systems possessed high glass-transition and crystallization temperatures, suggesting their high thermal stability. However, they showed low values of the reduced glass-transition temperatures, indicating that this system is difficult to prepare by the conventional way of preparations. Full article
(This article belongs to the Section Synthesis, Interfaces and Nanostructures)
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15 pages, 4391 KiB  
Article
A Guided Wave Transducer with Sprayed Magnetostrictive Powder Coating for Monitoring of Aluminum Conductor Steel-Reinforced Cables
by Fuzai Lv, Pengfei Zhang, Zhifeng Tang, Yonggang Yue and Keji Yang
Sensors 2019, 19(7), 1550; https://doi.org/10.3390/s19071550 - 30 Mar 2019
Cited by 19 | Viewed by 4673
Abstract
Aluminum conductor steel-reinforced (ACSR) cables are typically used in overhead transmission lines, requiring stringent non-destructive testing owing to the severe conditions they face. Ultrasonic guided wave inspection provides promising online monitoring of the wire breakage of cables with the advantages of high sensitivity, [...] Read more.
Aluminum conductor steel-reinforced (ACSR) cables are typically used in overhead transmission lines, requiring stringent non-destructive testing owing to the severe conditions they face. Ultrasonic guided wave inspection provides promising online monitoring of the wire breakage of cables with the advantages of high sensitivity, long-range inspection, and full cross-sectional coverage. It is a very popular method to generate and receive guided waves using magnetostrictive and piezoelectric transducers. However, uniformly coupling the acoustic energy excited by transducers into multi-wire structures is always a challenge in the field application of guided waves. Long-term field application of piezoelectric transducers is limited due to the small coupling surface area, localized excitation, and couplant required. Conventional magnetostrictive transducers for steel strand inspection are based on the magnetostrictive effect of the material itself. Two factors affect the transducing performance of the transducers on ACSR cables. On one hand, there is a non-magnetostrictive effect in aluminum wires. On the other hand, the magnetostriction of the innermost steel wires is too weak to generate guided waves. The bias magnetic field is attenuated by the outer layers of aluminum wires. In this paper, an alternative sprayed magnetostrictive powder coating (SMPC) transducer was developed for guided wave generation and detection in ACSR cables. The Fe83Ga17 alloy powder with large magnetostriction was sprayed uniformly on the surfaces of certain sections of the outermost aluminum wires where the transducer would be installed. Experimental investigations were carried out to generate and receive the most commonly used L(0,1) guided waves for wire breakage detection at frequencies of 50 and 100 kHz. The results demonstrate that the discernable reflected waves of the cable end and an artificial defect of three-wire breakage (5.5% reduction in the cable’s cross-sectional area) were received by the transducer with SMPC, which was impossible for the transducer without SMPC. This method makes long-term and online monitoring of ACSR cables feasible due to the high coupling efficiency and good structural surface adaptability. Full article
(This article belongs to the Special Issue Guided-Wave Acoustic Sensors)
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9 pages, 11847 KiB  
Article
Structural Effects of Magnetostrictive Materials on the Magnetoelectric Response of Particulate CZFO/NKNLS Composites
by Moon Hyeok Choi, Kyujin Ko and Su Chul Yang
Materials 2019, 12(7), 1053; https://doi.org/10.3390/ma12071053 - 30 Mar 2019
Cited by 5 | Viewed by 3869
Abstract
In this study, magnetostrictive powders of CoFe2O4 (CFO) and Zn-substituted CoFe2O4 (CZFO, Zn = 0.1, 0.2) were synthesized in order to decrease the optimal dc magnetic field (Hopt.), which is required to obtain a [...] Read more.
In this study, magnetostrictive powders of CoFe2O4 (CFO) and Zn-substituted CoFe2O4 (CZFO, Zn = 0.1, 0.2) were synthesized in order to decrease the optimal dc magnetic field (Hopt.), which is required to obtain a reliable magnetoelectric (ME) voltage in a 3-0 type particulate composite system. The CFO powders were prepared as a reference via a typical solid solution process. In particular, two types of heterogeneous CZFO powders were prepared via a stepwise solid solution process. Porous-CFO and dense-CFO powders were synthesized by calcination in a box furnace without and with pelletizing, respectively. Then, heterogeneous structures of pCZFO and dCZFO powders were prepared by Zn-substitution on calcined powders of porous-CFO and dense-CFO, respectively. Compared to the CFO powders, the heterogeneous pCZFO and dCZFO powders exhibited maximal magnetic susceptibilities (χmax) at lower Hdc values below ±50 Oe and ±10 Oe, respectively. The Zn substitution effect on the Hdc shift was more dominant in dCZFO than in pCZFO. This might be because the Zn ion could not diffuse into the dense-CFO powder, resulting in a more heterogeneous structure inducing an effective exchange-spring effect. As a result, ME composites consisting of 0.948Na0.5K0.5NbO3–0.052LiSbO3 (NKNLS) with CFO, pCZFO, and dCZFO were found to exhibit Hopt. = 966 Oe (NKNLS-CFO), Hopt. = 689–828 Oe (NKNLS-pCZFO), and Hopt. = 458–481 Oe (NKNLS-dCZFO), respectively. The low values of Hopt. below 500 Oe indicate that the structure of magnetostrictive materials should be considered in order to obtain a minimal Hopt. for high feasibility of ME composites. Full article
(This article belongs to the Special Issue Functional Electroceramics)
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5 pages, 653 KiB  
Proceeding Paper
Fabrication Methods for High-Performance Miniature Disks of Terfenol-D for Energy Harvesting
by Valentin Issindou, B. Viala, L. Gimeno, O. Cugat, C. Rado and S. Bouat
Proceedings 2017, 1(4), 579; https://doi.org/10.3390/proceedings1040579 - 8 Aug 2017
Viewed by 2195
Abstract
In this paper, we compare different techniques to manufacture high-performance miniature disks of Terfenol-D aiming at self-powered IoT sensors. To reach large in-plane magnetostriction while maintaining low driving field, microstructure engineering is essential. This work covers monocrystalline, polycrystalline and hot-pressed powder materials whose [...] Read more.
In this paper, we compare different techniques to manufacture high-performance miniature disks of Terfenol-D aiming at self-powered IoT sensors. To reach large in-plane magnetostriction while maintaining low driving field, microstructure engineering is essential. This work covers monocrystalline, polycrystalline and hot-pressed powder materials whose performances are analyzed. A “performance phase diagram per technique” is reported at the end. Full article
(This article belongs to the Proceedings of Proceedings of Eurosensors 2017, Paris, France, 3–6 September 2017)
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