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Keywords = layer-through fracturing

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49 pages, 95844 KB  
Article
Deformation Style and Structural Architecture of Faulted Well-Layered Platform Carbonates, Raparo Mt., Southern Italy
by Aji Maina Kyari, Ian Bala Abdallah, Eugenia Romaniello, Giacomo Prosser and Fabrizio Agosta
Geosciences 2026, 16(7), 246; https://doi.org/10.3390/geosciences16070246 (registering DOI) - 23 Jun 2026
Abstract
The results of a multiscale study of fault and fracture geometry, distribution, density, and intensity are reported for Mesozoic platform carbonates cropping out along the axial zones of the southern Apennines fold-and-thrust belt, Italy. By integrating field structural observations with digital outcrop analysis, [...] Read more.
The results of a multiscale study of fault and fracture geometry, distribution, density, and intensity are reported for Mesozoic platform carbonates cropping out along the axial zones of the southern Apennines fold-and-thrust belt, Italy. By integrating field structural observations with digital outcrop analysis, the study focuses on Cretaceous limestone rocks exposed along natural creeks and artificial trails of the Castelsaraceno area, Raparo Mt., southern Italy. There, the limestone beds are bounded by mm- to cm-thick marly–clayey interbeds, forming a well-layered succession made up of a few m-thick bed packages bounded by several cm-thick clayish interlayers. The carbonate multilayer was first affected by thrust tectonics, with the formation of low-angle intra-carbonate thrust faults and fault bend-folding. Then, the multilayer was crosscut by extensional–transtensional high-angle faults, which displaced the previously formed contractional structural elements, and allowed carbonate exhumation from shallow crustal depths. At outcrop scales, thrust-related deformation was solved by low-angle joints and veins, rare high-angle stylolites, and low-angle sheared fractures displaying reverse kinematics. Quantitative analyses of fracture density (P20) and intensity (P21) conducted on selected portions of the thrust fault zones indicate that the low-angle joints and veins attain their highest values in the vicinity of the main slip surfaces, whereas they are almost absent in the surrounding carbonate host rocks. Plio-Quaternary transtensional deformation was solved by NW–SE- and NE–SW striking faults. The latter fault set, nicely exposed along the flanks of the Raganello Creek, was characterized by right-lateral components of slip. Incipient faults, with ca. 1 cm throw, are made up of vertically discontinuous slip surfaces, which crosscut single bed packages and abut against clayish interlayers. The slip surfaces form conjugate geometries, and are associated to high-angle fractures and veins striking NE–SW, dissecting the bed packages. The fault core is virtually absent, whereas the damage zones are very discontinuous along dip. The P20 values computed for the high-angle fractures and veins increase toward the slip surfaces, whereas the P21 values remain nearly constant. These data are interpreted as being due to fault nucleation processes associated with fracture nucleation within the limestone rocks. NE–SW striking small faults displaying throws between 10 and 60 cm are comprised of through-going main slip surfaces crosscutting multiple bed packages, and poorly developed, discontinuous fault cores flanked by m-thick damage zones. The damage zones include sub-parallel high-angle shear fractures, fractures and veins showing a positive correlation between P20 and P21, whose values increase in the vicinity of the main slip surfaces. Such a positive correlation is interpreted as due to fault growth by linkage and coalescence of pre-existing high-angle fractures, and formation of fault-related joints and veins at the extensional quadrants of single shear fractures. Similarly, large-scale NE–SW striking mature faults with throws on the order of tens of meters, made up of a m-thick fault core and 10 s of m-thick damage zones including sub-parallel fractures and veins, also show a positive P20 and P21 correlation. The main outputs of this work are synthesized into a conceptual model illustrating the transition from thrust-related deformation to extensional–transtensional faulting, documenting the evolution of fracture networks from incipient-to-small-to-mature faults. Full article
(This article belongs to the Section Structural Geology and Tectonics)
19 pages, 28769 KB  
Article
Differences in Microstructure and Properties of 16 mm Thick 6082 Aluminum Alloy Under Different Heat Source Conditions
by Zan Ju, Ruxu Huang, Xiaozhong Xie, Shu Liu, Feiyun Wang and Juan Fu
Coatings 2026, 16(6), 739; https://doi.org/10.3390/coatings16060739 (registering DOI) - 21 Jun 2026
Viewed by 156
Abstract
6082 aluminum alloy is widely applied in marine engineering, rail transportation and other industries owing to its excellent comprehensive performance. Welding heat source characteristics exert a decisive influence on the microstructure and mechanical properties of welded joints and become a major constraint for [...] Read more.
