Flame-generated soot particles from two different fuels, benzene (B) and ethylene (E), at different ageing conditions, were analysed to assess their morphological and structural features. Samples were collected at 6, 10 and 14 mm from the nozzle loca...
Even though sub-micron and nano-sized iron particles generally display single or polycrystalline structures, a growing interest has also been dedicated to the class of amorphous ones, whose absence of a crystal structure is capable of modifying their...
The borehole transient electromagnetic (TEM) method can be useful in deep mineral exploration to detect blind ore bodies beside or below the borehole, and is especially adapted to finding small-scale, deep, rich ore bodies. In this method a transmitt...
Materials produced through equal channel angular extrusion (ECAE) may offer enhanced mechanical properties over classic thermomechanical processing like extrusion or rolling. Conventional techniques such as electron backscatter diffraction (EBSD) may...
Hydride artefacts are commonly induced by the TEM sample preparation process in Zirconium alloys as hydrogen-sensitive metals, including electron polishing and focused ion beam (FIB) technology. In the research, we present the application of chemical...
This work highlights some limitations of thermal stability analysis via in-situ transmission electron microscopy (TEM)-annealing experiments on ultrafine and nanocrystalline materials. We provide two examples, one on nanocrystalline pure copper and o...
The induced polarization (IP) effects in transient electromagnetic (TEM) responses pose difficulties to the TEM data interpretation and inversion. The IP effects break the monotony in TEM decay curves and can even cause sign reversals and lead to the...
1C1m-Fc, an anti-tumor endothelial marker 1 (TEM-1) scFv-Fc fusion protein antibody, was previously successfully radiolabeled with 177Lu. TEM-1 specific tumor uptake was observed together with a non-saturation dependent liver uptake that could be rel...
Transmission electron microscopy (TEM) is a highly effective method for scientific research, providing comprehensive analysis and characterization. However, traditional TEM is limited to observing static material structures at room temperature within...
Due to their rapid evolution and their impact on healthcare, beta-lactamases, protein degrading beta-lactam antibiotics, are used as generic models of protein evolution. Therefore, we investigated the mutation effects in two distant beta-lactamases,...
Induced polarization (IP) effects in transient electromagnetic (TEM) measurement play a significant role in the detection of minerals, such as sulfide ore, clay ore, etc. However, due to the complex impacts caused by the polarization parameters, the...
In this work, the nanostructure of oxide dispersion-strengthened steels was studied by small-angle neutron scattering (SANS), transmission electron microscopy (TEM), and atom probe tomography (APT). The steels under study have different alloying syst...
Carbon-based materials are widely applied in various devices due to their outstanding mechanical and tribological behaviors. In recent years, more attention has been paid to clarifying the nanocontact mechanisms of carbon-based materials, in order to...
In this manuscript, we report the application of graphene oxide (GO) in the preparation of cryo-electron microscopy (cryo-EM) and transmission electron microscopy (TEM) grids. We treated GO with water and organic solvents, such as, methanol, ethanol...
Ni-SiOC nanocomposites maintain crystal-amorphous dual-phase nanostructures after high-temperature annealing at different temperatures (600 °C, 800 °C and 1000 °C), while the feature sizes of crystal Ni and amorphous SiOC increase with th...
Steel infrastructure in tunnels significantly affects the accuracy of transient electromagnetic (TEM) data inversion. This study proposes and compares two methods to effectively mitigate this interference: the correction factor method and the prior i...
For decades, differentially pumped environmental transmission electron microscopy has been a powerful tool to study dynamic structural evolution of catalysts under a gaseous environment. With the advancement of micro-electromechanical system-based te...
Materials designed for nuclear reactors undergo microstructural changes resulting from a combination of several environmental factors, including neutron irradiation damage, gas accumulation and elevated temperatures. Typical ion beam irradiation expe...
Wire electrical discharge machining is an unconventional machining technology that is crucial in many industries. The surface quality of the machined parts is carefully monitored, but the condition of the subsurface layer also plays a crucial role, e...
Bacterial resistance to β-lactams, the most commonly used class of antibiotics, poses a global challenge. This resistance is caused by the production of bacterial enzymes that are termed β-lactamases (βLs). The evolution of serine-clas...
Serine β-lactamase TEM-1 is the first β-lactamase discovered and is still common in Gram-negative pathogens resistant to β-lactam antibiotics. It hydrolyzes penicillins and cephalosporins of early generations. Some of the emerging TEM-...
One of the main factors in the deterioration of automobile three-way catalysts is the sintering of platinum group metals (PGMs). In this study, we used in situ tunneling electron microscopy (TEM) to examine the sintering of Rh particles as the temper...
In the field of material micro-/nano-analysis, the lack of an efficient method for characterizing the same microregion has been an obstacle in scientific research. This not only severely affects the efficiency and depth of academic communication, but...
Amorphous alloys or metallic glasses (MGs) thin films have attracted extensive attention in various fields due to their unique functional properties. Here, we use in situ heating transmission electron microscopy (TEM) to investigate the thermal stabi...
The Qingchengzi orefield is an important polymetallic ore concentration zone in the northern margin of the North China Craton (NCC). The region has significant metallogenic potential for deep mining. Many areas with gold mineralization have been foun...
We used in situ transmission electron microscopy (TEM) to observe the dynamic changes of Si nanowires under electron beam irradiation. We found evidence of structural evolutions under TEM observation due to a combination of electron beam and thermal...
