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56 pages, 12556 KB  
Review
The Recent Advancements in Minimum Quantity Lubrication (MQL) and Its Application in Mechanical Machining—A State-of-the-Art Review
by Aqib Mashood Khan, MD Rahatuzzaman Rahat, Umayar Ahmed, Muhammad Jamil, Muhammad Asad Ali, Guolong Zhao and José V. Abellán-Nebot
Lubricants 2025, 13(9), 401; https://doi.org/10.3390/lubricants13090401 - 9 Sep 2025
Viewed by 693
Abstract
The move toward environmentally friendly methods in the global manufacturing sector has led to the use of minimum quantity lubrication (MQL) as an eco-friendly alternative to traditional flood cooling. However, the natural limits of MQL in high-performance settings have led to the use [...] Read more.
The move toward environmentally friendly methods in the global manufacturing sector has led to the use of minimum quantity lubrication (MQL) as an eco-friendly alternative to traditional flood cooling. However, the natural limits of MQL in high-performance settings have led to the use of nanotechnology, which has resulted in the creation of nanofluids, engineered colloidal suspensions that significantly improve the thermophysical and tribological properties of base fluids. This paper gives a complete overview of the latest developments in nanofluid technology for use in machining. It starts with the basics of MQL and the rules for making, describing, and keeping nanofluids stable. The review examines the application and effectiveness of single and hybrid nanofluids in various machining processes. It goes into detail about how they improve tool life, surface integrity, and overall efficiency. It also examines the benefits of integrating nanofluid-assisted MQL (NMQL) with more advanced and hybrid systems, including cryogenic cooling (cryo-NMQL), ultrasonic atomization, electrostatic–magnetic assistance, and multi-nozzle delivery systems. The paper also gives a critical look at the main problems that these technologies face, such as the long-term stability of nanoparticle suspensions, their environmental and economic viability as measured by life cycle assessment (LCA), and the important issues of safety, toxicology, and disposal. This review gives a full picture of the current state and future potential of nanofluid-assisted sustainable manufacturing by pointing out important research gaps, like the need for real-time LCA data, cost-effective scalability, and the use of artificial intelligence (AI) to improve processes, and by outlining future research directions. Full article
(This article belongs to the Special Issue Nanofluid Minimum Quantity Lubrication)
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30 pages, 9222 KB  
Article
Thermodynamic Modeling of Multilayer Insulation Schemes Coupling Liquid Nitrogen Cooled Shield and Vapour Hydrogen Cooled Shield for LH2 Tank
by Jingyang Lu, Liqiong Chen and Xingyu Zhou
Processes 2025, 13(8), 2574; https://doi.org/10.3390/pr13082574 - 14 Aug 2025
Viewed by 481
Abstract
The thermal insulation performance of liquid hydrogen (LH2) storage tanks is critical for long-distance transportation. The active cooled shield (ACS) technologies, such as the liquid nitrogen cooled shield (LNCS) and the vapor hydrogen cooled shield (VHVCS) are important thermal insulation methods. [...] Read more.
