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Keywords = acousto-ultrasonics

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56 pages, 3088 KiB  
Review
Controlling Sedimentation in Magnetorheological Fluids Through Ultrasound–Magnetic Field Coupling: Multiscale Analysis and Applications
by Annunziata Palumbo and Mario Versaci
Mathematics 2025, 13(15), 2540; https://doi.org/10.3390/math13152540 (registering DOI) - 7 Aug 2025
Abstract
Magnetorheological fluids (MRFs) are multiphase materials whose viscosity can be controlled via magnetic fields. However, particle sedimentation undermines their long-term stability. This review examines stabilization strategies based on the interaction between ultrasonic waves and time-varying magnetic fields, analyzed through advanced mathematical models. The [...] Read more.
Magnetorheological fluids (MRFs) are multiphase materials whose viscosity can be controlled via magnetic fields. However, particle sedimentation undermines their long-term stability. This review examines stabilization strategies based on the interaction between ultrasonic waves and time-varying magnetic fields, analyzed through advanced mathematical models. The propagation of acoustic waves in spherical and cylindrical domains is studied, including effects such as cavitation, acoustic radiation forces, and viscous attenuation. The Biot–Stoll poroelastic model is employed to describe saturated granular media, while magnetic field modulation is investigated as a means to balance gravitational settling. The analysis highlights how acousto-magnetic coupling supports the design of programmable and self-stabilizing intelligent fluids for complex applications. Full article
(This article belongs to the Special Issue Engineering Thermodynamics and Fluid Mechanics)
15 pages, 1130 KiB  
Article
Hong–Ou–Mandel Interference on an Acousto-Optical Beam Splitter
by Piotr Kwiek
Optics 2025, 6(2), 25; https://doi.org/10.3390/opt6020025 - 5 Jun 2025
Viewed by 447
Abstract
This paper presents the results of theoretical and experimental investigations of a Hong–Ou–Mandel interferometer in which an optical beam splitter is replaced by an ultrasonic wave. The ultrasonic wave acts as an acousto-optical beam splitter for light, which is based on the phenomenon [...] Read more.
This paper presents the results of theoretical and experimental investigations of a Hong–Ou–Mandel interferometer in which an optical beam splitter is replaced by an ultrasonic wave. The ultrasonic wave acts as an acousto-optical beam splitter for light, which is based on the phenomenon of Bragg diffraction on an ultrasonic wave. The Doppler effect was considered in the theoretical considerations and confirmed experimentally. It has been shown theoretically and experimentally that the Doppler effect changes the frequency of two-photon states at the outputs of an acousto-optical beam splitter. The frequency of the two-photon state in the positive diffraction order is increased by the frequency of the ultrasonic wave, whereas in the negative diffraction order, it is reduced by the frequency of the ultrasonic wave. It should be emphasized that there are no states 1112 in the outputs (diffraction orders), which disappear as a result of Hong–Ou–Mandel interference; consequently, the probability of detecting coincidences of photons between the plus first and minus first diffraction orders is zero, as it occurs in the Hong–Ou–Mandel interferometer. The frequency difference between the two-photon states at the outputs of the acousto-optical beam splitter was confirmed by recording the two-photon beat phenomenon. The obtained results changed the current view that the Doppler effect caused by ultrasonic waves can be neglected in the interaction of correlated pairs of photons with ultrasonic waves. Full article
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14 pages, 3424 KiB  
Article
Temperature Dependence of Nonlinear Elastic Moduli of Polystyrene
by Andrey V. Belashov, Anna A. Zhikhoreva, Yaroslav M. Beltukov and Irina V. Semenova
Polymers 2025, 17(8), 1008; https://doi.org/10.3390/polym17081008 - 8 Apr 2025
Viewed by 538
Abstract
Nonlinear elastic properties of polymers and polymer-based composites are essential for accurate prediction of their response to dynamic loads, which is crucial in a wide range of applications. These properties can be affected by strain rate, temperature, and pressure. The temperature susceptibility of [...] Read more.
