Search Results (11)

The use of agricultural waste fibres and natural binders is being investigated as alternatives to synthetic indoor acoustic materials. However, few studies have compared the fibre type, biopolymer type, and fibre-to-binder ratio for both sound absorption and sound transmission within a single controlled composite system. This study investigated the acoustic performance of sugarcane fibre (SF) and coconut fibre (CF) with a fixed thickness of 20 mm and density of 200 kg/m³, mixed with cassava, corn and potato starch binders with fibre–binder ratios from 1:1.0 to 1:0.1. Sound absorption coefficient was measured with an impedance tube, according to ISO 10534-2, and the sound transmission coefficient was determined using a four-microphone impedance tube system, according to ASTM E2611. Porosity was also tested for its relation to acoustic behaviour. The results showed that the coconut fibre composite recorded higher peak absorption, including α = 0.95 for cassava 1:0.6 to 1:0.7 and corn 1:0.6, while sugarcane fibre showed stronger transmission resistance, with SF-CAS-200-1:0.3 decreasing from τ = 0.11 at 160 Hz to 0.02 at 5000 Hz, and SF-PT-200-1:0.4 from τ = 0.10 to 0.03. The highest porosity values were 85.29%, recorded for SC-CAS-200-1:0.1, and 84.13% for CF-CAS-200-1:0.1. Overall, sugarcane fibre composites offered the best balance of absorption and low transmission, indicating strong potential for sustainable indoor acoustic panels, such as ceiling linings and wall systems. Further research should evaluate mechanical strength, fire performance, durability, and moisture resistance to support practical building applications. Full article

Cassava is a major starch crop in Africa, generating substantial amounts of solid (peels and fibres) and liquid (process press water) residues that remain underutilised, particularly in smallholder and semi-industrial processing units. In Mozambique, where cassava is a staple and processed primarily by local farmer associations, these residues—readily available and low-cost feedstocks—have significant potential for value-added applications. This study evaluated the potential of enzymatically hydrolysed cassava residues—peel and fibre hydrolysates—as substrates for independent yeast fermentations targeting microbial lipid and ethanol production. Rhodotorula toruloides CBS 14 efficiently converted sugars from both hydrolysates, producing up to 17.14 g L⁻¹ of cell dry weight (CDW) and 35% intracellular lipid content from the peel hydrolysate, and 16.5 g L⁻¹ CDW with 50% lipids from the fibre hydrolysate. Supplementation with ammonium sulphate accelerated sugar utilisation and reduced fermentation time but did not significantly increase the biomass or lipid yields. Saccharomyces cerevisiae J672 fermented the available sugars anaerobically, achieving ethanol yields of 0.45 ± 0.03 g g⁻¹ glucose from peels and 0.37 ± 0.06 g g⁻¹ glucose from fibres. These findings highlight the regional relevance of valorising cassava processing residues in Mozambique and demonstrate a dual-product valorisation strategy, whereby the same feedstocks are converted into either microbial lipids or ethanol through independent fermentations. This approach supports the sustainable, low-cost utilisation of agro-industrial residues, contributing to circular bioeconomy principles and enhancing the environmental and economic value of local cassava value chains. Full article

Additive manufacturing using fused deposition modelling (FDM) is increasingly explored for personalised drug delivery, but the lack of suitable biodegradable and printable filaments limits its pharmaceutical application. In this study, we investigated the influence of formulation and structural design on the performance of polyvinyl alcohol (PVA)-based filaments doped with theophylline anhydrous for 3D printing. To address the intrinsic brittleness and poor printability of PVA, cassava pulp-derived fibres—a sustainable and underutilised agricultural by-product—were incorporated together with polyethylene glycol (PEG 400), Eudragit^® NE 30 D, and calcium stearate. The addition of fibres modified the mechanical properties of PVA filaments through hydrogen bonding, improving flexibility but increasing surface roughness. This drawback was mitigated by Eudragit^® NE 30 D, which enhanced surface smoothness and drug distribution uniformity. The optimised composite formulation (P₁₀F₅E₅T₅) was successfully extruded and used to fabricate 3D-printed constructs. Release studies demonstrated that drug release could be modulated by pore geometry and construct thickness: wider pores enabled rapid Fickian diffusion, while narrower pores and thicker constructs shifted release kinetics toward anomalous transport governed by polymer swelling. These findings demonstrate, for the first time, the potential of cassava fibre as a functional additive in pharmaceutical FDM and provide a rational formulation–structure–performance framework for developing sustainable, geometry-tuneable drug delivery systems. Full article