The thermal insulation performance of liquid hydrogen (LH2) storage tanks is critical for long-distance transportation. The active cooled shield (ACS) technologies, such as the liquid nitrogen cooled shield (LNCS) and the vapor hydrogen cooled shield (VHVCS) are important thermal insulation methods. Many researchers installed the VHVCS inside the multilayer insulation (MLI) and obtained the optimal position. However, the MLI layer is often thinner than the vacuum interlayer between the inner and outer tanks, and there is a large vacuum interlayer between the outermost side of MLI and the inner wall of the outer tank. It is unknown whether the insulation performance can be improved if we install ACS in the mentioned vacuum interlayer and separate a portion of the MLI to be installed on the outer surface of ACS. In this configuration, the number of inner MLI (IMLI) layers and the ACS position are interdependent, a coupling that has not been thoroughly investigated. Therefore, thermodynamic models for MLI, MLI-LNCS, and MLI-VHVCS schemes were developed based on the Layer-by-Layer method. By applying Robin boundary conditions, the temperature distribution and heat leakage of the MLI scheme were predicted. Considering the coupled effects of IMLI layer count and ACS position, a co-optimization strategy was adopted, based on an alternating iterative search algorithm. The results indicate that for the MLI-LNCS scheme, the optimal number of IMLI layers and LNCS position are 36 layers and 49%, respectively. For the MLI-VHVCS scheme, the optimal values are 21 layers and 39%, respectively. Compared to conventional MLI, the MLI-LNCS scheme achieves an 88.09% reduction in heat leakage. However, this improvement involves increased system complexity and higher operational costs from LN2 circulation. In contrast, the MLI-VHVCS scheme achieves a 62.74% reduction in heat leakage, demonstrating that using sensible heat from cryogenic vapor can significantly improve the thermal insulation performance of LH2 storage tanks. The work of this paper provides a reference for the design and optimization of the insulation scheme of LH2 storage tanks. Full article
(This article belongs to the Section Chemical Processes and Systems)
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9 pages, 9442 KB  
Communication
Temperature-Insensitive Cryogenic Packaging for Thin-Film Lithium Niobate Photonic Chips
by Yongteng Wang, Yuxin Ma, Xiaojie Wang, Ziwei Zhao, Yongmin Li and Tianshu Yang
Photonics 2025, 12(6), 545; https://doi.org/10.3390/photonics12060545 - 28 May 2025
Cited by 1 | Viewed by 1221
Abstract
As photonic integrated circuits (PICs) gain prominence in quantum communication and quantum computation, the development of efficient and stable cryogenic packaging technologies becomes paramount. This paper presents a robust and scalable cryogenic packaging method for thin-film lithium niobate (TFLN) photonic chips. The packaged [...] Read more.
As photonic integrated circuits (PICs) gain prominence in quantum communication and quantum computation, the development of efficient and stable cryogenic packaging technologies becomes paramount. This paper presents a robust and scalable cryogenic packaging method for thin-film lithium niobate (TFLN) photonic chips. The packaged fiber-to-chip interface shows a coupling efficiency of 15.7% ± 0.3%, with minimal variation of ±0.5% as the temperature cools down from 295 K to 1.5 K. Furthermore, the packaged chip exhibits outstanding stability over multiple thermal cycling, highlighting its potential for practical applications in cryogenic environments. Full article
(This article belongs to the Section Optoelectronics and Optical Materials)
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20 pages, 30192 KB  
Article
Influence of Nanocomposite PVD Coating on Cutting Tool Wear During Milling of 316L Stainless Steel Under Air Cooling Conditions
by Jarosław Tymczyszyn, Artur Szajna and Grażyna Mrówka-Nowotnik
Materials 2025, 18(9), 1959; https://doi.org/10.3390/ma18091959 - 25 Apr 2025
Cited by 1 | Viewed by 605
Abstract
This study examines the impact of PVD coatings on cutting tool wear during the milling of 316L stainless steel under air cooling conditions. In the experiment, a carbide milling cutter coated with a nanocomposite nACo3 (AlTiSiN) coating was used. The coating was deposited [...] Read more.
This study examines the impact of PVD coatings on cutting tool wear during the milling of 316L stainless steel under air cooling conditions. In the experiment, a carbide milling cutter coated with a nanocomposite nACo3 (AlTiSiN) coating was used. The coating was deposited using a next-generation device, the PLATIT π411PLUS, which features one central and three lateral rotating cathodes. The nanocomposite nACo3 coating obtained with this method exhibits exceptionally high structural density and excellent mechanical properties. The new generation of the nACo3 coating demonstrates improved surface properties and a lower friction coefficient compared to previous generations. The findings indicate that PVD nACo3 coatings significantly enhance wear resistance, extending tool life while maintaining acceptable surface quality. The optimal cutting time was determined to be approximately 90 min, after which a sharp increase in surface roughness and tool wear was observed. After 120 min of machining, substantial deterioration of surface quality parameters was recorded, suggesting increasing cutting forces and cutting edge degradation. SEM and EDS analyses revealed the presence of adhered material on the tool and sulfide inclusions in the microstructure of 316L stainless steel, which influenced the machining process. The nACo3 coating demonstrated high thermal and wear resistance, making it an effective solution for machining difficult-to-cut materials. This study suggests that selecting appropriate cutting parameters, tool geometry, protective coatings, and cooling strategies can significantly affect tool longevity and machining quality. The novelty of this research lies in the application of innovative nanocomposite PVD coatings during the milling of 316L stainless steel under air cooling conditions. These studies indicate potential future research directions, such as the use of minimum quantity lubrication (MQL) or cryogenic cooling as methods to reduce tool wear and improve post-machining surface quality. Full article
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17 pages, 3791 KB  
Article
Multi-Objective Optimization of Milling Ti-6Al-4V Alloy for Improved Surface Integrity and Sustainability Performance
by Djordje Cica, Sasa Tesic, Milisav Markovic, Branislav Sredanovic, Stevo Borojevic, Milan Zeljkovic, Davorin Kramar and Franci Pušavec
Machines 2025, 13(3), 221; https://doi.org/10.3390/machines13030221 - 8 Mar 2025
Cited by 1 | Viewed by 1271
Abstract
Ti-6Al-4V is a titanium-based alloy that is widely used in a diverse range of applications, especially in industries such as biomedical and aerospace. Several lubricooling techniques have been introduced to enhance the machinability of these materials. Among them, environmentally friendly strategies are gaining [...] Read more.