6082 aluminum alloy is widely applied in marine engineering, rail transportation and other industries owing to its excellent comprehensive performance. Welding heat source characteristics exert a decisive influence on the microstructure and mechanical properties of welded joints and become a major constraint for the application of medium-thick aluminum alloy welded structures. In this work, comparative tests of TIG and MIG welding were carried out on 16 mm thick 6082 aluminum alloy plates. Combining thermal simulation, metallographic observation and mechanical property tests, the temperature field distribution, microstructure, microhardness, tensile properties and bending properties of the two kinds of joints were systematically studied. The results show that TIG welding possesses high heat input, forming a broad temperature field with steep thermal gradients. Its weld microstructure is coarse and accompanied by severe coarsening of Mg2Si precipitates, and the joint presents a highly fluctuating M-shaped microhardness distribution. The average tensile strength of TIG welded joints is 194 MPa, and all specimens fracture in the heat-affected zone. By contrast, MIG welding with low heat input produces a uniform temperature field, as well as a fine and homogeneous weld microstructure with dispersed precipitates. Its microhardness distribution is stable, and the average tensile strength reaches 256 MPa, 32% higher than that of TIG joints. Both welding methods deliver favorable bending performance. The difference in heat input and cooling behavior changes the grain evolution and precipitate characteristics and further dominates the final mechanical performance of joints. MIG welding is more suitable for multi-layer, multi-pass welding of 16 mm thick 6082 aluminum alloy. This work clarifies the correlation between heat input, microstructure and mechanical properties, and the optimized process can effectively improve the microstructural uniformity of the weld joint and enhance its mechanical properties. Full article
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31 pages, 20808 KB  
Article
Fracture Mode Transition and Energy Dissipation of Brittle Coal Under Confinement Induced by a Flexible Polyurea Coating
by Shan Ning, Weibing Zhu, Biao Fu, Pengjun Gao and Zishuo Jia
Polymers 2026, 18(12), 1538; https://doi.org/10.3390/polym18121538 (registering DOI) - 20 Jun 2026
Viewed by 225
Abstract
Brittle geomaterials such as coal and rock are prone to unstable failure under high stress and dynamic disturbances, where rapid release of stored elastic strain energy can trigger dynamic disasters. Polyurea, a high-strength and high-ductility elastomer, can form a continuous flexible coating on [...] Read more.
Brittle geomaterials such as coal and rock are prone to unstable failure under high stress and dynamic disturbances, where rapid release of stored elastic strain energy can trigger dynamic disasters. Polyurea, a high-strength and high-ductility elastomer, can form a continuous flexible coating on the surface of coal/rock to regulate their deformation–fracture behavior. Here, uniaxial compression tests were performed on coal specimens coated with polyurea layers of different thicknesses (0–1.25 mm). Acoustic emission (AE) and digital image correlation (DIC) were jointly employed to characterize macroscopic deformation, microcrack evolution, fracture-mode transition, and energy partitioning. The results show that polyurea provides passive lateral confinement that suppresses lateral expansion and shifts macroscopic failure from brittle splitting to progressive ductile damage. AE-based AF–RA analysis indicates that thicker coatings increase the normal stress and shear resistance along potential fracture planes, promoting a microfracture transition from shear-dominated to tension-dominated cracking. Energy analysis demonstrates that the coating enhances pre-peak energy dissipation via coordinated deformation with the coal, while thicker coatings (≥1.00 mm) exhibit pronounced post-peak elastic tensile deformation to absorb and buffer fracture-released energy, impeding the instantaneous energy release typical of bare coal. Moreover, the elastic energy index shows that polyurea markedly reduces impact tendency, with an appropriate thickness stabilizing specimens from strong to weak/non-impact propensity. These findings clarify the coupled confinement–fracture–energy regulation mechanisms of polyurea coatings and provide quantitative guidance for coating-thickness design to mitigate dynamic failure hazards in brittle materials. Full article
(This article belongs to the Section Polymer Networks and Gels)
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15 pages, 2877 KB  
Article
Oxidation Behavior of TiCN-HfC-WC Cermet at High Temperature
by Zhihui Wang, Jiaojiao Gao, Jiabao Liu and Jinpeng Song
Materials 2026, 19(12), 2648; https://doi.org/10.3390/ma19122648 (registering DOI) - 19 Jun 2026
Viewed by 143
Abstract
In this investigation, with increasing oxidation time or temperature, the observed mass gain abided by the parabolic law. TiCN-HfC-WC cermet contained different layers, with each one having a unique composition. Thermal fracture occurred in the sub-oxidation layer, and the flexural strength gradually decreased [...] Read more.