Titanium dioxide (TiO2) nanoparticles (NPs) are the subject of numerous studies and controversies on the risks they could pose to the environment and human health. When in contact with biological tissues, NPs can sometimes be challenging to precisely...
An air-coil sensor (ACS) is a type of induction magnetometer used as a transducer to measure the variations of a magnetic field. This device is widely applied in helicopter transient electromagnetic method (TEM) exploration. Most helicopter TEM explo...
Monazite ((Ce, La, Nd, Th)PO4) is one of the widely used minerals for U–Th–Pb dating in geochronology. To better understand the possible effects of radiogenic Pb on the in situ dating method, a natural monazite U–Th–Pb standar...
Nano-drugs based on nanoparticles (NP) or on nano-assemblies as carriers of the active pharmaceutical ingredient (API) are often expected to perform better compared to conventional dosage forms. Maximum realization of this potential though requires o...
In ceramic thin films, choosing an appropriate sample preparation method for transmission electron microscopy (TEM) analyses is of paramount importance to avoid preparation-induced damage and retain nanoscale features that require investigation. Here...
In our previous studies, we have developed a wet process to synthesize a copper-single walled carbon nanotube (Cu–SWCNT) metal nanocomposite with excellent mechanical properties. The nanostructure of this Cu–SWCNT composite was confirmed independentl...
The article presents the results of transient electromagnetic (TEM) prospecting surveys using an unmanned aerial system carried out at Lake Baikal, which is a unique geoelectrical setting where low-resistivity lacustrine sediments are located under a...
In this paper, we report the study of the low-voltage locally enhanced electric field treatment (LEEFT) of E. coli bacteria via TEM analysis and FT-IR and Raman spectrometry. The formation of pores was confirmed by TEM, which revealed the membrane ru...
High-resolution TEM (HRTEM) is a powerful tool for structure characterization. However, methylammonium lead iodide (MAPbI3) perovskite is highly sensitive to electron beams and easily decomposes into lead iodide (PbI2). Misidentifications, such as Pb...
A robust design of a 3D-printed 6–18 GHz double-ridged TEM horn antenna is proposed in this paper. The designed TEM horn antenna has two parts: an adaptor and a horn aperture. The adaptor is realized using a double-ridged waveguide to extend the oper...
In a previous study, using high-resolution transmission electron microscopy (HRTEM), we examined grain-boundary migration behavior in a Ni bicrystal. A specimen for transmission electron microscopy (TEM) was prepared using focused ion beam. The Ni la...
Geological contexts that lack minimal stratigraphic and piezometric information can be challenging to produce an initial hydrogeological map in remote territories. This study proposes an approach to characterize a regional aquifer using transient ele...
We performed in-situ transmission electron microscopy (TEM) on a dealloyed nanoporous NiCo catalyst used for the dry reforming of methane (DRM) to investigate the origin of the catalytic activity and structural durability. The in-situ observations an...
Background: Antimicrobial resistance (AMR) among Gram-negative pathogens, predominantly ESBL-producing clinical isolates, are increasing worldwide. The main aim of this study was to determine the prevalence of ESBL-producing clinical isolates, their...
We demonstrate for the first time the structure identification and narrow-bandgap property of 1D hybridized SnO/SnO2 nanoparticles derived from the calcination of a single-source precursor, i.e., tin(II) oxalate. Systematic Raman analysis together wi...
We present a versatile method for synthesizing high-quality molybdenum disulfide (MoS2) crystals on graphite foil edges via chemical vapor deposition (CVD). This results in MoS2/graphene heterostructures with precise epitaxial layers and no rotationa...
The fields of catalysis and energy storage nowadays quote the use of nanomaterials with well-defined size, morphology, chemical composition, and thermal stability in the high-temperature range and under harsh conditions of reactions. We present herei...
Matrix-related pores play a significant role in controlling hydrocarbon production in organic-rich shales. Multiple matrix-related pore types of typical marine shales in the Sichuan Basin have been visually investigated and identified by transmission...
We report on cooperative grain rotation accompanied by a strong Bauschinger effect in nanocrystalline (nc) palladium thin film. A thin film of nc Pd was subjected to cyclic loading–unloading using in situ TEM nanomechanics, and the evolving microstru...
In this paper, a dual-band metamaterial absorber (MMA) ring with a mirror reflexed C-shape is introduced for X and Ku band sensing applications. The proposed metamaterial consists of two square ring resonators and a mirror reflexed C-shape, which rev...
Block copolymer (BCP) self-assembly is a promising tool for next generation lithography as microphase separated polymer domains in thin films can act as templates for surface nanopatterning with sub-20 nm features. The replicated patterns can, howeve...
Seawater intrusion into near-shore aquifers is one of the main environmental problems that affect Mediterranean islands. Crete is the biggest and most populated island of Greece, characterized by limited surface waters and strong dependence on ground...
The effect of simultaneous introduction of Hf and Pt into aluminide coating deposited on Inconel 625 alloy was investigated using scanning and transmission electron microscopy (SEM/TEM) methods. The coating consisted of two layers: the additive and t...
The air-core coil sensor (ACS) is widely used as a transducer to measure the variation in magnetic fields of a helicopter transient electromagnetic (TEM) system. A high periodic emitting current induces the magnetic field signal of the underground me...
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