Ti-6Al-4V is a titanium-based alloy that is widely used in a diverse range of applications, especially in industries such as biomedical and aerospace. Several lubricooling techniques have been introduced to enhance the machinability of these materials. Among them, environmentally friendly strategies are gaining in importance, with sustainability trends rising in manufacturing. The present research investigates the effect of two eco-friendly lubricooling techniques (minimum quantity lubrication and cryogenic cooling), along with other cutting parameters (cutting speed and feed per tooth), on the surface roughness and microhardness of the machined surfaces, which are identified as one of the most frequently implemented indicators of surface integrity in the ball-end milling of the Ti-6Al-4V alloy. In addition, the total electrical energy consumption of the machine tools under different cooling/lubrication conditions was also analyzed. The results obtained showed that cryogenic cooling enhanced milling performance as compared to MQL. Moreover, a multi-objective parameter optimization model integrating the machining responses (surface roughness, microhardness, energy consumption, and productivity) and sustainability metrics (environmental impact, operator’s health and safety, and waste management) was introduced. It was found that cryogenic cooling outperformed the MQL method in terms of both machining performance and environmental impact. An analysis of variance (ANOVA) was carried out to evaluate the significance of each process parameter on the multiple performance index. The results indicate that feed per tooth, cooling method, and cutting speed were significant, with respective contributions of 39.4%, 36.8%, and 22.9%. Finally, the optimal parameter setting was verified through a confirmation test and the results reveal that an improvement was observed in the machining responses and multiple performance index. Full article
(This article belongs to the Section Advanced Manufacturing)
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54 pages, 3811 KB  
Review
Evolution and Latest Trends in Cooling and Lubrication Techniques for Sustainable Machining: A Systematic Review
by Samuel Polo, Eva María Rubio, Marta María Marín and José Manuel Sáenz de Pipaón
Processes 2025, 13(2), 422; https://doi.org/10.3390/pr13020422 - 5 Feb 2025
Cited by 2 | Viewed by 3051
Abstract
This document presents a review on cooling and lubrication methods in machining. A systematic search of information related to these methods was carried out based on the PRISMA (Preferred Reporting Items for Systematic Reviews and Meta-Analyses) methodology. The importance of the sustainability of [...] Read more.
This document presents a review on cooling and lubrication methods in machining. A systematic search of information related to these methods was carried out based on the PRISMA (Preferred Reporting Items for Systematic Reviews and Meta-Analyses) methodology. The importance of the sustainability of machining processes is highlighted, as they represent between 10 and 17% of the total manufacturing cost of the final part and have negative environmental and health impacts. Although dry machining completely eliminates the use of cutting fluids, in many cases it produces unsatisfactory results due to the increase in temperature inside the tool, which requires prior analysis to ensure its viability compared to conventional techniques. On the other hand, semi-dry machining, which significantly reduces the volume of cutting fluids, is a more competitive alternative, with results similar to those of conventional machining. Other sustainable cooling and lubrication methods are also being investigated, such as cryogenic and high-pressure cooling, which offer better machining results than conventional processes. However, they have a high initial cost and further research is needed to integrate them into industry. While the combination of these cooling and lubrication methods could lead to improved results, there is a notable lack of comprehensive studies on the subject. Full article
(This article belongs to the Special Issue Process Automation and Smart Manufacturing in Industry 4.0/5.0)
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15 pages, 1633 KB  
Article
Evaluation of Sustainability and Cost Effectiveness of Using LCO2 as Cutting Fluid in Industrial Hard-Turning Installations
by Iñigo Llanos, Iker Urresti Espilla, David Bilbatua and Oier Zelaieta
Sustainability 2024, 16(22), 10078; https://doi.org/10.3390/su162210078 - 19 Nov 2024
Cited by 1 | Viewed by 1390
Abstract
Conventional oil-based emulsions used in hard-turning processes present significant environmental and economic challenges, including high waste generation and hazardous disposal requirements. In response, cryogenic CO2 cooling has gained attention as a sustainable alternative, offering improved productivity, reduced tool wear and a diminished [...] Read more.