In this investigation, with increasing oxidation time or temperature, the observed mass gain abided by the parabolic law. TiCN-HfC-WC cermet contained different layers, with each one having a unique composition. Thermal fracture occurred in the sub-oxidation layer, and the flexural strength gradually decreased from 1270.6 MPa to 149.9 MPa. Ther-mal stress equations for calculating the radial, circumferential, and axial stresses were es-tablished. The thermal stress differences between neighboring layers determined the ther-mal fracture; when they were zero, the physical parameters of the layers were related, which could be used to guide cermet material design. Full article
(This article belongs to the Section Advanced and Functional Ceramics and Glasses)
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28 pages, 4167 KB  
Article
Sedimentary Evolution and Reservoir Formation of the Late Triassic Bolila Formation in the Central Qiangtang Basin, Tibet
by Shangke Xie, Haisheng Yi, Wangzhong Zhan, Ruiyu Cheng, Wei Sun, Shengqiang Zeng, Qian Hou and Keyu Zhu
Minerals 2026, 16(6), 641; https://doi.org/10.3390/min16060641 (registering DOI) - 18 Jun 2026
Viewed by 214
Abstract
The Late Triassic Bolila Formation in the central Qiangtang Basin is a typical carbonate buildup deposited during a regional transgression in the eastern Tethyan realm. Understanding its sedimentary evolution and reservoir-forming mechanisms is crucial for hydrocarbon exploration. This study integrates petrology, detrital zircon [...] Read more.
The Late Triassic Bolila Formation in the central Qiangtang Basin is a typical carbonate buildup deposited during a regional transgression in the eastern Tethyan realm. Understanding its sedimentary evolution and reservoir-forming mechanisms is crucial for hydrocarbon exploration. This study integrates petrology, detrital zircon U-Pb geochronology, carbon-oxygen isotopes, and reservoir property analysis of the Quemudongda section. The results show: (1) detrital zircon dating provides a maximum depositional age of 225.7–235.7 Ma (Carnian–Norian), correcting the previous Jurassic misassignment on the 1:250,000 geological map. Carbon-oxygen isotopes (average δ13C = +3.2‰, δ18O = −11.1‰) are consistent with the global Carnian–Norian positive δ13C excursion. (2) The section reveals a platform-margin reef (hexactinellid and calcareous sponges) and slump breccia (seven layers) association, representing a steep-rimmed carbonate platform margin. The sedimentary evolution comprises three stages: reef initiation, reef flourishing with frequent slumping, and reef decline with dolomitization. (3) Reservoirs are mainly breccia and reef dolostones, with intergranular, intercrystalline, and fracture-related pores. Porosity averages 2.8% (0.8%–7.2%), permeability averages 0.35 mD (0.001–8.5 mD), defining a low-porosity, ultra-low-permeability fracture-pore reservoir. Breccia dolostone has better properties (porosity 3.71%, permeability 2.412 mD). (4) Reservoir formation is controlled by sedimentation (platform-margin facies), diagenesis (dolomitization generates pores, but high-temperature recrystallization causes densification), and tectonics (microfractures enhance permeability). High-quality reservoirs occur where breccia dolostone and fractures overlap. (5) The Bolila reef-shoal complex and the overlying Bagong Formation source rocks form a “lower reservoir—upper source” assemblage, representing a new exploration target in the Tuonamu area. The breccia dolostone–fracture overlap zone is the core “sweet spot”. Full article
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16 pages, 5197 KB  
Article
High-Temperature Tribological Behavior and Wear Mechanisms of Stellite 6 Alloy
by Kai Jiang, Hongbin Lu, Weijie Chen, Fei Sun, Zhe Luo and Xiaomeng Gu
Materials 2026, 19(12), 2629; https://doi.org/10.3390/ma19122629 - 18 Jun 2026
Viewed by 172
Abstract
The temperature-dependent wear behavior of a cobalt-based Stellite 6 alloy was investigated from room temperature (RT) to 800 °C using high-temperature reciprocating sliding tests. The friction coefficient decreases monotonically with increasing temperature, from about 0.56 ± 0.12 at RT to 0.26 ± 0.11 [...] Read more.