Nonlinear elastic properties of polymers and polymer-based composites are essential for accurate prediction of their response to dynamic loads, which is crucial in a wide range of applications. These properties can be affected by strain rate, temperature, and pressure. The temperature susceptibility of nonlinear elastic moduli of polymers remains poorly understood. We have recently observed a significant frequency dependence of the nonlinear elastic (Murnaghan) moduli of polystyrene. In this paper we expanded this analysis by the temperature dependence. The measurement methodology was based on the acousto-elastic effect, and involved analysis of the dependencies of velocities of longitudinal and shear single-frequency ultrasonic waves in the sample on the applied static pressure. Measurements were performed at different temperatures in the range of 25–65 °C and at different frequencies in the range of 0.7–3 MHz. The temperature susceptibility of the nonlinear moduli l and m was found to be two orders of magnitude larger than that of linear moduli λ and μ. At the same time, the observed variations of n modulus with temperature were low and within the measurement tolerance. The observed tendencies can be explained by the shift of nonlinear moduli towards higher frequencies with increasing temperature. Full article
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17 pages, 4847 KiB  
Article
Ultrasonic Atomization—From Onset of Protruding Free Surface to Emanating Beads Fountain—Leading to Mist Spreading
by Katsumi Tsuchiya and Xiaolu Wang
Fluids 2025, 10(4), 89; https://doi.org/10.3390/fluids10040089 - 1 Apr 2025
Viewed by 532
Abstract
The process of ultrasonic atomization involves a series of dynamic/topological deformations of free surface, though not always, of a bulk liquid (initially) below the air. This study focuses on such dynamic interfacial alterations realized by changing some acousto-related operating conditions, including ultrasound excitation [...] Read more.
The process of ultrasonic atomization involves a series of dynamic/topological deformations of free surface, though not always, of a bulk liquid (initially) below the air. This study focuses on such dynamic interfacial alterations realized by changing some acousto-related operating conditions, including ultrasound excitation frequency, acoustic strength or input power density, and the presence/absence of a “stabilizing” nozzle. High-speed, high-resolution imaging made it possible to qualitatively identify four representative transitions/demarcations: (1) the onset of a protrusion on otherwise flat free surface; (2) the appearance of undulation along the growing protuberance; (3) the triggering of emanating beads fountain out of this foundation-like region; and (4) the induction of droplets bursting and/or mist spreading. Quantitatively examined were the two-parameters specifications—on the degrees as well as induction—of the periodicity in the protrusion-surface and beads-fountain oscillations, detected over wider ranges of driving/excitation frequency (0.43–3.0 MHz) and input power density (0.5–10 W/cm2) applied to the ultrasound transducer of flat surface on which the nozzle was either mounted or not. The resulting time sequence of images processed for the extended operating ranges, regarding the fountain structure pertaining, in particular, to recurring beads, confirms the wave-associated nature, i.e., their size “scalability” to the ultrasound wavelength, predictable from the traveling wave relationship. The thresholds in acoustic conditions for each of the four transition states of the fountain structure have been identified—notably, the onset of plausible “bifurcation” in the chain-beads’ diameter below a critical excitation frequency. Full article
(This article belongs to the Special Issue Advances in Multiphase Flow Science and Technology, 2nd Edition)
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13 pages, 6101 KiB  
Proceeding Paper
Characterisation of Novel Self-Healing Composites Using Acousto-Ultrasonic Testing
by Claudia Barile, Vimalathithan Paramsamy Kannan, Giulia Derosa and Giovanni Pappalettera
Eng. Proc. 2025, 85(1), 23; https://doi.org/10.3390/engproc2025085023 - 19 Feb 2025
Viewed by 267
Abstract
Self-healing composites are designed based on natural healing processes such as bone regeneration and blood coagulation. These composites have polymeric material containing covalent adaptable networks that rearrange their molecular structure when heated, thereby serving as a healing agent. The inclusion of the healing [...] Read more.
