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Search Results (1,707)

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Keywords = freeze–thaw cycles

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28 pages, 30309 KB  
Article
Mechanical Properties and Microstructural Evolution of Dispersive Soils Under Freeze–Thaw Cycles
by Xingchao Liu, Xionglong Zhang, Jiangjiang Shen, Yangming Zhang, Renhui Guan, Qixun Lv, Enliang Wang, Liqiang Wang, Haiqiang Jiang and Hongwei Han
Water 2026, 18(17), 2147; https://doi.org/10.3390/w18172147 - 31 Aug 2026
Abstract
Dispersive soils are widely distributed in the seasonally frozen regions of northeastern China, where hydrothermal dynamics driven by seasonal freeze–thaw (FT) cycles dominate the hydrological evolution and mechanical deterioration of soil masses, posing a serious threat to the long-term stability of hydraulic engineering [...] Read more.
Dispersive soils are widely distributed in the seasonally frozen regions of northeastern China, where hydrothermal dynamics driven by seasonal freeze–thaw (FT) cycles dominate the hydrological evolution and mechanical deterioration of soil masses, posing a serious threat to the long-term stability of hydraulic engineering in cold regions. However, the hydro–thermo–mechanical (HTM) coupled degradation mechanisms of dispersive clay from the South Nenjiang Main Canal remain poorly understood, particularly the linkage between FT-induced microstructural evolution and macroscopic mechanical behavior. In this study, low-plasticity dispersive clay specimens were subjected to 0–12 FT cycles. Unconsolidated undrained (UU) triaxial tests were conducted to evaluate mechanical behavior, while scanning electron microscopy (SEM) combined with the Pore and Crack Analysis System (PCAS) was used to quantify microstructural evolution. Results indicated that increasing FT cycles transformed the stress–strain response from mild strain-softening to strain-hardening, with the failure mode evolving toward bulging-type ductile failure. Cohesion exhibited a pronounced exponential decay, with the most significant degradation occurring within the first three FT cycles and stabilizing after approximately six FT cycles, whereas the internal friction angle showed only minor variation. At the microscale, porosity and total pore area increased continuously through micropore coalescence and macropore development, with a slight decrease in fractal dimension indicating reduced pore boundary complexity and smoothed pore interfaces due to frost heave-induced pore merging. The FT-induced hydrothermal disturbance promoted pore-water phase transition and redistribution, resulting in progressive pore enlargement and loss of structural integrity. Because the specimens were tested in sealed, closed-system conditions with a nearly constant total water content, this degradation chain is attributable specifically to in situ ice–water phase transitions and internal pore-water redistribution, i.e., water-phase-change-driven processes, rather than to external water supply. It is demonstrated that interparticle bond breakage and pore expansion–coalescence driven by ice–water phase transitions dominate strength degradation, promoting a transition from structure-dominated to friction-dominated strength behavior. A normalized cohesion reduction factor and a cohesion degradation index are further proposed to quantify the progressive loss of structural integrity and to provide a design-oriented tool for cold-region geotechnical practice. These findings provide a basis for stability assessment and hazard mitigation of dispersive soils in cold-region engineering. Full article
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24 pages, 2066 KB  
Article
Durability Evolution of Low Liquid Limit Clay-Based CLSM Incorporating Industrial Wastes Under Freeze–Thaw, Wet–Dry, and Drying Actions
by Aijun Chen, Yifan Zhou and Junhua Chen
J. Compos. Sci. 2026, 10(9), 463; https://doi.org/10.3390/jcs10090463 (registering DOI) - 31 Aug 2026
Abstract
A sustainable controlled low-strength material (CLSM) was developed using ground granulated blast-furnace slag, steel slag, and flue gas desulfurization gypsum in combination with cement to synergistically utilize engineering excavated soil and industrial solid wastes for stabilizing low liquid limit clay. However, the long-term [...] Read more.