The temperature-dependent wear behavior of a cobalt-based Stellite 6 alloy was investigated from room temperature (RT) to 800 °C using high-temperature reciprocating sliding tests. The friction coefficient decreases monotonically with increasing temperature, from about 0.56 ± 0.12 at RT to 0.26 ± 0.11 at 800 °C, whereas the wear rate exhibits a pronounced non-monotonic evolution. Specifically, the wear rate increases from 18.4 ± 1.5 × 10−6 mm3·N−1·m−1 at RT to a maximum of 54.8 ± 1.6 × 10−6 mm3·N−1·m−1 at 600 °C, followed by an anomalous reduction to 10.2 ± 1.5 × 10−6 mm3·N−1·m−1 at 800 °C, which is even lower than that at RT. Microstructural and elemental analyses indicate that this behavior is governed by the temperature-dependent evolution of oxide layers. At RT–600 °C, thin and mechanically unstable oxide films repeatedly form and fracture, promoting oxidation-assisted abrasive and adhesive wear. In contrast, at 800 °C, a continuous and dense oxide layer forms and acts as a stable tribo-oxide film, effectively suppressing severe material removal. These findings clarify the temperature-driven wear mechanism transition of Stellite 6 alloy under high-temperature sliding conditions. Full article
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22 pages, 5549 KB  
Article
Mechanisms of Cross-Layer Fracturing in Thin Interbedded Formations: Roles of Stress Shadow, Interlayer Stress Difference, and Interface Failure
by Zhi Chang, Runsen Li, Mingfang He, Linjun Zou and Xinjia Liu
Processes 2026, 14(12), 1966; https://doi.org/10.3390/pr14121966 - 17 Jun 2026
Viewed by 201
Abstract
Hydraulic fracture height growth in thin sandstone–mudstone interbeds is often limited by bedding interface failure and multi-cluster stress interference. In this study, a coupled fracture–matrix interface finite element model was developed for the He-8 sandstone–mudstone interbeds in the Sulige Gas Field and validated [...] Read more.
Hydraulic fracture height growth in thin sandstone–mudstone interbeds is often limited by bedding interface failure and multi-cluster stress interference. In this study, a coupled fracture–matrix interface finite element model was developed for the He-8 sandstone–mudstone interbeds in the Sulige Gas Field and validated against previously published true triaxial hydraulic fracturing experiments. The simulations indicate that vertical–horizontal stress difference (VSD; the difference between overburden stress and minimum horizontal stress within a layer) promotes fracture-height growth, whereas interlayer stress difference (ISD; the minimum horizontal stress contrast between adjacent layers) acts as a stress barrier that promotes bedding interface shear failure and arrests vertical growth. For the investigated reservoir configuration, each 4 MPa increase in VSD increased fracture height by approximately 1.5 m in the three-cluster case and 1.8 m in the four-cluster case, whereas each 2 MPa increase in ISD reduced the average fracture height by approximately 4.0 m in the three-cluster case and 3.5 m in the four-cluster case. Under moderate ISD, increasing the fluid viscosity was more effective than increasing the injection rate alone, although the benefit depended on cluster number and interface failure state. These results clarify how stress contrast, interface strength, and multi-cluster stress shadows jointly control cross-layer fracture propagation in thin interbedded reservoirs. Full article
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23 pages, 32139 KB  
Article
Mining-Induced Deformation and Slope Stability in Steep Mountainous Areas Based on InSAR Monitoring and Rock Movement Theory: A Case Study from Southwestern China
by Xiaoqiang Chen, Xin Yao, Zhenkai Zhou, Xuwen Tian, Tao Tao, Qiyu Li, Yi Wen and Guangyao Song
Remote Sens. 2026, 18(12), 2008; https://doi.org/10.3390/rs18122008 - 16 Jun 2026
Viewed by 219
Abstract
Geological disasters are frequently triggered in steep mountainous mining areas due to the coupling effects of underground excavation and slope stability, yet the applicability of traditional rock movement theories in such terrains remains unclear. This study investigates an extremely steep coal mine in [...] Read more.