Self-healing composites are designed based on natural healing processes such as bone regeneration and blood coagulation. These composites have polymeric material containing covalent adaptable networks that rearrange their molecular structure when heated, thereby serving as a healing agent. The inclusion of the healing polymers into the principal matrix of the fiber-reinforced composites alters their off-axis properties. In addition, the healing agents tend to bleed out of the composite structures upon heating. It is, therefore, essential to characterize the extent of the changes in the off-axis properties of the self-healing composites. In this research work, three different configurations of self-healing composites are subjected to three-point bending tests, and their healing characteristics are studied using Acousto-Ultrasonic tests. Frequencies of the propagating stress waves in the AU tests are used to analyze the different conditions of the self-healing composites, such as virgin, damaged, damaged-partially healed, and damaged-fully healed. The results show that the AU test could potentially be used to evaluate the healing behavior of these fiber-reinforced self-healable composites. Full article
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11 pages, 2991 KiB  
Article
High-Bandwidth Heterodyne Laser Interferometer for the Measurement of High-Intensity Focused Ultrasound Pressure
by Ke Wang, Guangzhen Xing, Ping Yang, Min Wang, Zheng Wang and Qi Tian
Micromachines 2023, 14(12), 2225; https://doi.org/10.3390/mi14122225 - 11 Dec 2023
Cited by 1 | Viewed by 1812
Abstract
As a high-end medical technology, high-intensity focused ultrasound (HIFU) is widely used in cancer treatment and ultrasonic lithotripsy technology. The acoustic output level and safety of ultrasound treatments are closely related to the accuracy of sound pressure measurements. Heterodyne laser interferometry is applied [...] Read more.
As a high-end medical technology, high-intensity focused ultrasound (HIFU) is widely used in cancer treatment and ultrasonic lithotripsy technology. The acoustic output level and safety of ultrasound treatments are closely related to the accuracy of sound pressure measurements. Heterodyne laser interferometry is applied to the measurement of ultrasonic pressure owing to its characteristics of non-contact, high precision, and traceability. However, the upper limit of sound pressure measurement is limited by the bandwidth of the interferometer. In this paper, a high-bandwidth heterodyne laser interferometer for the measurement of high-intensity focused ultrasound pressure is developed and tested. The optical carrier with a frequency shift of 358 MHz is realized by means of an acousto-optic modulator. The selected electrical devices ensure that the electrical bandwidth can reach 1.5 GHz. The laser source adopts an iodine frequency-stabilized semiconductor laser with high-frequency spectral purity, which can reduce the influence of spectral purity on the bandwidth to a negligible level. The interference light path is integrated and encapsulated to improve the stability in use. An HIFU sound pressure measurement experiment is carried out, and the upper limit of the sound pressure measurement is obviously improved. Full article
(This article belongs to the Special Issue Progress and Application of Ultra-Precision Laser Interferometry)
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12 pages, 3125 KiB  
Article
Acousto-Optic Transfer Function Control by a Phased-Array Piezoelectric Transducer
by Konstantin B. Yushkov, Alexander I. Chizhikov and Vladimir Ya. Molchanov
Photonics 2023, 10(10), 1167; https://doi.org/10.3390/photonics10101167 - 19 Oct 2023
Cited by 2 | Viewed by 1855
Abstract
We present analysis and numerical simulations of the acousto-optic spatial filter (AOSF) transfer function under the condition of dual-transducer operation and phase control. Based on these simulations, the AOSF crystal configuration is optimized for operation in the near-infrared wavelength region from 0.7 to [...] Read more.
We present analysis and numerical simulations of the acousto-optic spatial filter (AOSF) transfer function under the condition of dual-transducer operation and phase control. Based on these simulations, the AOSF crystal configuration is optimized for operation in the near-infrared wavelength region from 0.7 to 1.0 μm. We demonstrate that ultrasonic phase control can provide efficient tuning of the transfer function, which is independent of conventional frequency control. Thus, the application of phase control coupled with frequency control can reduce the transfer function asymmetry that is inherent to anisotropic Bragg diffraction in uniaxial crystals. Full article
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18 pages, 40385 KiB  
Article
An Efficient Procedure for Bonding Piezoelectric Transducers to Thermoplastic Composite Structures for SHM Application and Its Durability in Aeronautical Environmental Conditions
by Tasdeeq Sofi, Maria R. Gude, Peter Wierach, Isabel Martin and Eduardo Lorenzo
Sensors 2023, 23(10), 4784; https://doi.org/10.3390/s23104784 - 16 May 2023
Cited by 8 | Viewed by 2450
Abstract
Piezoceramic transducers (PCTs) bonded to carbon fiber-reinforced plastic (CFRP) composite structures must be durable as well as remain properly bonded to the structure in order to provide reliable data for accurate guided-wave-based structural health monitoring (SHM) of aeronautical components. The current method of [...] Read more.