Conventional oil-based emulsions used in hard-turning processes present significant environmental and economic challenges, including high waste generation and hazardous disposal requirements. In response, cryogenic CO2 cooling has gained attention as a sustainable alternative, offering improved productivity, reduced tool wear and a diminished environmental footprint. While technical advances have been reported, the industrial adoption of cryogenic cooling is still limited due to the lack of clear data on its actual viability. This paper moves beyond the analysis of the technical performance of cryogenic CO2 cooling analyzed in previous works to conduct a detailed evaluation of its environmental and economic performance when machining roller bearing components with pCBN tools on a hard-turning installation. Utilizing Life Cycle Assessment (LCA) and Return-on-Investment (ROI) methodologies, this study compares cryogenic CO2 with traditional cooling methods, quantitatively assessing the environmental impact and economic viability across different manufacturing scenarios. The findings reveal that cryogenic cooling can outperform conventional cooling regarding both environmental impact and cost-effectiveness thanks to the tool life improvements provided by cryogenic cooling, specifically in cases where high tool consumption is generated during hard-turning operations. These results provide critical insights for selecting cooling strategies during the design phase of industrial turnkey projects, highlighting the potential of cryogenic CO2 as a superior solution for sustainable and efficient hard-turning operations. Full article
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20 pages, 10195 KB  
Article
Finite Element Simulation of Ti-6Al-4V Alloy Machining with a Grain-Size-Dependent Constitutive Model Considering the Ploughing Effect Under MQL and Cryogenic Conditions
by Guang Chen, Zhuoyang Wu, James Caudill and I. S. Jawahir
J. Manuf. Mater. Process. 2024, 8(6), 239; https://doi.org/10.3390/jmmp8060239 - 28 Oct 2024
Cited by 2 | Viewed by 2132
Abstract
The finite element modeling method has been widely applied in the modeling of the cutting process to characterize the instantaneous and microscale deformation mechanism that was difficult to obtain using physical experiments. The lubrication and cooling conditions, such as minimum quantity lubrication and [...] Read more.
The finite element modeling method has been widely applied in the modeling of the cutting process to characterize the instantaneous and microscale deformation mechanism that was difficult to obtain using physical experiments. The lubrication and cooling conditions, such as minimum quantity lubrication and cryogenic liquid nitrogen, affect the thermo-mechanical behaviors and machined surface integrity in the cutting process. In this work, a grain-size-dependent constitutive model was used to model orthogonal cutting for Ti-6Al-4V alloy with MQL and LN2 conditions. The cutting forces and chip morphologies that were measured in the cutting experiments of Ti-6Al-4V alloy were used to validate the simulated forces. The relative errors between the measured and simulated principal forces were less than 8%, while the relative errors of thrust forces were less than 19%. The predicted chip morphologies and surface grain refinement agreed well with the experimental results under the conditions with different uncut chip thicknesses and edge radii. Additionally, the relationship between the plastic displacement and grain refinement, as well as the microhardness and residual stresses under MQL and cryogenic conditions, were discussed. This work provides an effective modeling method for the orthogonal cutting of Ti-6Al-4V alloy to understand the mechanism of the plastic deformation and machined surface integrity under the MQL and LN2 conditions. Full article
(This article belongs to the Special Issue Advances in High-Performance Machining Operations)
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18 pages, 6821 KB  
Article
Effect of Cryogenic Treatment on Residual Stress and Microstructure of 6061 Aluminum Alloy and Optimization of Parameters
by Xuemei Niu, Zhi Chen, Linwang Jing, Yao Huang and Yuhang Liu
Materials 2024, 17(19), 4873; https://doi.org/10.3390/ma17194873 - 4 Oct 2024
Cited by 3 | Viewed by 1750
Abstract
Residual stress induced by solution treatment in 6061 aluminum alloy can lead to workpiece deformation, or even premature failure. The efficiency of traditional heat treatment for relieving residual stress is relatively low. Therefore, this study introduces a novel cryogenic treatment technique to reduce [...] Read more.