Geological disasters are frequently triggered in steep mountainous mining areas due to the coupling effects of underground excavation and slope stability, yet the applicability of traditional rock movement theories in such terrains remains unclear. This study investigates an extremely steep coal mine in southwestern China, integrating engineering geological surveys, unmanned aerial vehicle (UAV) measurements, InSAR monitoring, and rock movement theoretical calculations to analyze the impact of mining on mountain deformation and slope stability. The results show that the study area exhibits steep slopes (55–85°) and gently inclined, reverse-layered rock masses controlled by structural fracture zones, creating a geological environment prone to mining-induced landslides. The 1151 working face lies at a depth of 286–470 m, with a protective coal pillar of approximately 160 m left between the excavation and the cliff zone. InSAR monitoring indicates cumulative LOS deformation rates of −0.98 to 0.55 cm/a, with subsidence concentrated above the working face, while existing landslides in the cliff zone show no significant deformation. Comparison between theoretical calculations and InSAR inversion reveals that InSAR boundary angles (downslope 61–68°, upslope 67–73°) exceed theoretical predictions (downslope 48–52°, upslope 55°), indicating that complex topography and rock mass structure constrain mining-induced deformation propagation. The findings demonstrate that appropriately designed protective coal pillars and avoidance of unstable slopes can effectively mitigate the impact of mining-induced disturbances on existing hazards. This study provides valuable reference for landslide risk assessment and disaster prevention in extremely steep mining regions. Full article
(This article belongs to the Section Engineering Remote Sensing)
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26 pages, 76890 KB  
Article
Combining High-Frequency GPR, Laser Scanning, and Digital Photogrammetry to Guide the Detachment of a Roman Mosaic in the Latomia dei Niccolini in Marsala (Italy)
by Alessandra Carollo, Patrizia Capizzi, Raffaele Martorana, Alessandro Abrignani, Angelina Castiglia and Mauro Lo Brutto
Appl. Sci. 2026, 16(12), 6095; https://doi.org/10.3390/app16126095 - 16 Jun 2026
Viewed by 237
Abstract
This study presents the diagnostic and conservation work carried out on the Roman mosaic of the South cubiculum in the Latomia dei Niccolini (Marsala, western Sicily). The mosaic, decorated with polychrome tesserae featuring a kantharos motif, presented severe structural damage, including fractures, subsurface [...] Read more.
This study presents the diagnostic and conservation work carried out on the Roman mosaic of the South cubiculum in the Latomia dei Niccolini (Marsala, western Sicily). The mosaic, decorated with polychrome tesserae featuring a kantharos motif, presented severe structural damage, including fractures, subsurface voids, and progressive material loss. To assess the causes of deterioration and design an effective conservation strategy, an integrated approach combining non-invasive geophysical and 3D survey methods was applied. Ground-penetrating radar (GPR) was selected as the main diagnostic tool because it allows high-resolution subsurface imaging while preserving the integrity of the fragile mosaic surface. By utilizing high-frequency 2 GHz antennas and complementary video inspection, a significant subsurface cavity beneath the mosaic preparation layer was successfully mapped, determining its critical relationship with the main diagonal surface fracture. Simultaneously, laser scanning and close-range photogrammetry enabled the creation of accurate 3D models supporting both documentation and restoration planning. The conservation concluded with surface cleaning, mortar consolidation, and the successful structural detachment and relocation of the compromised section onto a lightweight support for future museum display. The findings demonstrate that integrating 3D digital and geophysical data provides a quantitative, low-risk roadmap for preserving highly vulnerable archaeological floorings, moving beyond qualitative technical documentation to establish a replicable preservation framework. Full article
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14 pages, 5651 KB  
Article
Flexural Strength and Clinical Classification of Different Layers in 4/5Y-PSZ Zirconia Materials
by Ulrich Lohbauer, Margit Schwarz and Renan Belli
J. Funct. Biomater. 2026, 17(6), 300; https://doi.org/10.3390/jfb17060300 - 16 Jun 2026
Viewed by 381
Abstract
Multilayer 4Y/5Y-PSZ zirconia materials have been developed to combine strength and translucency in monolithic “all-in-one” dental restorations. This study evaluated the flexural strength of different layers (incisal, transition, and dentin) in four commercially available multilayer zirconia systems using three-point bending tests in accordance [...] Read more.