Piezoceramic transducers (PCTs) bonded to carbon fiber-reinforced plastic (CFRP) composite structures must be durable as well as remain properly bonded to the structure in order to provide reliable data for accurate guided-wave-based structural health monitoring (SHM) of aeronautical components. The current method of bonding transducers to composite structures through epoxy adhesives faces some shortcomings, such as difficult reparability, lack of weldability, longer curing cycles, and shorter shelf life. To overcome these shortcomings, a new efficient procedure for bonding the transducers to thermoplastic (TP) composite structures was developed by utilizing TP adhesive films. Application-suitable TP films (TPFs) were identified and characterized through standard differential scanning calorimetry (DSC) and single lap shear (SLS) tests to study their melting behavior and bonding strength, respectively. Special PCTs called acousto-ultrasonic composite transducers (AUCTs) were bonded to high-performance TP composites (carbon fiber Poly-Ether-Ether-Ketone) coupons with a reference adhesive (Loctite EA 9695) and the selected TPFs. The integrity and durability of the bonded AUCTs in aeronautical operational environmental conditions (AOEC) were assessed in accordance to the standard Radio Technical Commission for Aeronautics DO-160. The AOEC tests performed were operating low and high temperatures, thermal cycling, hot-wet, and fluid susceptibility tests. The health and bonding quality of the AUCTs were evaluated by the electro-mechanical impedance (EMI) spectroscopy method and ultrasonic inspections. The AUCT defects were created artificially and their influence on the susceptance spectra (SS) was measured to compare them with the AOEC-tested AUCTs. The results show that a small change occurred in the SS characteristics of the bonded AUCTs in all of the adhesive cases after the AOEC tests. After comparing the changes in SS characteristics of simulated defects with that of the AOEC-tested AUCTs, the change is relatively smaller and therefore it can be concluded that no serious degradation of the AUCT or the adhesive layer has occurred. It was observed that the most critical tests among the AOEC tests are the fluid susceptibility tests, which can cause the biggest change in the SS characteristics. Comparing the performance of the AUCTs bonded with the reference adhesive and the selected TPFs in the AOEC tests, it was seen that some of the TPFs, e.g., Pontacol 22.100 outperforms the reference adhesive, while the other TPFs have similar performance to that of the reference adhesive. Therefore, in conclusion, the AUCTs bonded with the selected TPFs can withstand the operational and environmental conditions of an aircraft structure, and hence, the proposed procedure is easily installed, reparable, and a more reliable method of bonding sensors to aircraft structures. Full article
(This article belongs to the Special Issue Structural Health Monitoring Based on Piezoelectric Transducers)
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30 pages, 12366 KiB  
Article
A Freehand 3D Ultrasound Reconstruction Method Based on Deep Learning
by Xin Chen, Houjin Chen, Yahui Peng, Liu Liu and Chang Huang
Electronics 2023, 12(7), 1527; https://doi.org/10.3390/electronics12071527 - 23 Mar 2023
Cited by 9 | Viewed by 6756
Abstract
In the medical field, 3D ultrasound reconstruction can visualize the internal structure of patients, which is very important for doctors to carry out correct analyses and diagnoses. Furthermore, medical 3D ultrasound images have been widely used in clinical disease diagnosis because they can [...] Read more.