Residual stress induced by solution treatment in 6061 aluminum alloy can lead to workpiece deformation, or even premature failure. The efficiency of traditional heat treatment for relieving residual stress is relatively low. Therefore, this study introduces a novel cryogenic treatment technique to reduce residual stress. The optimal cryogenic process parameters were achieved by orthogonal experiments: cryogenic temperature of 113 K, holding time of 24 h, 1 cryogenic cycle, and a cooling rate of 3 K·min−1, and the residual stress of aluminum alloy was measured by the blind hole method. The microstructural evolutions in 6061 aluminum alloy were tested by OM, SEM, and TEM. The results show that the introduction of cryogenic treatment can reduce residual stress in 6061 aluminum alloy by 64%, mainly due to the reduction of dislocations and the uniform distribution of β’’ phase. Full article
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17 pages, 6642 KB  
Review
Therapeutic Effect of Superficial Scalp Hypothermia on Chemotherapy-Induced Alopecia in Breast Cancer Survivors
by Kefah Mokbel, Alevtina Kodresko, Jon Trembley and Hussam Jouhara
J. Clin. Med. 2024, 13(18), 5397; https://doi.org/10.3390/jcm13185397 - 12 Sep 2024
Cited by 3 | Viewed by 3524
Abstract
Alopecia is a common adverse effect of neoadjuvant or adjuvant chemotherapy in patients with early breast cancer. While hair typically regrows over time, more than 40% of patients continue to suffer from permanent partial alopecia, significantly affecting body image, psychological well-being, and quality [...] Read more.
Alopecia is a common adverse effect of neoadjuvant or adjuvant chemotherapy in patients with early breast cancer. While hair typically regrows over time, more than 40% of patients continue to suffer from permanent partial alopecia, significantly affecting body image, psychological well-being, and quality of life. This concern is a recognized reason why some breast cancer patients decline life-saving chemotherapy. It is critical for healthcare professionals to consider the impact of this distressing side effect and adopt supportive measures to mitigate it. Among the various strategies investigated to reduce chemotherapy-induced alopecia (CIA), scalp cooling has emerged as the most effective. This article reviews the pathophysiology of CIA and examines the efficacy of different scalp cooling methods. Scalp cooling has been shown to reduce the incidence of CIA, defined as less than 50% hair loss, by 50% in patients receiving chemotherapy. It is associated with high patient satisfaction and does not significantly increase the risk of scalp metastasis or compromise overall survival. Promising new scalp cooling technologies, such as cryogenic nitrogen oxide cryotherapy, offer the potential to achieve and maintain lower scalp temperatures, potentially enhancing therapeutic effects. Further investigation into these approaches is warranted. Research on CIA is hindered by significant heterogeneity and the lack of standardised methods for assessing hair loss. To advance the field, further interdisciplinary research is crucial to develop preclinical models of CIA, establish a uniform, internationally accepted and standardised classification system, and establish an objective, personalised prognosis monitoring system. Full article
(This article belongs to the Section Oncology)
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22 pages, 8360 KB  
Review
Review Regarding the Influence of Cryogenic Milling on Materials Used in the Aerospace Industry
by Bogdan Nita, Raluca Ioana Tampu, Catalin Tampu, Bogdan Alexandru Chirita, Eugen Herghelegiu and Carol Schnakovszky
J. Manuf. Mater. Process. 2024, 8(5), 186; https://doi.org/10.3390/jmmp8050186 - 24 Aug 2024
Cited by 1 | Viewed by 3231
Abstract
In the aerospace industry, an important number of machined parts are submitted for high-performance requirements regarding surface integrity. Key components are made of materials selected for their unique properties and they are obtained by milling processes. In most situations, the milling process uses [...] Read more.