Multilayer 4Y/5Y-PSZ zirconia materials have been developed to combine strength and translucency in monolithic “all-in-one” dental restorations. This study evaluated the flexural strength of different layers (incisal, transition, and dentin) in four commercially available multilayer zirconia systems using three-point bending tests in accordance with ISO 6872. A total of 360 CAD/CAM-fabricated bar-shaped specimens were prepared from the materials CE (Cercon yo ML, DentsplySirona), KA (Katana YML, Kuraray Noritake), PZ (3D ProZir, Aidite), PE (IPS e.max ZirCAD Prime esthetic), and assigned to layer-specific groups based on their position within the discs. After sintering and standardized surface finishing, specimens were tested under three-point bending conditions. Fracture strength was calculated and statistically analysed. Microstructural and fractographic analyses were performed to assess grain structure and to identify fracture origins. The results demonstrated significant differences in flexural strength both among materials and between layers. In general, dentin layers exhibited the highest strength, reaching mean values up to 1143 MPa, while incisal layers showed significantly lower values, with minima around 572 MPa. Only one material (CE) maintained flexural strength above the ISO threshold of 800 MPa across all layers, qualifying for unrestricted (class 5) clinical use. Other materials showed limitations, particularly in the more translucent incisal regions (KA, PE). One material fell below the ISO threshold (PZ). Weibull moduli revealed differences in reliability, with moduli ranging from 4.7 to 16.5. Fractographic evaluation identified typical fracture patterns such as surface grinding defects and internal porosity, but no abnormal fracture origins. The strength gradient corresponds to microstructural differences, particularly grain size and phase composition, influenced by yttria content. Increased translucency in incisal layers is associated with reduced mechanical performance. These findings emphasize that, despite aesthetic advantages, layer-dependent strength variations must be considered when selecting multilayer zirconia for clinical applications, especially in long-span restorations. Full article
(This article belongs to the Special Issue Medical Application of Functional Biomaterials (3rd Edition))
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22 pages, 50000 KB  
Article
Mechanical Anisotropy and Fatigue Behavior of 3D-Printed Dentures: A Comparison with CAD/CAM Milled Bases After Thermomechanical Aging
by Mohamed Ahmed Alkhodary, Ramy Elmoazen, Bandar Awadh Alresheedi, Ali Alenezi, Naji Alharethi and Rawan Alrethia
J. Funct. Biomater. 2026, 17(6), 297; https://doi.org/10.3390/jfb17060297 - 15 Jun 2026
Viewed by 480
Abstract
To investigate the effect of print orientation (0°, 45°, and 90°) and artificial aging on flexural strength and fatigue resistance of 3D-printed denture bases compared to CAD/CAM milled controls, we fabricated 320 maxillary complete dentures, divided into 8 groups based on the fabrication [...] Read more.
To investigate the effect of print orientation (0°, 45°, and 90°) and artificial aging on flexural strength and fatigue resistance of 3D-printed denture bases compared to CAD/CAM milled controls, we fabricated 320 maxillary complete dentures, divided into 8 groups based on the fabrication method: horizontal, oblique, and vertical printing, alongside milled controls. Half of the specimens in each group were pre-conditioned via thermocycling and 240,000 cycles of chewing simulation. All specimens underwent static flexural strength testing and cyclic fatigue testing, followed by SEM fractography. The CAD/CAM milled bases demonstrated the highest mechanical durability, with non-aged specimens peaking at 149.43 ± 5.35 MPa. The horizontally 3D-printed non-aged specimens yielded the highest flexural strength (101.14 ± 4.80 MPa), while vertically printed aged specimens recorded the lowest (70.35 ± 8.18 MPa). Artificial aging degraded flexural strength uniformly across all orientations. Conversely, cyclic loading disproportionately devastated the older people’s vertical group, resulting in a 70% fracture rate. Fractography corroborated these findings, revealing severe interlaminar delamination in vertical builds, contrasting with cohesive, trans-layer fractures in horizontal prints. In conclusion, Horizontal orientation provided improved structural durability; however, CAD/CAM milled dentures remain superior and are recommended for long-term clinical applications. Full article
(This article belongs to the Section Dental Biomaterials)
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29 pages, 35717 KB  
Article
Multi-Objective Optimization Design and Impact Protection Efficacy of Locally Reinforced P-TPMS Forehead Helmet Liner
by Bin Yang, Hao Feng, Xin Li, Peng Zhang, Li Li, Xinyu Wei, Zongchen Su, Qi Jin, Jiawei Zhang and Jianhao Zhang
Materials 2026, 19(12), 2571; https://doi.org/10.3390/ma19122571 - 14 Jun 2026
Viewed by 237
Abstract
The objective of this study is to mitigate the bottom-out failure and improve the energy absorption of conventional helmet liners during high-energy impacts, thereby reducing the risk of head injuries. To this end, a locally reinforced Primitive-type triply periodic minimal surface (P-TPMS) energy-absorbing [...] Read more.