In the medical field, 3D ultrasound reconstruction can visualize the internal structure of patients, which is very important for doctors to carry out correct analyses and diagnoses. Furthermore, medical 3D ultrasound images have been widely used in clinical disease diagnosis because they can more intuitively display the characteristics and spatial location information of the target. The traditional way to obtain 3D ultrasonic images is to use a 3D ultrasonic probe directly. Although freehand 3D ultrasound reconstruction is still in the research stage, a lot of research has recently been conducted on the freehand ultrasound reconstruction method based on wireless ultrasonic probe. In this paper, a wireless linear array probe is used to build a freehand acousto-optic positioning 3D ultrasonic imaging system. B-scan is considered the brightness scan. It is used for producing a 2D cross-section of the eye and its orbit. This system is used to collect and construct multiple 2D B-scans datasets for experiments. According to the experimental results, a freehand 3D ultrasonic reconstruction method based on depth learning is proposed, which is called sequence prediction reconstruction based on acoustic optical localization (SPRAO). SPRAO is an ultrasound reconstruction system which cannot be put into medical clinical use now. Compared with 3D reconstruction using a 3D ultrasound probe, SPRAO not only has a controllable scanning area, but also has a low cost. SPRAO solves some of the problems in the existing algorithms. Firstly, a 60 frames per second (FPS) B-scan sequence can be synthesized using a 12 FPS wireless ultrasonic probe through 2–3 acquisitions. It not only effectively reduces the requirement for the output frame rate of the ultrasonic probe, but also increases the moving speed of the wireless probe. Secondly, SPRAO analyzes the B-scans through speckle decorrelation to calibrate the acousto-optic auxiliary positioning information, while other algorithms have no solution to the cumulative error of the external auxiliary positioning device. Finally, long short-term memory (LSTM) is used to predict the spatial position and attitude of B-scans, and the calculation of pose deviation and speckle decorrelation is integrated into a 3D convolutional neural network (3DCNN). Prepare for real-time 3D reconstruction under the premise of accurate spatial pose of B-scans. At the end of this paper, SPRAO is compared with linear motion, IMU, speckle decorrelation, CNN and other methods. From the experimental results, it can be observed that the spatial pose deviation of B-scans output using SPRAO is the best of these methods. Full article
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13 pages, 4776 KiB  
Article
Direct Underwater Sound Velocity Measurement Based on the Acousto-Optic Self-Interference Effect between the Chirp Signal and the Optical Frequency Comb
by Zihui Yang, Fanpeng Dong, Hongguang Liu, Xiaoxia Yang, Zhiwei Li and Bin Xue
J. Mar. Sci. Eng. 2023, 11(1), 18; https://doi.org/10.3390/jmse11010018 - 23 Dec 2022
Cited by 2 | Viewed by 2479
Abstract
Underwater sound speed plays a vital role in maritime safety. Based on the acousto-optic self-interference effect, we proposed a new method to measure underwater sound speed utilizing Raman–Nath diffraction, generated by the acousto-optic effect between an optical frequency comb and pulsed chirp signal. [...] Read more.
Underwater sound speed plays a vital role in maritime safety. Based on the acousto-optic self-interference effect, we proposed a new method to measure underwater sound speed utilizing Raman–Nath diffraction, generated by the acousto-optic effect between an optical frequency comb and pulsed chirp signal. When the pulsed chirp travels between the measurement and reference arm in the experimental setup that we constructed, the same signal resulting from acousto-optic self-interference is produced. The time gap between the two identical signals represents the time interval. Thus, we can determine the time-of-flight using cross-correlation. The optical path difference between the two arms is double the flight distance of ultrasonic waves and can easily be obtained using femtosecond laser interferometry. The time gap and the distance can be used to measure sound speed. The experimental results show that the chirp signal improves the signal-to-noise ratio and expands the applicable time-of-flight algorithm. The waveform pulse width after cross-correlation is 1.5 μs, compared with 40 μs before. The time-of-flight uncertainty can achieve 1.03 ns compared to 8.6 ns before. Uncertainty of sound velocity can achieve 0.026 m/s. Full article
(This article belongs to the Special Issue Application of Advanced Technologies in Maritime Safety)
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11 pages, 3918 KiB  
Article
Acousto–Optic Modulation and Deflection of Terahertz Radiation
by Pavel Alekseevich Nikitin, Vasily Valerievich Gerasimov and Ildus Shevketovich Khasanov
Materials 2022, 15(24), 8836; https://doi.org/10.3390/ma15248836 - 10 Dec 2022
Cited by 4 | Viewed by 2135
Abstract
It is known that one of the ways to increase the energy efficiency of acousto–optic devices is to use ultrasound beams with a higher power density. It has been established experimentally that the use of a partially electroded ultrasonic transducer significantlyincreases the energy [...] Read more.
