Search Results (462)

This study aims to determine the optimal low-temperature stress relieving heat treatment that minimizes residual stresses while preserving corrosion resistance in Laser Powder Bed Fusion (L-PBF) processed Ti6Al4V alloy. Specifically, it investigates the effects of stress relieving at 400 °C, 600 °C, and 800 °C on microstructure, residual stress, and electrochemical performance. Specimens were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), and electrochemical techniques. A novel microcapillary electrochemical method was employed to precisely assess passive layer stability and corrosion behaviour under simulated oral conditions, including fluoride contamination and tensile loading. Results show that heat treatments up to 600 °C effectively reduce residual stress with minimal impact on corrosion resistance. However, 800 °C treatment leads to a phase transformation from α′ martensite to a dual-phase α + β structure, significantly compromising passive film integrity. The findings establish 600 °C as the optimal stress-relieving temperature for balancing mechanical stability and electrochemical performance in biomedical and aerospace components. Full article

The manufacture of lightweight components is one of the most important requirements in the automotive and aerospace industries. Gears, on the other hand, are among the heaviest parts in terms of their total weight. Accordingly, a spur gear was considered, the body of which was configured as a lattice structure to make it lightweight. In addition, the structure was optimized by topology optimization using ProTOP software. Subsequently, the gear was manufactured by a selective laser melting process by using a strong and lightweight material, namely Ti-6Al-4V. This study defeated the problems of manufacturing orientation, surface roughness, support structure, and bending due to the high thermal gradient in the selective laser melting process. To experimentally investigate the benefits of such a lightweight gear body structure, a new test rig with a closed loop was developed. This rig enabled measurements of strains in the gear ring, hub, and tooth root. The experimental results confirmed that a specifically designed and selectively laser-melted, lightweight cellular lattice structure in the gear body can significantly influence strain. This is especially significant with respect to strain levels and their time-dependent variations in the hub section of the gear body. Full article

This work presents a multiscale, microstructure-aware framework for predicting fatigue strength distributions in additively manufactured (AM) alloys—specifically, laser powder bed fusion (L-PBF) AlSi10Mg and Ti-6Al-4V—by integrating density functional theory (DFT), instrumented indentation, and Bayesian inference. The methodology leverages principles common to all 3D printing (additive manufacturing) processes: layer-wise material deposition, process-induced defect formation (such as porosity and residual stress), and microstructural tailoring through parameter control, which collectively differentiate AM from conventional manufacturing. By linking DFT-derived cohesive energies with indentation-based modulus measurements and a MAP-based statistical model, we quantify the effect of additive-manufactured microstructural heterogeneity on fatigue performance. Quantitative validation demonstrates that the predicted fatigue strength distributions agree with experimental high-cycle and very-high-cycle fatigue (HCF/VHCF) data, with posterior modes and 95 % credible intervals of ${\widehat{\sigma }}_f^{\mathrm{AlSi}10\mathrm{Mg}}={86}_{-7}^{+8}\mathrm{MPa}$ and ${\widehat{\sigma }}_f^{\mathrm{Ti}–6\mathrm{Al}–4\mathrm{V}}={115}_{-9}^{+10}\mathrm{MPa}$, respectively. The resulting Woehler (S–N) curves and Paris crack-growth parameters envelop more than 92 % of the measured coupon data, confirming both accuracy and robustness. Furthermore, global sensitivity analysis reveals that volumetric porosity and residual stress account for over 70 % of the fatigue strength variance, highlighting the central role of process–structure relationships unique to AM. The presented framework thus provides a predictive, physically interpretable, and data-efficient pathway for microstructure-informed fatigue design in additively manufactured metals, and is readily extensible to other AM alloys and process variants. Full article

In this study, we delve into the intricate microstructural features of Ti-6Al-4V alloy additively manufactured and heat-treated at 800 °C for 4 h. Our in-depth analysis will enable us to gain a better understanding of the β-Ti precipitation process, its dependence on temperature, and its ultimate effect on the overall mechanical properties. As well as α-Ti martensite grains and β-Ti particles interspersed in the α-Ti grain boundaries, there is a third microstructural feature, overlooked by many researchers. This feature is observed as nano-sized particles homogeneously embedded inside the α-Ti laths. Using high-resolution transmission electron microscopy, we reveal that these nano-sized features do not constitute a different phase. Instead, they define isolated regions of α-Ti in its relaxed form, surrounded by the heavily strained form of the α-Ti phase. This phenomenon is a result of the “incomplete” precipitation of the β-Ti phase following the heat treatment stage. The straining of the α-Ti phase appears as a shift in the equilibrium atomic position. Full article