Spontaneous fermentation is currently used to produce lafun from cassava, leading to inconsistent product quality and decreased safety. Using starter cultures and optimising the selection of the raw materials can overcome this. This study evaluated the impact of various lactic acid bacteria (LAB) starters and varieties of cassava (bitter: IBA30527; vitamin A fortified bitter: IBA011371; and sweet: TMEB117) on the proximate, rheological, and volatile profiles of lafun. The varieties were fermented with four selected LAB (two strains of Weissella koreensis, Lactococcus lactis, and Leuconostoc mesenteroides). The use of fortified cassava showed higher potential to improve the quality of lafun. The combination of fortified cassava and Leuconostoc mesenteroides gave the highest nutritional value (ash: 4.37% cf. 1.33%; protein: 3.08% cf. 0.87%; and fibre: 7.43% cf. 1.43%). Fermenting the fortified cassava with Weissella koreensis-2 produced lafun gruel with the best viscoelastic properties, indicating an overall better product quality. The fortified cassava fermented with combined cultures of W. koreensis-1 and L. lactis resulted in a product with lower levels of carboxylic acids (cheesy) and lipid oxidation products (fried, rancid) but higher concentrations of carotenoid-derived compounds (fruity). The use of LAB in the controlled fermentation of fortified cassava could be a sustainable alternative to improve the physical, nutritional, and flavour properties of lafun. Full article

Dietary fibre deficiency has been associated with various global health challenges. Starch, as a main component of many staple foods, is typically very low in fibre content. The primary aim of this research was to increase the dietary fibre and alter the physicochemical properties of some common and emerging starches (cassava, quinoa, and chickpea starch) using eco-friendly modifications. Citric acid, a safe, natural, and environmentally friendly cross-linking agent, was employed for this purpose. Starch samples were treated with 30% citric acid and dry-heated at 130 °C for 5 h. This process resulted in relatively high degrees of substitution: 0.124 for cassava, 0.117 for quinoa, and 0.112 for chickpea starches. The modification successfully produced rich sources of dietary fibre suitable for food applications. It also reduced water interactions, pasting properties, and crystallinity. The highest reduction in swelling power and solubility was observed in quinoa starch (−67.34% and −82.10%, respectively), while the lowest values were obtained for cassava starch (−35.39% and −44.22%). All starches retained their granular integrity; however, they lost birefringence and Maltese crosses and showed some erosions on the granule surfaces. The citrate starches produced in this research offer thermally stable starch suitable for various food applications. Full article

In response to the growing demand for high-quality food ingredients, starches from underutilised sources like quinoa and faba bean are gaining attention due to their unique properties and high tolerance to adverse environmental conditions. Acid hydrolysis is a well-established chemical method for producing modified starch with improved solubility, lower gelatinisation temperature, and reduced pasting viscosity. However, various outcomes can be achieved depending on the type of starch and modification conditions. This study comparatively investigated the effects of acid hydrolysis on the functional and physicochemical properties of emerging starches from quinoa and faba bean, with cassava starch serving as a reference from a leading source. The results demonstrated increased dietary fibre content across all three starches, with faba bean starch showing the most significant rise. Acid treatment also enhanced the crystallinity of the starches, with faba bean starch exhibiting the highest increase in relative crystallinity, which led to a shift towards higher temperatures in their thermal properties. Additionally, water solubility and oil adsorption capacity increased, while swelling power decreased following acid treatment. The acid treatment reduced the pasting properties of all samples, indicating that the modified starches were more resistant to heating and shearing in the rapid visco analyser. While quinoa starch gel remained soft after acid hydrolysis, the gel strength of cassava and faba bean starches improved significantly, making them suitable as plant-based gelling agents. Full article

Cymbopogan citratus fibre (CCF) is an agricultural waste plant derived from a natural cellulosic source of fibre that can be used in various bio-material applications. This paper beneficially prepared thermoplastic cassava starch/palm wax blends incorporated with Cymbopogan citratus fibre (TCPS/PW/CCF) bio-composites at different CCF concentrations of 0, 10, 20, 30, 40, 50 and 60 wt%. In contrast, palm wax loading remained constant at 5 wt% concentration using the hot moulding compression method. TCPS/PW/CCF bio-composites were characterised in the present paper via their physical and impact properties. The addition of CCF significantly improved impact strength by 50.65% until 50 wt% CCF loading. Furthermore, it was observed that the inclusion of CCF resulted in a little decrement in biocomposite solubility compared to neat TPCS/PW biocomposite from 28.68% to 16.76%. Water absorption showed higher water resistance in the composites incorporating 60 wt.% fibre loading. The TPCS/PW/CCF biocomposites with different fibre contents had 11.04–5.65% moisture content, which was lower than the control biocomposite. The thickness of all samples decreased gradually with increasing fibre content. Overall, these findings provide evidence that CCF waste can be utilised as a high-quality filler in biocomposites due to its diverse characteristics, including improving the properties of biocomposites and strengthening their structural integrity. Full article