It is known that one of the ways to increase the energy efficiency of acousto–optic devices is to use ultrasound beams with a higher power density. It has been established experimentally that the use of a partially electroded ultrasonic transducer significantlyincreases the energy efficiency of the acousto–optic modulator of terahertz radiation. In addition, the operation of an acousto–optic deflector of terahertz radiation with the use of a sectioned ultrasound transducer was theoretically investigated. It showed that a deflector of this kind enables one to achieve higher angular resolution. Full article
(This article belongs to the Special Issue Acousto-Optical Spectral Technologies)
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12 pages, 4310 KiB  
Article
Phase Stability Control of Optical Fiber Partial Discharge Ultrasonic Sensing System
by Chao Xing, Qian Zang, Ruidong He, Jun Zhao, Lili Wang, Lujian Dai, Rongbin Shi, Sihan Wang and Guoming Ma
Sensors 2022, 22(21), 8495; https://doi.org/10.3390/s22218495 - 4 Nov 2022
Cited by 8 | Viewed by 2578
Abstract
Optic fiber interferometers are highly sensitive ultrasonic sensors for partial discharge detection. However, low-frequency vibration and environmental noise will disturb the sensors in the field, and cause a phase fading suppression effect that reduces sensitivity. This paper analyzed the problems existing in the [...] Read more.
Optic fiber interferometers are highly sensitive ultrasonic sensors for partial discharge detection. However, low-frequency vibration and environmental noise will disturb the sensors in the field, and cause a phase fading suppression effect that reduces sensitivity. This paper analyzed the problems existing in the phase feedback control system based on PZT, and an improved scheme incorporating a high-frequency carrier phase demodulation is proposed. Based on an acousto-optic modulator, the proposed phase feedback control system overcomes the phase fading suppression effect. A test is carried out on an ultrasonic calibration platform and a transformer oil discharge platform. The test results show that the stability of the improved phase demodulation system has been significantly improved, and meets the requirements of field applications. Compared with the signal-to-noise ratio at the time of phase fading of the system before the improvement, the signal-to-noise ratio of the improved system is improved by 69 dB. Full article
(This article belongs to the Special Issue Advanced Sensing Detection in Electrical Equipment)
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15 pages, 2940 KiB  
Article
Defects Detection and Identification in Adhesively Bonded Joints between CFRP Laminate and Reinforced Concrete Beam Using Acousto-Ultrasonic Technique
by Cheikh A. T. Sarr, Sylvain Chataigner, Laurent Gaillet and Nathalie Godin
J. Compos. Sci. 2022, 6(11), 334; https://doi.org/10.3390/jcs6110334 - 3 Nov 2022
Cited by 2 | Viewed by 1978
Abstract
Adhesively bonded composite reinforcements have been increasingly used in civil engineering since the 1980s. They depend on the effective transfer of forces throughout the adhesive joint that may be affected by defects or damages. It is therefore necessary to provide methods to detect [...] Read more.