The objective of this study is to mitigate the bottom-out failure and improve the energy absorption of conventional helmet liners during high-energy impacts, thereby reducing the risk of head injuries. To this end, a locally reinforced Primitive-type triply periodic minimal surface (P-TPMS) energy-absorbing liner is proposed for the helmet forehead region, which facilitates progressive energy dissipation through layer-by-layer buckling deformation. A finite element model of a helmet–head coupling was created based on a previously verified high-fidelity head model and subsequently validated against the ECE 22.06 standard drop-test methodology. Three critical design parameters—outer protective layer thickness, triply periodic minimal surface (TPMS) unit cell size, and wall thickness—were optimized employing the Box–Behnken Design (BBD) response surface methodology, resulting in quadratic regression models for the head injury criteria (HIC) and peak linear acceleration (PLA) with good fit (R2 > 0.97). Optimal parameter combinations were established using multi-objective optimization, with protective efficacy carefully assessed from both head dynamic response and biomechanical response perspectives. The ideal P-TPMS liner possesses an outer protective layer thickness of 14.95 mm, a TPMS unit cell size of 12.23 mm, and a wall thickness of 3.93 mm. Compared to the traditional expanded polystyrene (EPS) liner, the optimized P-TPMS liner significantly reduces HIC (by ∼16%) and PLA (by ∼14%) while extending the impact duration. More critically, it transitions both intracranial pressure and brain tissue strain below their respective clinical injury thresholds, substantially lowering the risks of skull fracture and mild traumatic brain injury (mTBI). The P-TPMS construction facilitates continuous energy dissipation during impacts via incremental layer-by-layer buckling deformation, hence extending impact duration and markedly improving helmet protective efficacy. These findings offer theoretical foundations and technical direction for the creation of localized heterogeneous liner designs in advanced high-performance helmets, although the results are limited to frontal flat-anvil impact conditions. Full article
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15 pages, 5718 KB  
Article
Tailoring Interfacial Bonding and Tensile Properties in Cu/Al/Cu Laminated Composites by Adjusting Thickness Ratio
by Wenbo Bai, Mahmoud Ebrahimi, Huisheng Cai, Yuchao Zhao, Nannan Zhang and Qudong Wang
Metals 2026, 16(6), 656; https://doi.org/10.3390/met16060656 - 14 Jun 2026
Viewed by 161
Abstract
The design of the overall thickness and thickness ratio in multilayered composites is vital because it affects interfacial microstructures and mechanical properties. These elements are significant in the application of multilayered composites in diverse scenarios. This study systematically investigated the interfacial microstructure, mechanical [...] Read more.
The design of the overall thickness and thickness ratio in multilayered composites is vital because it affects interfacial microstructures and mechanical properties. These elements are significant in the application of multilayered composites in diverse scenarios. This study systematically investigated the interfacial microstructure, mechanical properties, and fracture mechanisms of Cu/Al/Cu trilayered composites with varying overall thicknesses and copper thickness ratios. The microstructure results showed that the distribution and thickness of intermetallic compounds (IMCs) at the Cu/Al interface changed significantly with different thickness designs. As the Cu thickness ratio increased from 20% to 35%, the intermetallic layer transitioned from a continuous structure to a fragmented one in both the 1 mm and 2 mm composites. Additionally, the bonding mechanism evolved from primarily metallurgical bonding to a combination of metallurgical and mechanical bonding. In the 4 mm composite with a 35% Cu thickness ratio, the interfacial intermetallic layer comprised three sublayers identified as Al4Cu9, AlCu, and Al2Cu. Tensile results indicated that increasing the Cu thickness ratio markedly enhanced strength and ductility: the 1 mm composite showed increases of 22.3% in ultimate tensile strength and 70.9% in elongation, while the 2 mm composite exhibited increases of 32.4% and 38.7%, respectively. In contrast, increasing the overall thickness had only a limited effect. Fractography revealed ductile fracture features in both the Al and Cu layers, characterized by more compact interfaces, deeper dimples, and more pronounced tear ridges at higher Cu thickness ratios. These findings demonstrate that optimizing the Cu thickness ratio is an effective strategy for enhancing interfacial bonding strength and overall mechanical performance in Cu/Al/Cu composites. Full article
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18 pages, 2518 KB  
Article
Design and Field Assessment of a Pressurized Driving-Down Air Multilevel Sampler for Depth-Discrete Groundwater Monitoring in NAPL Impacted Wells
by Giuseppe Passarella, Rita Masciale, Antonio Di Fazio and Costantino Masciopinto
Sensors 2026, 26(12), 3788; https://doi.org/10.3390/s26123788 - 14 Jun 2026
Viewed by 314
Abstract
This study presents the development and field testing of a Pressurized Driving-Down Air Multilevel Sampler (PDA-MLS), an integrated groundwater sampling device designed for depth-discrete sampling in boreholes affected by floating non-aqueous phase liquids (NAPLs). Conventional sampling methods—such as low-flow pumps, bailers, and packer-isolated [...] Read more.