A sustainable controlled low-strength material (CLSM) was developed using ground granulated blast-furnace slag, steel slag, and flue gas desulfurization gypsum in combination with cement to synergistically utilize engineering excavated soil and industrial solid wastes for stabilizing low liquid limit clay. However, the long-term durability evolution of this material under harsh and coupled environmental conditions—particularly freeze–thaw cycles, wet–dry cycles, and prolonged drying—has not been systematically investigated. In this study, systematic freeze–thaw cycling (up to 11 cycles), wet–dry cycling (up to 11 cycles), and natural drying (until mass stabilization) tests were conducted on specimens with binder contents ranging from 8% to 16%. The evolution of mechanical performance was evaluated via unconfined compressive strength (UCS) tests, while microstructural changes were characterized using scanning electron microscopy (SEM) and X-ray diffraction (XRD). The results revealed a distinctive “S-shaped” fluctuation in UCS under freeze–thaw cycles. High-binder (16%) specimens maintained strengths of 1783–2395 kPa with intact surfaces and no visible cracking—significantly outperforming low-binder specimens. Under wet–dry cycles, strength initially increased after the first cycle and then declined progressively, with the lowest strength loss observed at 10% binder content. During drying, both water loss rate and drying shrinkage strain decreased with increasing binder content: from 8% to 16% binder, the water loss rate dropped from 34.16% to 29.03%. Microstructural analysis revealed that higher binder content promoted the formation of a dense, interwoven network of C–S–H gel and ettringite, which effectively filled intergranular pores and encapsulated soil particles, thereby enhancing macroscopic durability. This study provides a sustainable material solution for utilizing industrial solid wastes in the stabilization of low liquid limit clay for CLSM applications under severe environmental conditions, supporting the broader adoption of waste-to-resource strategies in construction engineering. Full article
(This article belongs to the Section Composites Applications)
23 pages, 1538 KB  
Article
Analysis of Uniaxial Fatigue Mechanical Properties and Constitutive Modeling for Freeze–Thaw Cycled Red Sandstone with Double Fissures
by Jianxi Ren, Zhengtao Jiang, Mufan Tan, Mengchen Yun, Kun Zhang, Kechen Zhang and Haojun Wang
Appl. Sci. 2026, 16(17), 8680; https://doi.org/10.3390/app16178680 (registering DOI) - 31 Aug 2026
Abstract
This study addresses the challenge of the mechanical behavior of fractured rock masses in cold regions under freeze–thaw-fatigue coupling. Uniaxial step-incremental cyclic loading tests were conducted on double-cracked red sandstone subjected to different numbers of freeze–thaw cycles to reveal the damage evolution laws. [...] Read more.
This study addresses the challenge of the mechanical behavior of fractured rock masses in cold regions under freeze–thaw-fatigue coupling. Uniaxial step-incremental cyclic loading tests were conducted on double-cracked red sandstone subjected to different numbers of freeze–thaw cycles to reveal the damage evolution laws. Based on the variable-order fractional derivative theory, the traditional Nishihara model was improved by replacing the Abel dashpot in the viscoplastic component with a variable-order fractional dashpot, thereby establishing a fatigue deformation constitutive model that accounts for freeze–thaw damage. The novelty of the model lies in coupling the variable-order fractional viscoplastic element with stepwise cyclic loading equivalence, fatigue-threshold-controlled deformation, and freeze–thaw damage degradation, rather than merely replacing the dashpot in the classical Nishihara framework. The experimental results indicate that freeze–thaw cycles accelerate macroscopic damage of the rock mass. As the number of freeze–thaw cycles increases, the crack initiation stress, dilatancy stress, and peak stress decrease in a stepwise manner. The rock specimens exhibit significant softening characteristics, accompanied by intensified dilatancy, propagation of secondary cracks at the tips of pre-existing flaws, and a transition of the failure mode towards shear failure. By analyzing the mean stress versus axial deformation curves of the last two stages of cyclic loading, the fatigue threshold stress ratio of freeze–thaw damaged double-cracked sandstone was determined, confirming that freeze–thaw damage reduces the fatigue strength of the rock mass. Full article
24 pages, 4747 KB  
Article
Mechanical, Durability, Carbon Footprint, and Economic Assessment of Sand–Gravel–Gneiss Aggregate Mixtures for Sustainable Road Construction
by Agnieszka Nowaczek, Joanna Kulczycka, Marek Bęben, Dariusz Kasperek, Zygmunt Kowalski, Agnieszka Makara and Natalia Generowicz-Caba
Materials 2026, 19(17), 3679; https://doi.org/10.3390/ma19173679 - 29 Aug 2026
Abstract
This study evaluates the influence of different crushed gneiss contents on the mechanical, durability, environmental, and economic performance of sand–gravel/gneiss mixtures for sustainable road construction. Natural sand–gravel aggregate was blended with crushed gneiss at three proportions (10%, 30%, and 50% by mass). The [...] Read more.