Growing environmental concerns have heightened interest in the development of environmentally friendly materials. The purpose of this study is to evaluate how the mechanical and thermal properties of thermoplastic cassava starch (TPCS) are affected by the presence of banana leaf fibre (BLF). By incorporating between 10% and 80% by weight of banana leaf fibre into the TPCS matrix, the biocomposites were created. The thermal and mechanical parameters of the samples were determined. The results revealed that the material’s flexural and tensile characteristics improved significantly, with 50% BLF content in the matrix achieving the highest strength of 20.86 MPa, a flexural strength of 32 MPa, and tensile modulus values. Thermogravimetric examination observed that the addition of BLF improved the material’s thermal stability. The Scanning Electron Microscopy (SEM) morphological tests demonstrated an even spread of banana leaf fibre and a matrix with strong adhesion, which improved the mechanical properties of the biocomposites. The Fourier Transform Infrared Spectroscopy (FT-IR) testing, which confirmed the biocomposite presence of O-H bonds, also confirmed the strong intermolecular hydrogen bonding between TPCS and banana leaf fibre. Full article

Increasing environmental awareness and concern have shifted the focus of research and development towards biodegradable materials development. In the current study, Cymbopogan citratus fibre (CCF) were incorporated into thermoplastic cassava starch (TPCS) with various content of CCF (10, 20, 30, 40, 50, 60 wt.%) via compression moulding. The determination of fundamental characteristics of TPCS/CCF biopolymer composites was conducted to assess their potential as biodegradable reinforcements. Characterization of the samples was conducted via Fourier-transform infrared spectroscopy (FT-IR), thermogravimetric analysis (TGA), and scanning electron microscopy (SEM), as well as mechanical, moisture absorption, and soil burial testings. The findings showed that the improved tensile and flexural features of the TPCS composites with CCF incorporation, with 50 wt.% CCF content yielded the maximum modulus and strength. The thermal properties of the biocomposite demonstrated that CCF addition improved the material’s thermal stability, as shown by a higher-onset decomposition temperature and ash content. Meanwhile, the CCF incorporation into TPCS slowed down the biodegradation of the composites. In term of morphological, homogeneous fibres and matrix dispersion with excellent adhesion was observed in morphological analyses using scanning electron microscopy (SEM), which is crucial for the enhancement of the mechanical performance of biocomposites. Full article

Increasing environmental concerns have led to greater attention to the development of biodegradable materials. The aim of this paper is to investigate the effect of banana leaf fibre (BLF) on the thermal and mechanical properties of thermoplastic cassava starch (TPCS). The biocomposites were prepared by incorporating 10 to 50 wt.% BLF into the TPCS matrix. The samples were characterised for their thermal and mechanical properties. The results showed that there were significant increments in the tensile and flexural properties of the materials, with the highest strength and modulus values obtained at 40 wt.% BLF content. Thermogravimetric analysis showed that the addition of BLF had increased the thermal stability of the material, indicated by higher-onset decomposition temperature and ash content. Morphological studies through scanning electron microscopy (SEM) exhibited a homogenous distribution of fibres and matrix with good adhesion, which is crucial in improving the mechanical properties of biocomposites. This was also attributed to the strong interaction of intermolecular hydrogen bonds between TPCS and fibre, proven by the FT-IR test that observed the presence of O–H bonding in the biocomposite. Full article

This study was driven by the stringent environmental legislation concerning the consumption and utilization of eco-friendly materials. Within this context, this paper aimed to examine the characteristics of starch and fibres from the Dioscorea hispida tuber plant to explore their potential as renewable materials. The extraction of the Dioscorea hispida starch and Dioscorea hispida fibres was carried out and the chemical composition, physical, thermal, morphological properties, and crystallinity were studied. The chemical composition investigations revealed that the Dioscorea hispida starch (DHS) has a low moisture t (9.45%) and starch content (37.62%) compared to cassava, corn, sugar palm, and arrowroot starches. Meanwhile, the Dioscorea hispida fibres (DHF) are significantly low in hemicellulose (4.36%), cellulose (5.63%), and lignin (2.79%) compared to cassava, corn hull and sugar palm. In this investigation the chemical, physical, morphological and thermal properties of the Dioscorea hispida fibre and Dioscorea hispida starch were examined by chemical composition investigation, scanning electron microscopy (SEM), particle size distribution, thermogravimetric analysis (TGA), X-ray powder diffraction (XRD), and Fourier transform infrared (FTIR), respectively. It was found that Dioscorea hispida waste is promising alternative biomass and sustainable material with excellent potential as a renewable filler material for food packaging applications. Full article