Adhesively bonded composite reinforcements have been increasingly used in civil engineering since the 1980s. They depend on the effective transfer of forces throughout the adhesive joint that may be affected by defects or damages. It is therefore necessary to provide methods to detect and/or identify these defects present in the bonded joints without affecting their future use. This should be carried out through nondestructive methods (NDT) and should be able to discriminate the different types of defects that may be encountered. The acousto-ultrasonic technique shows good potential to answer to this challenge, as illustrated in recent studies led on small-scale model samples. In this paper, we assess the robustness of this methodology on larger scale samples using reinforced concrete beams (RC beam), that is a mandatory step prior to on-site applications. A mono-parametric analysis allows the detection of all types of defects using a simple criterion set. For the identification, it was necessary to conduct a data-driven strategy by means of a Principal Component Analysis (PCA) and a random forest (RF) method used from extracted parameters. Full article
(This article belongs to the Special Issue Feature Papers in Journal of Composites Science in 2022)
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8 pages, 1328 KiB  
Article
Frequency-Dependent Ultrasonic Stimulation of Poly(N-Isopropylacrylamide) Microgels in Water
by Atieh Razavi, Matthias Rutsch, Sonja Wismath, Mario Kupnik, Regine von Klitzing and Amin Rahimzadeh
Gels 2022, 8(10), 628; https://doi.org/10.3390/gels8100628 - 1 Oct 2022
Cited by 6 | Viewed by 2577
Abstract
As a novel stimulus, we use high-frequency ultrasonic waves to provide the required energy for breaking hydrogen bonds between Poly(N-isopropylacrylamide) (PNIPAM) and water molecules while the solution temperature is maintained below the volume phase transition temperature (VPTT = 32 °C). Ultrasonic waves propagate [...] Read more.
As a novel stimulus, we use high-frequency ultrasonic waves to provide the required energy for breaking hydrogen bonds between Poly(N-isopropylacrylamide) (PNIPAM) and water molecules while the solution temperature is maintained below the volume phase transition temperature (VPTT = 32 °C). Ultrasonic waves propagate through the solution and their energy will be absorbed due to the liquid viscosity. The absorbed energy partially leads to the generation of a streaming flow and the rest will be spent to break the hydrogen bonds. Therefore, the microgels collapse and become insoluble in water and agglomerate, resulting in solution turbidity. We use turbidity to quantify the ultrasound energy absorption and show that the acousto-response of PNIPAM microgels is a temporal phenomenon that depends on the duration of the actuation. Increasing the solution concentration leads to a faster turbidity evolution. Furthermore, an increase in ultrasound frequency leads to an increase in the breakage of more hydrogen bonds within a certain time and thus faster turbidity evolution. This is due to the increase in ultrasound energy absorption by liquids at higher frequencies. Full article
(This article belongs to the Special Issue Thermoresponsive Microgels)
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17 pages, 1810 KiB  
Article
Interpolation of Pathway Based Non-Destructive Testing (NDT) Data for Defect Detection and Localization in Pre-Baked Carbon Anodes
by Daniel Rodrigues, Carl Duchesne and Julien Lauzon-Gauthier
Metals 2022, 12(9), 1411; https://doi.org/10.3390/met12091411 - 26 Aug 2022
Cited by 1 | Viewed by 1696
Abstract
Producing consistent quality pre-baked carbon anodes for the Hall–Héroult aluminum reduction process is challenging due to the decreasing quality and increasing variability of anode raw materials. Non-destructive testing techniques (NDT) have been developed and recently implemented in manufacturing plants to establish better suited [...] Read more.
Producing consistent quality pre-baked carbon anodes for the Hall–Héroult aluminum reduction process is challenging due to the decreasing quality and increasing variability of anode raw materials. Non-destructive testing techniques (NDT) have been developed and recently implemented in manufacturing plants to establish better suited and more efficient quality control schemes than core sampling and characterization. These technologies collect measurements representing effective properties of the materials located along a pathway between two transducers (emitter and receiver), and not spatially-resolved distribution of properties within the anode volume. A method to interpolate pathway-based measurements and provide spatially-resolved distribution of properties is proposed in this work to help NDT technologies achieve their full potential. The interpolation method is tested by simulating acousto-ultrasonic data collected from a large number of 2D and 3D toy examples representing simplified anode internal structures involving randomly generated defects. Experimental validation was performed by characterizing core samples extracted from a set of industrial anodes and correlating their properties with interpolated speed of sound by the algorithm. The method is shown to be successful in determining the defect positions, and the interpolated results are shown to correlate significantly with mechanical properties. Full article
(This article belongs to the Special Issue Production of Quality Anodes in Aluminum Industry)
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