This study evaluates the influence of different crushed gneiss contents on the mechanical, durability, environmental, and economic performance of sand–gravel/gneiss mixtures for sustainable road construction. Natural sand–gravel aggregate was blended with crushed gneiss at three proportions (10%, 30%, and 50% by mass). The experimental program included grain size analysis, compaction characteristics, California Bearing Ratio (CBR), deformation modulus, and freeze–thaw durability tests. Environmental performance was assessed using a cradle-to-site carbon footprint approach based on Life Cycle Assessment principles according to ISO 14040, ISO 14044, and ISO 14067, with the analysis focused on Global Warming Potential (GWP100), combined with a Total Cost of Ownership analysis. Increasing gneiss content improved mechanical performance, with CBR increasing from 45% to 95% and deformation modulus from 110 to 185 MPa. The 70/30 sand–gravel/gneiss mixture provided the most balanced performance among the investigated compositions, combining high bearing capacity, satisfactory freeze–thaw resistance, and favorable environmental and economic characteristics. Its carbon footprint was 3.90 kg CO2 eq./t, with diesel consumption during aggregate handling identified as the dominant emission source (69%), followed by gneiss transportation (20%) and electricity consumption (12%). Higher gneiss contents and longer transport distances increased environmental impacts and production costs. The results indicate that selecting an appropriate aggregate composition and reducing transport-related emissions can support lower-carbon construction materials while maintaining required engineering performance. Full article
(This article belongs to the Section Construction and Building Materials)
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10 pages, 7562 KB  
Article
Influence of Oil Shale Residue on the Frost Resistance of Fly-Ash-Based Autoclaved Aerated Concrete
by Lei Zhao, Yao Xiao, Jiayu Luo, Wenqi E, Xinze Gao and Cong Zeng
Materials 2026, 19(17), 3675; https://doi.org/10.3390/ma19173675 - 29 Aug 2026
Viewed by 24
Abstract
To promote the high-value utilization of industrial solid waste and enhance the durability of construction materials in cold regions, this study investigates an autoclaved aerated concrete (AAC) system prepared primarily with fly ash and oil shale residue, with a particular focus on its [...] Read more.
To promote the high-value utilization of industrial solid waste and enhance the durability of construction materials in cold regions, this study investigates an autoclaved aerated concrete (AAC) system prepared primarily with fly ash and oil shale residue, with a particular focus on its frost resistance. The physical and chemical properties of the raw materials were characterized using X-ray fluorescence (XRF) and X-ray diffraction (XRD) to optimize the pore structure and mineral composition. A systematic evaluation of 15 continuous freeze–thaw cycles was conducted, comprehensively analyzing the compressive strength retention, mass loss rate, and thermal conductivity. The experimental results indicate that a 50% replacement of fly ash with oil shale residue, combined with an optimized water-to-binder ratio (0.66), significantly improves the pore uniformity and skeleton stability of the AAC. The optimized mixture (YYY50W) achieved a compressive strength of 5.2 MPa and a low thermal conductivity of 0.1654 W/(m·K). After 15 freeze–thaw cycles, the mass loss was minimal (<3 g), and the compressive strength retention rate ($R$) reached 90.0%, demonstrating superior frost resistance. This study elucidates the microstructural mechanism by which oil shale residue promotes the formation of low-crystallinity tobermorite and C-S-H gels, providing potential experimental evidence for the utilization of industrial by-products in building materials for cold environments. Full article
(This article belongs to the Section Construction and Building Materials)
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37 pages, 56594 KB  
Review
A Review of the Mechanism of Degradation of the Structure and Properties of Concrete Under the Simultaneous Effect of Freezing–Thawing Cycles and Corrosion
by Jingbiao Liu, Mingyu Li, Gang Wang, Keke Liu, Aiguo Dang, Shaohua Cao and Ting Zhang
Buildings 2026, 16(17), 3447; https://doi.org/10.3390/buildings16173447 - 28 Aug 2026
Viewed by 76
Abstract
The durability deterioration of concrete under the coupled action of freeze–thaw cycles and corrosive media is a critical technical challenge for engineering structures in cold regions and salt corrosive environments. This paper systematically reviews the research progress on the mechanical properties of concrete [...] Read more.