In the aerospace industry, an important number of machined parts are submitted for high-performance requirements regarding surface integrity. Key components are made of materials selected for their unique properties and they are obtained by milling processes. In most situations, the milling process uses cooling methods because, in their absence, the material surface could be affected by the generated heat (temperatures could reach up to 850 °C), the residual stress, the cutting forces, and other factors that can lead to bad integrity. Cryogenic cooling has emerged as a pivotal technology in the manufacturing of aeronautical materials, offering enhanced properties and efficiency in the production process. By utilizing extremely low temperatures, typically involving liquid nitrogen or carbon dioxide, cryogenic cooling can significantly enhance the material’s properties and machining processes. Cryogenic gases are tasteless, odorless, colorless, and nontoxic, and they evaporate without affecting the workers’ health or producing residues. Thus, cryogenic cooling is also considered an environmentally friendly method. This paper presents the advantages of cryogenic cooling compared with the classic cooling systems used industrially. Improvements in terms of surface finishing, tool life, and cutting force are highlighted. Full article
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11 pages, 8218 KB  
Article
Research on Tool Wear and Machining Characteristics of TC6 Titanium Alloy with Cryogenic Minimum Quantity Lubrication (CMQL) Technology
by Zhaoyuan Zhang, Weikun Zhang, Xueni Zhang, Xingkai Li, Luyan Ju and Tianping Gu
Processes 2024, 12(8), 1747; https://doi.org/10.3390/pr12081747 - 20 Aug 2024
Cited by 1 | Viewed by 1287
Abstract
Titanium alloys are crucial in precision manufacturing due to their exceptional properties, but traditional machining methods lead to tool wear, deformation, and high costs. Conventional cooling fluids reduce heat but cause environmental issues, necessitating more sustainable solutions. Cryogenic Minimum Quantity Lubrication (CMQL) technology, [...] Read more.
Titanium alloys are crucial in precision manufacturing due to their exceptional properties, but traditional machining methods lead to tool wear, deformation, and high costs. Conventional cooling fluids reduce heat but cause environmental issues, necessitating more sustainable solutions. Cryogenic Minimum Quantity Lubrication (CMQL) technology, using liquid nitrogen or carbon dioxide with minimal amounts of cutting fluid, offers an eco-friendly alternative that reduces machining temperatures and friction. This study tested the TC6 titanium alloy under conventional and CMQL conditions, focusing on tool wear, surface quality, and machining efficiency. Results showed that CMQL significantly decreased tool wear and surface roughness, with a 42% reduction in surface roughness during drilling and a 20–30% efficiency increase. The findings highlight CMQL’s potential to improve machining quality and efficiency while promoting environmentally friendly practices in the industry. Full article
(This article belongs to the Section Manufacturing Processes and Systems)
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12 pages, 2082 KB  
Article
Laser Scanning Method for Time-Resolved Measurements of Wavefront Distortion Introduced by Active Elements in High-Power Laser Amplifiers
by Alyona O. Kuptsova, Gleb V. Kuptsov, Vladimir A. Petrov, Victor V. Atuchin and Victor V. Petrov
Photonics 2024, 11(8), 748; https://doi.org/10.3390/photonics11080748 - 9 Aug 2024
Cited by 1 | Viewed by 1092
Abstract
A novel method was proposed for the experimental investigation of wavefront distortion introduced to amplified radiation by pumped active elements in high-power laser amplifiers. The method is based on the simultaneous measurement of temperature distribution and the distribution of population density of the [...] Read more.
A novel method was proposed for the experimental investigation of wavefront distortion introduced to amplified radiation by pumped active elements in high-power laser amplifiers. The method is based on the simultaneous measurement of temperature distribution and the distribution of population density of the excited laser level in active elements. The underlying theory of the technique was presented; various factors affecting the accuracy of wavefront distortion determination were analyzed. The method was tested to study the wavefront distortion and the depolarization of radiation introduced by the Yb:YAG active element of a cryogenically cooled laser amplifier with high-power diode pumping. The focal length of the thermal lens was 0.40 ± 0.03 and 0.47 ± 0.05 m for the horizontal and vertical planes, respectively. The focal length of the electron lens was two orders of magnitude larger. The maximum value of losses induced by depolarization was 8.5%. Full article
(This article belongs to the Special Issue New Perspectives in Ultrafast Intense Laser Science and Technology)
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30 pages, 14918 KB  
Article
Wear Mechanism of an AlCrN-Coated Solid Carbide Endmill Cutter and Machined Surface Quality under Eco-Friendly Settings during Open Slot Milling of Tempered JIS SKD11 Steel
by Ly Chanh Trung and Tran Thien Phuc
Coatings 2024, 14(8), 923; https://doi.org/10.3390/coatings14080923 - 23 Jul 2024
Cited by 1 | Viewed by 1427
Abstract
In the die and mold industry, tempered JIS SKD11 steel is selected to manufacture cold-forming dies that require an optimum balance of toughness, strength, and wear resistance. Therefore, the machinability of tempered JIS SKD11 in the milling machining process is challenging. The use [...] Read more.