The purpose of this study was to estimate the peak stresses in a laser powder bed fusion (LPBF) additive-manufactured (AM) osteosynthesis plate during physiological loading and establish if the mechanical properties of LPBF titanium alloy were suitable for this use case. Finite element models of subject-specific osteosynthesis plates for a cohort of 28 patients were created and used to calculate the peak maximum principal stresses during physiological loading, which was estimated to be 166 MPa twelve weeks post-operatively. All specimens were LPBF additively manufactured in Ti-6Al-4V alloy. ISO compliant tests were performed for tensile and fatigue, respectively. Fatigue testing was performed for specimens that had been heat-treated only and those that had been heat-treated and polished. The Upper Yield Stress was 1012.5 ± 19.2 MPa. The fatigue limit was 227 MPa for heat-treated only specimens and increased to 286 MPa for heat-treated and polished specimens. The finite element predicted stresses were below the experimentally established limits of yield and fatigue. The tensile and fatigue properties of heat-treated LPBF Ti-6Al-4V are therefore sufficient to meet the mechanical requirements of osteosynthesis plates. Polishing is recommended to improve fatigue resistance. Full article

Laser powder-bed fusion (L-PBF) additive manufacturing has been widely explored for fabricating intricate metallic parts such as lattice structures with thin struts. However, L-PBF-fabricated small parts (e.g., thin struts) exhibit different morphological and mechanical characteristics compared to bulk-sized parts due to distinct scan lengths, affecting the melt pool behavior between transient and quasi-steady states. This study investigates the keyhole porosity in Ti6Al4V thin struts fabricated by L-PBF, incorporating a range of strut sizes, along with various levels of linear energy densities. Micro-scaled computed tomography and image analysis were employed for porosity measurements and evaluations. Generally, keyhole porosity lessens with decreasing energy density, though with varying patterns across a higher energy density range. Keyhole porosity in struts predictably becomes severe at high laser powers and/or low scan speeds. However, a major finding reveals that the porosity is reduced with decreasing strut size (if less than 1.25 mm diameter), plausibly because the keyhole formed has not reached a stable state to produce pores in a permanent way. This implies that a higher linear energy density, greater than commonly formulated in making bulk components, could be utilized in making small-scale features to ensure not only full melting but also minimum keyhole porosity. Full article

Titanium alloys, especially Ti6Al4V, are widely used in biomedical implants due to their biocompatibility and mechanical strength. However, their high elastic modulus (>100 GPa), compared to that of human bone (10–30 GPa), often causes stress shielding, reducing implant lifespan. To address this, titanium alloys with lower elastic modulus are under development. In this study, Ti-based multi-element alloy with 16 wt.% Nb samples were fabricated using laser powder bed fusion (L-PBF) from a premixed powder blend of Ti6Al4V and Nb-Hf-Ti. Processing high-melting Nb-based alloys via L-PBF poses challenges, which were mitigated through optimized parameters, including a maximum laser power of 100 W. Eleven parameter sets were employed to evaluate printability, microstructure, and mechanical properties. Microstructural analysis revealed Widmanstätten structures composed of α and β phases, along with isolated spherical pores. Reduced hatch spacing and slower laser speed led to increased hardness. The highest hardness (~43 HRC) was observed at the highest energy density (266 J/mm³), while the lowest (~28 HRC) corresponded to 44 J/mm³. Elastic modulus values ranged from 30 to 35 GPa, closely matching that of bone. These results demonstrate the potential of the developed Ti-based alloy containing 16 wt.% Nb as a promising candidate for load-bearing biomedical implants. Full article

Lattice structures offer the possibility to obtain lightweight components with additional functionalities, improving their shock absorption and thermal exchange properties. Recently, a body-centered cubic (BCC) lattice structure has been used to fabricate metal lattice sandwich panels (MLSPs) for aerospace applications. MLSPs are made of two external skins and a lattice core and can be produced thanks to laser powder bed fusion technology (LPBF), which is characterized by its superior printing accuracy with respect to other additive manufacturing processes for metals. Since few studies can be found in the literature on Ti-6Al-4V MLSPs, further work is needed to evaluate the mechanical response of these panels. Moreover, due to their design complexity and to avoid a costly experimental campaign, numerical simulation could be used to encourage the industrial application of these structures. In this paper, different cell configurations were printed and tested in compression to study the influence of the cell’s geometrical parameters, i.e., the cell size and beam radius, on the mechanical response of MLSPs. Numerical simulations of the LPBF of these geometries were also carried out to understand how the residual stresses can be varied by varying the cell configuration. A geometrical evaluation was carried out to quantitatively express the influence of the beam radius and cell size on the resulting volume fraction, which strongly influences the mechanical behavior and residual stress profiles of MLSPs. From the analysis, we found that the C2-R0.35 sample resulted in the configuration with the highest compressive strength, while C3-R0.25 showed the lowest and most uniform residual stress profile. Full article