The durability deterioration of concrete under the coupled action of freeze–thaw cycles and corrosive media is a critical technical challenge for engineering structures in cold regions and salt corrosive environments. This paper systematically reviews the research progress on the mechanical properties of concrete subjected to coupled freeze–thaw and corrosion effects. Starting from the mechanisms of freeze–thaw damage and corrosion damage, it analyzes the material degradation laws under individual factors and the synergistic failure mechanism of the coupled freeze–thaw–corrosion condition. The coupling effect is revealed: freeze–thaw-induced microcracks accelerate the penetration of corrosive media, while the expansion of corrosion products in turn aggravates freeze–thaw damage. Building on this, from the perspective of factors influencing concrete failure, this paper systematically summarizes the key factors governing concrete damage under single-factor and coupled-factor conditions as well as their nonlinear response characteristics. The review indicates that the damage degree under the coupled action is far greater than the simple superposition of damage caused by individual factors and presents complex patterns, including the concentration threshold effect, the time-sequence effect, and sensitivity to a low water–cement ratio. Existing reviews predominantly focus on qualitative descriptions of single-factor deterioration mechanisms, while systematic comparative analyses of threshold behaviors under multi-factor coupling and quantitative consolidation of mechanical degradation metrics remain limited. Furthermore, targeted durability design guidance tailored to cold saline environments is rarely summarized in the prior literature, which motivates the present comprehensive review. Although existing studies are relatively well-established for single damage mechanisms, further efforts are still needed to deepen the understanding of multi-factor interaction thresholds and dynamic evolution processes. The findings of this review can provide theoretical support and engineering reference for the durability design and service life prediction of concrete structures in cold regions and salt corrosive environments. The summarized threshold laws and quantitative mechanical degradation data can provide targeted parameter guidance for the durability design of hydraulic structures, bridge substructures, and port engineering in northwest saline soil, northern severe cold, and eastern coastal salt fog areas. Full article
(This article belongs to the Special Issue Research and Development of Cement-Based Materials)
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19 pages, 3214 KB  
Article
Influence of Water-to-Powder Ratio on the Frost Resistance of Tuff Powder-Modified Self-Compacting Concrete
by Cun Zhang, Xiaoyun Qin, Jingbin Zhang, Haozhe Sui, Yichen Zhang, Zhuoma Pingcuo, Gengchen Yan and Xuehui An
Buildings 2026, 16(17), 3442; https://doi.org/10.3390/buildings16173442 - 28 Aug 2026
Viewed by 151
Abstract
Self-compacting concrete (SCC) shows considerable potential for infrastructure applications on the Qinghai–Tibet Plateau, which is characterized by a hypoxic environment. However, the quantitative effects of the volumetric water-to-powder ratio (VW/VP) on the freeze–thaw durability of SCC remain poorly understood, [...] Read more.
Self-compacting concrete (SCC) shows considerable potential for infrastructure applications on the Qinghai–Tibet Plateau, which is characterized by a hypoxic environment. However, the quantitative effects of the volumetric water-to-powder ratio (VW/VP) on the freeze–thaw durability of SCC remain poorly understood, particularly when tuff powder is incorporated as a filler. This research explores the effects of VW/VP on the frost resistance of SCC incorporating tuff powder. Three SCC mixtures with VW/VP values of 1.0, 1.1, and 1.2 were prepared to systematically evaluate their mechanical performance and freeze–thaw durability. Scanning electron microscopy (SEM) and mercury intrusion porosimetry (MIP) were employed to characterize the microstructure of the corresponding hardened pastes. The findings indicate that both compressive and splitting tensile strengths decrease markedly as VW/VP rises. Under the same number of freeze–thaw cycles (FTCs), higher VW/VP gives rise to an increased mass loss rate and accelerated degradation of the relative dynamic elastic modulus (RDEM). Over the course of 250 FTCs, the RDEM decreased from 75.5% to 67.3%, accompanied by an increase in mass loss from 1.34% to 5.20%. Microstructural analyses reveal that the proportions of harmful pores (100–200 nm) and multi-harmful pores (>200 nm) increase as VW/VP rises, indicating that a reduced VW/VP enhances pore structure densification and the frost resistance of SCC. The forecasted trajectories of mass loss and RDEM derived from our established damage model are in close accordance with the measured laboratory data, confirming that lower VW/VP effectively prolongs the operational life of SCC under harsh freeze–thaw environments. Furthermore, an improved comprehensive performance evaluation considering mechanical performance, freeze–thaw resistance, cost, and environmental impact was proposed, demonstrating that SCC with lower VW/VP exhibits superior overall performance. Full article
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19 pages, 10468 KB  
Article
Optimization of Recycled Fine Aggregate Content for All-Solid-Waste-Based Flowable Solidified Soil: Performance and Microstructure
by Anhui Wang, Liwei Ju, Jiaojiao Ni, Lili Li and Enze Zhen
Materials 2026, 19(17), 3638; https://doi.org/10.3390/ma19173638 - 27 Aug 2026
Viewed by 170
Abstract
To promote the high-value utilization of construction and industrial solid wastes, this study prepared an all-solid-waste-based flowable solidified soil (FSS) using soft clay and recycled fine aggregate (RFA) as the main constituents. The binder system comprised ground-granulated blast-furnace slag (GGBS), carbide slag (CS), [...] Read more.
