Search Results (67)

This paper proposes a mathematical description of nitriding atmospheres obtained from a one-component ammonia ingoing atmosphere and a two-component ammonia inlet nitrogen-diluted atmosphere. The Fe-N phase equilibrium diagrams of the nitriding atmosphere in the hydrogen content-temperature (Q-T) system for selected NH₃/N₂ atmosphere compositions are presented. The nitriding atmosphere obtained with different degrees of nitrogen dilution of the ingoing atmosphere was characterized. It has been shown that in processes carried out in nitriding atmospheres obtained from a two-component atmosphere with nitrogen, there is no direct relationship between the value of the nitrogen potential and the degree of dilution of the ingoing atmosphere with nitrogen. It has been shown analytically and confirmed experimentally that with changes in the degree of dilution of ammonia with nitrogen, the hydrogen content of the nitriding atmosphere and, consequently, the nitrogen availability of the nitriding atmosphere change. Using the example of nitriding AISI 52100 steel, it has been experimentally demonstrated that the change in nitrogen availability, caused by a change in the degree of dilution of the ingoing atmosphere with nitrogen, is not accompanied by a change in the value of the nitrogen potential. It has also been shown that the change in the nitrogen availability of the nitriding atmosphere, induced by the change in the composition of the aNH₃/bN₂ ingoing atmosphere, affects the kinetics of nitrogen mass gain in the nitrided layer and the distribution of nitrogen mass between the iron nitride layer and the solution zone. It has also been shown that with the change in nitrogen availability, what changes in addition to the thickness of the iron nitride layer is also the phase composition of the layer. Using gravimetric tests, the mass of nitrogen in the iron nitride layer and the solution zone has been determined. To describe the equilibrium between the NH₃/H₂ atmosphere and nitrogen in the different iron phases, a modified Lehrer diagram in the coordinate system of temperature and hydrogen content in the nitriding atmospheres (T-Q) has been proposed. Full article

This paper describes a simulation study on the hard turning of AISI 52100 alloy steel with coated carbide tools under minimal cutting fluid conditions using the commercial software AdvantEdge. A finite element analysis coupled with adaptive meshing was carried out to accurately capture temperature gradients. To minimise the number of experiments while optimising the cutting parameters along with fluid application parameters, a cutting speed (v) of 80 m/min, feed rate (f) of 0.05 mm/rev, depth of cut (d) of 0.15 mm, nozzle stand-off distance (NSD) of 20 mm, jet angle (JA) of 30°, and jet velocity (JV) of 50 m/s were observed to be the optimal process parameters based on the combined response’s signal-to-noise ratios. The effects of each parameter on machined surface temperature, cutting force, cutting temperature, and tool–chip contact length were determined using ANOVA. The depth of cut affected cutting force, while cutting speed and jet velocity affected cutting temperature and tool–chip contact length. Cutting speed influenced machined surface temperature significantly, whereas other parameters showed minimal effect. Nozzle stand-off distance exhibited less significant effect. Taguchi optimisation determined the optimal combination of process parameters for minimising thermal effects during hard turning. Cutting temperature and cutting force simulation results were found to be highly consistent with experimental results. On the other hand, the simulated results for the tool–chip contact length and machined surface temperature were very close to the values found in the literature. The result validated the finite element model’s ability to accurately simulate thermal behaviour during hard-turning operations. Full article

Hard turning is a precision machining process used in the manufacturing industry for the finishing of hardened alloy steel, which is known for its high hardness and wear resistance. In this work, an experimental investigation was conducted to predict surface roughness and cutting temperature during the hard turning of AISI 52100 steel using the minimal cutting fluid application (MCFA). The MCFA is a sustainable high-velocity pulsed jet technique that has emerged as an eco-friendly approach for reducing the environmental impact and improving surface integrity in machining processes. The influence of key machining parameters, such as cutting speed, feed rate, and depth of cut, on the performance indicators was modeled using the response surface methodology (RSM) and the artificial neural network (ANN). The RSM was employed for a structured, statistical analysis, while an ANN provided a data-driven approach for capturing complex non-linear relationships. Various network architectures were established and evaluated with a fixed number of cycles. Results showed that the ANN exhibited superior accuracy in predicting both responses. In comparison to the QR model, the ANN exhibited the lowest average error rate in accurately predicting the response. This was further validated through experimental trials, demonstrating that the ANN consistently outperformed the RSM across different parameter settings. Additionally, the use of the MCFA contributed to sustainable manufacturing by minimizing the use of cutting fluids while maintaining machining quality. Full article