MIL-STD-1530D and the United States Air Force (USAF) Structures Bulletin EZ-SB-19-01 require an ability to predict the growth of naturally occurring three-dimensional cracks with crack depths equal to what they term an equivalent initial damage size (EIDS) of 0.254 mm. This requirement holds for both additively manufactured and conventionally built parts. The authors have previously presented examples of how to perform such predictions for additively manufactured (AM) Ti-6Al-4V; wire arc additively manufactured (WAAM) 18Ni 250 Maraging steel; and Boeing Space, Intelligence and Weapon Systems laser bed powder fusion (LPBF) Scalmalloy^®, which is an additively manufactured Aluminium-Scandium-Mg alloy, using the Hartman-Schijve crack growth equation. In these studies, the constants used were as determined from ASTM E647 standard tests on long cracks, and the fatigue threshold term in the Hartman-Schijve equation was set to a small value (namely, 0.1 MPa √m). This paper illustrates how this approach can also be used to predict the growth of naturally occurring three-dimensional cracks in WAAM CP-Ti (commercially pure titanium) specimens built by Solvus Global as well as in WAAM-built Inconel 718. As in the prior studies mentioned above, the constants used in this analysis were taken from prior studies into the growth of long cracks in conventionally manufactured CP-Ti and in AM Inconel 718, and the fatigue threshold term in these analyses was set to 0.1 MPa √m. These studies are complemented via a prediction of the growth of naturally occurring three-dimensional cracks in conventionally built M300 steel. Full article

Bone diseases lead to an increasing demand for implants to treat long bone defects and for load-bearing applications. Osteoporosis care and accidental injuries are major contributors to this rising need. Our research aims to demonstrate innovative material systems and methods for preparing implants that can be used in regenerative medicine. We hypothesize that by combining titanium alloys (Ti6Al4V) with hydroxyapatite (Hap), we can enhance biocompatibility and tribo-mechanical performance, which are critical for the longevity of Ti-based surgical implants. Additionally, we investigate the application of laser surface treatments to expose the underlying porosity, thereby enhancing cell transport and promoting cell growth. In this study, we investigate the effects of two fabrication techniques—Spark Plasma Sintering (SPS) and powder metallurgy (PM)—on the properties of laser-textured Ti64/Hap biocomposites. Our findings demonstrate that the selected processing route significantly influences the microstructure, tribological performance, and surface properties of these materials. An X-ray diffraction (XRD) analysis corroborates our results from incubation studies in simulated body fluids, highlighting the impact of phase transformations during sintering on the chemical properties of Ti-Hap composites. Additionally, while laser surface texturing was found to slightly increase the friction coefficient, it markedly enhanced the wear resistance, particularly for the PM and SPS Ti + 5%Hap composites. Full article

One of the most popular alloys for biomedical applications is TiAl6V4. Even though TiAl6V4 is widely used, it faces several challenges. Firstly, TiAl6V4 is prone to stress shielding caused by the difference in Young’s moduli of the alloy (110 GPa) and human bones (20–30 GPa). Secondly, there is the presence of cytotoxic elements, aluminum and vanadium. Researchers have proposed Ti-35Nb-7Zr-5Ta (TNZT) alloy to overcome these disadvantages, an excellent substitute for natural human bones. This alloy offers a lower elastic modulus (up to 81 GPa), much closer to human bones than TiAl6V4 alloy. Also, TNZT alloy contains no cytotoxic elements and has excellent biocompatibility and high corrosion resistance. Given the positive outcomes on powder-mixed micro electro-discharge machining (PM-μ-EDM) of Ti alloy using hydroxyapatite (HA) powder, we studied the machinability of TNZT alloy using HA powder mixed-μ-EDM by changing the HA powder concentration (0, 5, and 10 g/L), gap voltage (90, 100, and 110 V), and capacitance (10, 100, and 400 nF) according to the Taguchi L9 method. Machining performance metrics such as material removal rate (MRR), overcut, and circularity were examined using a tungsten carbide tool of 237 µm diameter. The results showed an overcut of 10.33 µm, circularity of 8.47 µm, and MRR of 6030.89 µm³/s for the lowest energy setup. Full article