To promote the high-value utilization of construction and industrial solid wastes, this study prepared an all-solid-waste-based flowable solidified soil (FSS) using soft clay and recycled fine aggregate (RFA) as the main constituents. The binder system comprised ground-granulated blast-furnace slag (GGBS), carbide slag (CS), and desulfurization gypsum (DG), while fly ash (FA) was incorporated to improve workability. The primary objective was to identify an appropriate RFA content for this FSS system through a combined evaluation of workability, mechanical performance, durability, and microstructural characteristics. The results showed that increasing the RFA content increased flowability and shortened the setting time. Unconfined compressive strength (UCS) and ultrasonic pulse velocity (UPV) both increased initially and then decreased as the RFA content increased, and relatively favorable mechanical performance was observed at RFA contents of 40–60%. In the durability tests, the mixture containing 40% RFA exhibited the lowest mass loss and UCS loss after both wetting–drying and freeze–thaw cycles within the investigated range. X-ray diffraction (XRD) and scanning electron microscopy (SEM) analyses suggested that a moderate RFA content was associated with the development of C-(A)-S-H-gel-related phases and ettringite (AFt), together with a denser and more continuous microstructure. The improved strength and durability at moderate RFA contents were therefore interpreted as the combined results of hydration-product development and the physical skeleton effect provided by RFA. By contrast, the performance decline at excessive RFA contents appeared to be related to a less favorable internal structure, as indicated by SEM observations. Overall, when workability, mechanical performance, durability, and microstructural observations are considered together, 40% RFA is recommended as the most suitable content for the material system and test conditions investigated in this study. These findings demonstrate the potential of RFA to regulate the performance of all-solid-waste-based FSS and to improve the resource efficiency of multiple solid-waste streams. Full article
(This article belongs to the Section Construction and Building Materials)
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25 pages, 6556 KB  
Article
Coupling Water-Ice Phase Transition DEM to Characterize Freeze-Thaw ITZ Damage in Cold Recycled Mixtures
by Jian Gao, Pengfei Xue, Huwei Li, Le Han, Zhizhou Wang, Yutong Wang, Zhibo Wang, Jie Sun, Yusheng Li, Jiankun Xue and Yaoyao Meng
Processes 2026, 14(17), 2735; https://doi.org/10.3390/pr14172735 - 26 Aug 2026
Viewed by 149
Abstract
Cold recycled mixtures with bitumen emulsion (CRME) serving in seasonally frozen regions are susceptible to mechanical deterioration under repeated freeze-thaw (F-T) cycles, which is primarily manifested as interfacial damage and crack propagation. However, the micro-mechanical processes associated with the transmission and dissipation of [...] Read more.
Cold recycled mixtures with bitumen emulsion (CRME) serving in seasonally frozen regions are susceptible to mechanical deterioration under repeated freeze-thaw (F-T) cycles, which is primarily manifested as interfacial damage and crack propagation. However, the micro-mechanical processes associated with the transmission and dissipation of frost-heaving stresses induced by water-ice phase transition within the interfacial transition zone (ITZ) between reclaimed asphalt pavement (RAP) and asphalt mortar remain to be further characterized. In this study, a numerical simulation approach coupling frost heave effects with the phase transition of water-ice particles was developed based on X-ray computed tomography (CT) and the discrete element method (DEM), and the micro-mechanical parameters of the RAP-asphalt mortar ITZ were determined through laboratory experiments. Combined with acoustic emission (AE) monitoring, the damage evolution characteristics of cold recycled mixtures and the associated interfacial damage mechanisms under freeze-thaw action were systematically investigated. The results indicate that the optimal micro-parameters of the RAP-asphalt mortar ITZ can be taken as approximately 85% of those of virgin asphalt mortar. After 20 freeze-thaw cycles, the number of shear cracks and tensile cracks in ITZ on RAP surface reached 493 and 92, respectively, which were much higher than 11 and five on the surface of new aggregate. ITZ was the main control weak area of freeze-thaw damage. Compared with the unfrozen specimens, the minimum effective contact number of mortar decreased by 1.63%, 4.52% and 8.52% respectively after 5, 10 and 20 freeze-thaw cycles, and the total effective contact number decreased from 75,842 to 69,383. Freeze-thaw cycles significantly reduce the strain energy storage capacity of CRME: the maximum energy storage capacity of the adhesive spring decreased from 2.15 J in the non-freeze-thaw state to 1.28 J in 10 cycles (a decrease of 40.47%) and 1.16 J in 20 cycles (a decrease of 46.05%), and the damage mode changed from brittle fracture to interface-controlled energy dissipation. The proposed water-ice phase transition-based DEM framework provides a reliable numerical tool for investigating freeze-thaw damage mechanisms and supporting durability-oriented design of cold recycled pavement materials. Full article
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21 pages, 11791 KB  
Article
From Pore Expansion to Throat Extension: Effects of Freezing Temperature on Microstructural Evolution and Dynamic Strength Decay in Sandstone
by Junce Xu, Hai Pu, Zhuangli Zheng and Kangsheng Xue
Processes 2026, 14(17), 2729; https://doi.org/10.3390/pr14172729 - 26 Aug 2026
Viewed by 197
Abstract
Repeated freeze–thaw (F–T) action, together with dynamic disturbances, can progressively weaken rock masses in cold regions. However, how freezing temperature affects the relationship between microstructural evolution and dynamic strength decay remains insufficiently quantified. This study investigated yellow sandstone subjected to F–T cycles at [...] Read more.