In the die and mold industry, tempered JIS SKD11 steel is selected to manufacture cold-forming dies that require an optimum balance of toughness, strength, and wear resistance. Therefore, the machinability of tempered JIS SKD11 in the milling machining process is challenging. The use of eco-friendly machining settings is intended to diminish tool wear and enhance the quality of the machined surface as well as the accuracy of the machined components. Adapting to the aforementioned factors for cold-forming dies is a pivotal issue. In this study, the machinability of tempered JIS SKD11 steel was analyzed under dry, MQL, cryogenic cooling with liquid nitrogen (LN2), and liquid carbon dioxide (LCO2) machining settings during open slot milling operations with varying input parameters, including cutting speeds and cutting feeds. An in-depth evaluation of output responses, including tool wear, surface roughness, cutting temperature in the cutting zone, and microhardness of the machined surface, was also conducted. The findings unveiled that the flank wear of the cutters and surface roughness of the machined surfaces obtained minimum values of 0.22 mm and 0.197 µm, respectively, during open slot milling operations at a cutting speed of 100 m/min and a cutting feed of 204 mm/min under cryogenic cooling with liquid carbon dioxide (LCO2). The findings from this study suggest that employing cryogenic cooling with LCO2 could serve as a viable substitute for dry, MQL, and cryogenic cooling with LN2 methods to enhance the machinability of hardened JIS SKD11 steel. Full article
(This article belongs to the Special Issue Friction and Wear Behaviors in Mechanical Engineering)
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14 pages, 2575 KB  
Article
Development of a Refrigerant-Free Cryotrap Unit for Pre-Concentration of Biogenic Volatile Organic Compounds in Air
by Xiaoxiao Ding, Daocheng Gong, Qinqin Li, Shiwei Liu, Shuo Deng, Hao Wang, Hongjie Li and Boguang Wang
Atmosphere 2024, 15(5), 587; https://doi.org/10.3390/atmos15050587 - 11 May 2024
Cited by 4 | Viewed by 1582
Abstract
Biogenic volatile organic compounds (BVOCs) are key compounds in atmospheric chemistries, but difficult to measure directly. In this study, a pre-concentration unit combined with gas chromatography-mass spectrometry (GC-MS) was developed for the quantitative analysis of 18 BVOCs in ambient air. The analytes are [...] Read more.
Biogenic volatile organic compounds (BVOCs) are key compounds in atmospheric chemistries, but difficult to measure directly. In this study, a pre-concentration unit combined with gas chromatography-mass spectrometry (GC-MS) was developed for the quantitative analysis of 18 BVOCs in ambient air. The analytes are trapped on an empty silonite-coated tube, which is cooled by a thermoacoustic cooler to cryotrap at −150 °C, and then desorbed by rapid heating to 200 °C. The set-up involves neither the exchange of solid adsorbents nor any further condensation or refocusing steps. Reliable operation is ensured by the thermoacoustic cooler, which neither contains a liquid refrigerant nor requires refilling a cryogen. The pre-concentration unit parameters such as water removal temperature, desorption temperature and desorption time were optimized. All compounds had correlation coefficients that were better than 0.95, and the detection limits were 0.005–0.009 ppbv when the injection volume is 400 mL. The repeatability ranges were 0.9–5.8%. The recoveries were ranged from 81.8% to 93.2%. This new method was applied for the first time to measure ambient BVOCs in suburb Guangzhou in summer 2022. Isoprene concentrations ranged from 0.375 ppbv to 2.98 ppbv. In addition, several extremely low-level monoterpenes (e.g., α-pinene, β-pinene, and D-limonene) were also detected by the method. Full article
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