This study presents the development and field testing of a Pressurized Driving-Down Air Multilevel Sampler (PDA-MLS), an integrated groundwater sampling device designed for depth-discrete sampling in boreholes affected by floating non-aqueous phase liquids (NAPLs). Conventional sampling methods—such as low-flow pumps, bailers, and packer-isolated systems—often fail under these conditions due to limited accessibility, cross-contamination, or disturbance of the water column. The proposed system addresses these limitations through a controlled pressurized-gas actuation mechanism that transfers groundwater from multiple PTFE-membrane chambers installed at discrete depths. This configuration enables low-disturbance sampling below floating contaminant layers. The use of chemically inert materials (stainless steel and PTFE) minimizes sampling artifacts and ensures compatibility with volatile organic compound (VOC) analyses. A simplified hydraulic conceptual framework describing inflow, outflow, and pressure-driven displacement was developed to support purge-duration estimation and operational parameter definition. The device was tested in a 90 m deep fractured limestone aquifer contaminated by tetrachloroethylene (PCE), where floating hydrocarbons limited the applicability of conventional sampling techniques. Field testing showed stable discharge conditions (~145–160 mL/min), repeatable sampling cycles, and successful collection of depth-discrete groundwater samples under the investigated site conditions. No evidence of sampler-related hydrocarbon entrainment was observed in the collected samples within the analytical detection limits of the adopted laboratory methods. To the authors’ knowledge, the PDA-MLS represents one of the few groundwater sampling systems specifically designed to combine low-disturbance multilevel sampling with operation in wells affected by floating NAPL. These features make it a promising tool for environmental monitoring, high-resolution characterization of fractured aquifers, and long-term assessment of contaminated sites. Full article
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Article
Mechanical Properties of 3D-Printed Nylon-Based Composites Reinforced with Continuous Carbon Fiber: Effect of Reinforcement Layer Distribution
by Boyuan Ding, Jingjing Liu, Mouaz Al Kouzbary, Hanie Nadia Shasmin, Jingang Liu, Shengyan Ge and Noor Azuan Abu Osman
Polymers 2026, 18(12), 1491; https://doi.org/10.3390/polym18121491 - 13 Jun 2026
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Abstract
The application of continuous carbon fiber (CCF) can reinforce the mechanical properties of 3D-printed parts, but the effect of reinforcement layer distribution on composite performance remains unclear. This study investigates the effect of concentrated and separated distributions of CCF layers with different numbers [...] Read more.
The application of continuous carbon fiber (CCF) can reinforce the mechanical properties of 3D-printed parts, but the effect of reinforcement layer distribution on composite performance remains unclear. This study investigates the effect of concentrated and separated distributions of CCF layers with different numbers of reinforcement layers. Tensile and flexural tests are conducted in accordance with ASTM D5083 and ASTM D790, respectively. Under the conditions of a solid-filled matrix (Onyx) and 0° CCF deposition, both concentrated and separated CCF layers improve several mechanical properties. Compared with pure Onyx, one-layer CCF increases the tensile modulus by about six times and more than doubles the tensile strength. Increasing the CCF volume leads to further increases in these properties. With concentrated three-layer CCF, the tensile modulus and tensile strength reach 7.153 ± 0.090 GPa and 109.045 ± 5.124 MPa, respectively. For flexural properties, separated two- and three-layer CCFs significantly improve the tangent modulus of elasticity from 0.467 ± 0.106 GPa for pure Onyx to 2.246 ± 0.333 GPa and 3.394 ± 0.081 GPa, respectively. This study also compares the tensile and flexural strength-to-weight ratio of all specimen groups and analyzes the failure mechanisms based on macroscopic fracture appearance. The results can provide guidance for selecting appropriate CCF layer distribution strategies to reinforce composites in different applications. Full article
(This article belongs to the Section Polymer Processing and Engineering)
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