Repeated freeze–thaw (F–T) action, together with dynamic disturbances, can progressively weaken rock masses in cold regions. However, how freezing temperature affects the relationship between microstructural evolution and dynamic strength decay remains insufficiently quantified. This study investigated yellow sandstone subjected to F–T cycles at freezing temperatures of 0, −3, −5, and −20 °C. CT-based 3D reconstruction and Split Hopkinson pressure bar (SHPB) tests were combined with grey relational analysis (GRA) to characterize pore-structure evolution, dynamic strength decay, and their relationship. The results indicated that lower freezing temperatures promoted increases in pore connectivity and structural complexity. After 60 F–T cycles at −20 °C, connected porosity increased from 11.15% to 18.67%, while the ratio of connected porosity to total porosity increased from 51.1% to 85.7%. At an impact pressure of 0.3 MPa, the dynamic strength after 60 cycles decreased by 9.51%, 20.9%, 38.1%, and 61.5% at 0, −3, −5, and −20 °C, respectively. Among the examined microstructural parameters, average throat length had the highest overall grey relational grade (0.821), suggesting that throat development is closely associated with dynamic strength decay. Lower freezing temperatures enhanced pore-ice expansion and unfrozen-water migration, promoting pore enlargement, throat extension, and crack connection. These results quantitatively link pore-network evolution to dynamic strength decay under different freezing temperatures, providing a microstructural basis for assessing the dynamic deterioration of sandstone in cold regions. Full article
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24 pages, 6145 KB  
Article
Fatigue Performance and Pore Characteristics of SBS/Micro Carbon Fiber Composite-Modified Asphalt Concrete for Ultra-Thin Overlays
by Xiaodong Yang, Mingxin Liu, Xiaojin Lu, Jingyu Xiao, Jifa Liu and Quanman Zhao
Polymers 2026, 18(17), 2062; https://doi.org/10.3390/polym18172062 - 25 Aug 2026
Viewed by 255
Abstract
Durability deterioration and interlayer bonding failure of ultra-thin overlays remain critical challenges under coupled environmental and mechanical actions. Although environmental damage to asphalt mixtures has been widely investigated, the relationship between pore-structure evolution and interlayer fatigue deterioration in polymer-composite-modified ultra-thin overlays incorporating styrene–butadiene–styrene [...] Read more.
Durability deterioration and interlayer bonding failure of ultra-thin overlays remain critical challenges under coupled environmental and mechanical actions. Although environmental damage to asphalt mixtures has been widely investigated, the relationship between pore-structure evolution and interlayer fatigue deterioration in polymer-composite-modified ultra-thin overlays incorporating styrene–butadiene–styrene (SBS) and micro carbon fiber (MCF) remains insufficiently understood. This study therefore extends existing research by clarifying this relationship under freeze–thaw cycling and water immersion. Three-point bending and direct shear fatigue tests were conducted to evaluate bending and interlayer shear fatigue performance, respectively, while nanoindentation and X-ray computed tomography (CT) were used to characterize micromechanical properties and three-dimensional pore-structure evolution. The results showed that five freeze–thaw cycles reduced the bending fatigue life by 75.3% and the interlayer shear fatigue life by 49.6%, while six days of water immersion reduced the interlayer shear fatigue life by 55.1%. Freeze–thaw cycling promoted open-pore and pore-throat development and increased total porosity by 23.9%, contributing to aggregate displacement and redistribution of the internal skeleton. In contrast, immersion increased the proportion of small and closed pores, while isolated pores concentrated near the interlayer weakened interlayer shear resistance. Although immersion caused greater reductions in hardness and modulus, freeze–thaw-induced pore development was associated with greater deterioration in bending fatigue performance. Furthermore, an adaptive-network-based fuzzy inference system (ANFIS) was developed to predict pore tortuosity from equivalent diameter, shape factor, and porosity, with testing errors ranging from 0.102 to 0.129 for untreated, freeze–thaw, and immersed specimens. An exponential relationship was further identified between tortuosity and the pore comprehensive effect index (PCEI), providing a quantitative approach for characterizing pore connectivity and evaluating environmental deterioration in polymer-composite-modified asphalt concrete. Full article
(This article belongs to the Special Issue Sustainable Polymer Materials for Pavement Applications)
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25 pages, 11528 KB  
Article
Uniaxial Damage Mechanisms in Roller-Compacted Concrete Subjected to Freeze–Thaw Cycles
by Kaide Liu, Xinping Wang, Yu Xia, Wenping Yue, Kekuo Yuan, Chaowei Sun, Dingbo Wang and Songxin Zhao
Buildings 2026, 16(17), 3360; https://doi.org/10.3390/buildings16173360 - 24 Aug 2026
Viewed by 254
Abstract
Water-retaining roller-compacted concrete (RCC) dams suffer severe deterioration under coupled moisture ingress and freeze–thaw (F-T) cycles. To elucidate the damage mechanisms, this study employed industrial X-ray computed tomography (CT) synchronized with uniaxial compression and acoustic emission (AE) monitoring. The cross-scale damage evolution of [...] Read more.