The melt track overlap rate is a crucial process parameter in selective laser melting (SLM). It exerts a substantial influence on the forming quality of Ti-6Al-4V alloy. This paper investigates the impact of different melt track overlap rates on the quality of Ti-6Al-4V samples formed by SLM through a combination of simulation and experimentation. The findings reveal that if the overlap rate is overly small (<14.3%), the powder at the bottom of the overlap zone cannot be fully melted, thereby forming pores. Additionally, the densification effect causes the actual powder spreading thickness to be greater than the theoretical one. Consequently, when the overlap rate is less than 20%, it is challenging to ensure a close bond between the upper and lower melt tracks. Both the simulation and experimental results demonstrate that an excessive melt track overlap rate will lead to grain growth in the overlap zone and reduce the tensile properties of the sample. Thus, both excessive and insufficient overlap rates are detrimental to the density and mechanical properties of the formed sample. The multi-layer and multi-track model established in this study effectively replicates the actual processing conditions. The retention of the temperature field of the first layer makes the simulation of the melt tracks of the second layer more realistic and reliable. This provides a reference basis for accurately predicting the forming quality of SLM using numerical models in the future. Full article

To address the insufficient bonding performance between TC4 (Ti-6Al-4V) coating and carbon fiber-reinforced thermoplastic (CFRP) matrices that limits engineering applications of composite structures, TC4 coatings were fabricated on CFRP polymer composites via laser cladding and analyzed using scanning electron microscopy (SEM) and transmission electron microscopy (TEM) to examine the interface morphology, microstructure, and phase composition. The influence of laser processing parameters on the cladding quality was assessed based on the mechanical performance of the TC4 coating. The findings revealed that insufficient laser power (<230 W) or excessive scanning speed (>1.4 m/min) led to incomplete melting of TC4 powder, preventing the formation of intermetallic compound (IMC) layers. Conversely, excessive laser power (>270 W) or a low scanning speed (<1.0 m/min) caused thermal decomposition of the CFRP due to its limited thermal resistance, leading to interfacial defects such as cracks and pores. The interface between the CFRP and TC4 coating primarily comprised granular TiC and acicular α′ martensite, with minor TiS₂ detected. Optimal mechanical performance was achieved at a laser power of 250 W and a scanning speed of 1.2 m/min, yielding a maximum interfacial shear strength of 18.5 MPa. These findings provide critical insights for enhancing the load-bearing capacity of TC4/CFRP aeronautical composites, enabling their reliable operation in extreme aerospace environments. Full article

Laser powder bed fusion (L-PBF) has become a highly viable method for manufacturing metal structural components for a variety of industries. Despite many attractive qualities, the rough surfaces of L-PBF components often necessitates post-processing treatments to improve the surface finish. Furthermore, heat treatments are generally necessary to control the microstructure and properties of L-PBF components, which can impart a detrimental surface oxide layer that requires removal. In this investigation, cavitation abrasive surface finishing (CASF) was adopted for the surface treatment of Ti6Al4V components produced by L-PBF and removal of the surface oxide layer. The surface texture, residual stress, and material removal were evaluated over a range of treatment conditions and as a function of the target surface orientation. Results showed that CASF reduced the average surface roughness from the as-built condition (R_a ≈ 15 µm) to below 5 µm as well as imparted a surface compressive residual stress of up to 600 MPa. The CASF treatment removed the alpha case from direct line-of-sight surfaces under a range of treatment intensity. However, deep valleys and surfaces at large oblique angles of incidence (≥60°) proved challenging to treat uniformly. Overall, results suggest that CASF could serve as a potent alternative to chemical treatments for post-processing of L-PBF components of titanium and other metals. Further investigation is recommended for improving the process effectiveness and to characterize the fatigue performance of the treated metal. Full article

Ti6Al4V is widely utilized in orthopedic implants due to its excellent mechanical properties, corrosion resistance, and biocompatibility. However, traditional solid titanium implants exhibit an elastic modulus (90–115 GPa) significantly higher than that of human bone (10–30 GPa), leading to stress shielding and implant loosening. To address this, porous titanium alloys have been developed to better match bone elasticity. Additive manufacturing, particularly selective laser melting (SLM), enables precise control over pore size and porosity, thereby tuning mechanical properties. Nevertheless, SLM-produced porous structures often suffer from powder adhesion, which compromises bone integration and patient safety. In this study, bulk Ti6Al4V samples were fabricated via SLM with a fixed laser power of 200 W and varying scanning speeds (800–1400 mm/s). Density measurements and surface defect analysis identified 1200 mm/s as the optimal scanning speed. Cubic unit cell scaffolds with different pore diameters (400, 600, 800 μm) and porosities (60%, 80%) were subsequently designed. Compression tests revealed that scaffolds with a 400 μm pore diameter and 60% porosity exhibited the highest compressive strength (794 MPa) and fracture strain (41.35%). Chemical polishing using a diluted HF-HNO₃ solution (1:2:97) effectively removed adhered powder without significant structural degradation, with 40 min identified as the optimal polishing duration. Full article