Water-retaining roller-compacted concrete (RCC) dams suffer severe deterioration under coupled moisture ingress and freeze–thaw (F-T) cycles. To elucidate the damage mechanisms, this study employed industrial X-ray computed tomography (CT) synchronized with uniaxial compression and acoustic emission (AE) monitoring. The cross-scale damage evolution of RCC was investigated under dry, water-saturated, 25, and 50 F-T cycle conditions. The results indicate the following: (1) Macroscopically, F-T damage causes linear peak stress attenuation, shifting the failure mode from brittle axial splitting to ductile oblique shear. (2) Mesoscopically, frost-heaving stress expands native mesopores (500–2500 μm), increasing their volume fraction from 8.45% to 14.86% and remodeling isolated voids into a 3D interconnected defect network. (3) Microscopically, GMM-based AE clustering reveals a fracture transition. Driven by moisture lubrication and defect propagation, global shear cracks surpass the 50% threshold at 25 cycles (53.5%), reaching 68.6% at 50 cycles. (4) For cross-scale mapping, calibrating the AE b-value via Aki’s method decouples pore-water signal attenuation. Its pre-peak characteristic (an initial decrease followed by a rebound) accurately maps microcracks unstably coalescing along interconnected pores to form macroscopic shear planes. This cross-scale mechanism provides a scientific paradigm for condition monitoring of massive concrete in cold regions. Full article
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21 pages, 6799 KB  
Article
Effect of Superplasticizer Dosage on Mechanical and Durability Properties of Low-Volume Steel Microfiber Reinforced Self-Compacting Concrete
by Jinchi Wu, Conteh Santigie Morlor, Donghua Yu, Linbin Wang, Gengying Li and Jingjing Huang
Materials 2026, 19(16), 3557; https://doi.org/10.3390/ma19163557 - 21 Aug 2026
Viewed by 169
Abstract
This study investigates the effects of low-volume steel microfibers (0–0.4 vol.%) and superplasticizer (SP) dosage (0.8 wt.% and 1.5 wt.%) on the mechanical and durability properties of self-compacting concrete (SCC) for railing structures, with a constant water-binder ratio of 0.28. Fresh (slump flow), [...] Read more.
This study investigates the effects of low-volume steel microfibers (0–0.4 vol.%) and superplasticizer (SP) dosage (0.8 wt.% and 1.5 wt.%) on the mechanical and durability properties of self-compacting concrete (SCC) for railing structures, with a constant water-binder ratio of 0.28. Fresh (slump flow), mechanical (compressive strength up to 90 days, 28-day flexural strength), durability (drying shrinkage, freeze–thaw resistance after 200 cycles), and microstructural (mercury intrusion porosimetry) properties were evaluated. SP enhances flowability while steel fibers reduce it. All mixtures except that with 0.8% SP and 0.4% fibers meet the workability requirements of Chinese standard JGJ/T 283-2012 for SCC. Compressive and flexural strengths generally increase with fiber content but decrease when the SP dosage rises from 0.8% to 1.5%. Steel fibers effectively reduce drying shrinkage and improve freeze–thaw resistance, as indicated by higher relative dynamic elastic moduli and lower mass loss after 200 cycles. Microstructural analysis reveals that the higher SP dosage (1.5 wt.%) significantly increases porosity, which explains the observed higher shrinkage and lower strength. Considering mechanical properties, durability, and castability, the SCC mixture with 0.3 vol.% steel fibers and 0.8 wt.% SP is recommended for railing structure applications. Full article
(This article belongs to the Section Construction and Building Materials)
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23 pages, 47456 KB  
Article
Durability Properties of PVA-Strengthened Waste-Based Foam Lightweight Soil Under Freeze–Thaw Cycles and Solution Immersion Conditions
by Xiaoyan Tian, Kun Dong, Yiheng Feng and Zhuo Liu
Buildings 2026, 16(16), 3307; https://doi.org/10.3390/buildings16163307 - 20 Aug 2026
Viewed by 257
Abstract
Traditional cement-based foamed lightweight soils suffer from high construction costs, poor durability, and low solid waste utilization efficiency, which severely restrict their engineering application. A novel polyvinyl alcohol (PVA)-reinforced solid waste-based foamed lightweight soil is fabricated using Bayer red mud, mineral powder, and [...] Read more.
Traditional cement-based foamed lightweight soils suffer from high construction costs, poor durability, and low solid waste utilization efficiency, which severely restrict their engineering application. A novel polyvinyl alcohol (PVA)-reinforced solid waste-based foamed lightweight soil is fabricated using Bayer red mud, mineral powder, and fly ash. To clarify the durability evolution mechanisms, systematic freeze–thaw cycling, long-term water immersion, and sodium sulfate erosion tests were conducted on PVA-reinforced solid waste-based, unreinforced solid waste-based, and pure cement-based specimens. The results demonstrate that the PVA-reinforced specimen achieves optimal freeze–thaw resistance with only 17.10% strength loss after 50 cycles, owing to the internal three-dimensional fiber network that restrains crack propagation and enhances matrix toughness. It also exhibits excellent long-term water immersion stability, with a mild strength increment of 4.04–10.33% after 120 days. In contrast, the CN exhibited a strength increase of 43.62%, attributed to its lower initial strength caused by incomplete hydration; however, its final strength remained between those of the other two groups. In sulfate environments, unreinforced solid waste-based specimens present superior corrosion resistance, while PVA fiber-induced interconnected pores slightly weaken sulfate erosion resistance. Microscopic analysis confirms that the generation of alunite and gypsum hydration products fundamentally causes performance discrepancies among different specimens. Different from previous studies focusing on single fiber modification or single solid waste partial replacement of cement, this study innovatively adopts a composite modification strategy of “multi-solid waste alkali-activated matrix + PVA fiber toughening”, and systematically reveals the durability evolution mechanism under multiple harsh environments. Full article
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Article
The Effect of Natural Pozzolanic Coated Waste Tire Aggregates on the Mechanical, Transport and Durability Properties of Fiber-Reinforced and One-Part Hybrid Geopolymer Composites
by Wiam Abdelmagid Taher Elabade, Oğuzhan Yavuz Bayraktar, Halil Oğuzhan Kara, İhsan Kasım Karataş, Mehmet Uğur Yılmazoğlu, Adem Ahıskalı, Mohamed A. Salem Elmekahal and Gökhan Kaplan
Polymers 2026, 18(16), 2014; https://doi.org/10.3390/polym18162014 - 19 Aug 2026
Viewed by 350
Abstract
This study examined the effects of coating waste tire aggregates (WTAs) with pumice, perlite, or diatomite, combined with polypropylene (PP) fiber addition, on the fresh, mechanical, transport, and durability properties of one-part hybrid geopolymer composites. Sixteen mixtures were produced using a Taguchi L16 [...] Read more.
This study examined the effects of coating waste tire aggregates (WTAs) with pumice, perlite, or diatomite, combined with polypropylene (PP) fiber addition, on the fresh, mechanical, transport, and durability properties of one-part hybrid geopolymer composites. Sixteen mixtures were produced using a Taguchi L16 design with a binder system of fly ash, CEM II/B-S cement, and sodium metasilicate powder. Coating type, WTA ratio, and PP fiber content were the key performance factors. Pumice coating performed best overall by improving the interfacial transition zone: 28-day compressive strength reached 15.5 MPa and flexural strength 1.60 MPa, while porosity and capillary water absorption decreased significantly. Among the studied WTA levels, 10% WTA yielded the most positive direct responses in compressive strength, flexural strength, toughness, and capillary water absorption, whereas higher contents weakened matrix continuity. The effect of PP fiber was response-dependent: 0.5% fiber maximized compressive strength and durability-related responses, while 2% fiber gave the greatest flexural strength and toughness; no single dosage was universally optimal. The pumice-coated series was also the most stable under high temperature, freeze–thaw, MgSO4, and H2SO4 exposure. Overall, waste tire aggregates can be technically incorporated into one-part hybrid geopolymer composites; a dedicated life-cycle assessment is nevertheless required to quantify the net environmental benefit. Full article
(This article belongs to the Special Issue Research Progress on Mechanical Behavior of Polymers, 2nd Edition)
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