This paper analyzes the surface quality characteristics, such as arithmetic average roughness (Ra), maximum peak-to-valley height (Rt), and average peak-to-valley height (Rz), in hard turning of AISI 52100 steel using a (TiN/TiCN/Al₂O₃) coated carbide insert under a minimal cutting fluid environment (MCFA). MCFA, a sustainable high-velocity pulsed jet technique, reduces harmful effects on human health and the environment while improving machining performance. Taguchi’s L27 orthogonal array was used to conduct the experiments. The findings showed that surface roughness increases with feed rate, identified as the most influential parameter, while the depth of cut shows a negligible effect. The main effects plot of signal-to-noise (S/N) ratios for the combined response of Ra, Rt, and Rz revealed the optimal cutting conditions: cutting speed of 140 m/min, feed rate of 0.05 mm/rev, and depth of cut of 0.3 mm. Feed rate ranked highest in influence, followed by cutting speed and depth of cut. The lower values of surface roughness parameters were observed in the ranges of Ra ≈ 0.248–0.309 µm, Rt ≈ 2.013–2.186 µm, and Rz ≈ 1.566 µm at a feed rate of 0.05–0.07 mm/rev. MCFA-assisted hard turning reduces surface roughness by 35–40% compared to dry hard turning and 10% to 24% when compared to the MQL technique. Moreover, this study emphasizes the significant environmental benefits of MCFA, as it incorporates minimal eco-friendly cutting fluids that minimize ecological impact while enhancing surface finish. Full article

High-strength nickel–chromium steel (20Cr2Ni4A) is typically used in bearing applications. Alternating magnetic field treatment, which is based on the use of a magnetiser, and which is fast and cost-effective in comparison to conventional processes, was applied to the material to improve its wear resistance. The results of pin-on-disc wear testing using a AISI 52100 alloy counter pin revealed a decrease in the specific wear rate of the treated samples by 58% and a reduction in the value of the coefficient of friction by 28%. X-ray diffraction analysis showed a small increase in the amount of martensite and higher surface compressive residual stresses by 28% leading to improved hardness. The observed changes were not induced thermally. The volume expansion by the formation of martensite was achieved at near room temperature and led to a further increase in compressive residual stresses. The significance of this study is that the improvement in the properties was achieved at a current density value that was two orders of magnitude higher than the threshold for phase transformation and dislocation movement. The reasons for the effect of the alternating magnetic field treatment on the friction and wear properties are discussed in terms of the contribution of the magnetic field to the austenite-to-martensite phase transformation and the interaction between the magnetic domain walls and dislocations. Full article

This article compares the properties of the diamond-like carbon (DLC) coating with those of ZrN and (Zr,Hf)N coatings deposited on the Ti-6Al-4V titanium alloy substrate. To improve substrate adhesion during the deposition of the DLC coating, preliminary etching with chromium ions was conducted, ensuring the formation of a chromium-saturated diffusion surface layer in the substrate. A Si-DLC layer followed by a pure DLC layer was then deposited. The hardness of the coatings, their surface morphology, fracture strength in the scratch test, and tribological properties and wear resistance in the pin-on-disk test in contact with Al₂O₃ and steel indenters were investigated. The structure of the DLC coating was studied using transmission electron microscopy, and its corrosion resistance in an environment simulating blood plasma was also investigated. In the pin-on-disk test in contact with Al₂O₃ and AISI 52100 indenters, the DLC-coated sample demonstrates a much lower friction coefficient and significantly better wear resistance compared to the nitride-coated and uncoated samples. Both nitride coatings—(Zr,Hf)N and ZrN—and the DLC coating slow down the corrosive dissolution of the base compared to the uncoated sample. The corrosion currents of the (Zr,Hf)N-coated samples are 37.01 nA/cm², 20% higher than those of the ZrN-coated samples. The application of (Zr,Hf)N, ZrN, and DLC coatings on the Ti-6Al-4V alloy significantly inhibits dissolution currents (by 30–40%) and increases polarization resistance 1.5–2.0-fold compared to the uncoated alloy in 0.9% NaCl at 40 °C. Thus, the DLC coating of the described structure simultaneously provides effective wear and corrosion resistance in an environment simulating blood plasma. This coating can be considered in the manufacture of medical products (in particular, implants) from titanium alloys, including those functioning in the human body and subject to mechanical wear (e.g., knee joint endoprostheses). Full article

Titanium possesses many useful properties and is a technologically important material in engineering. However, lubrication of titanium has long been a problem that has prevented titanium from being more widely used. This is due to its poor tribological properties, deriving from its high tendency towards adhesive wear, material transfer, and abrasive wear. Lubrication is a system engineering which involves material combinations, material surfaces, lubricants, and operating conditions as a system. In this work, the boundary lubrication behavior of commercially pure titanium (CP-Ti) sliding against various counterbody materials in a motor oil (0W-30) was investigated under ball-on-plate reciprocating sliding conditions. The counterbody materials (balls) include CP-Ti, ceramic (Al₂O₃), steel (AISI 52100), and polymer (nylon). The results show that depending on material combination, the lubricating behavior can be divided into three categories, i.e., (1) lubrication failure (Ti-Ti), (2) improved lubrication but with friction instability (Ti-Al₂O₃), and (3) effective lubrication (Ti–steel and Ti–nylon). Lubrication failure of the Ti-Ti pair leads to high and unstable friction and severe wear from both the plate and ball, while friction instability of the Ti-Al₂O₃ pair leads to friction spikes and high wear rates. Effective lubrication of the Ti–steel pair results in low and smooth friction and much-reduced wear rates of the Ti plate by nearly 10,000 times. However, there is a load-dependence of the lubrication effectiveness of the Ti–steel pair. Although the Ti–nylon pair is effectively lubricated in terms of much-reduced friction, the nylon ball suffers from severe wear. The friction and wear mechanisms of the various sliding pairs are discussed in this paper. Full article

Casting AISI 52100 steel represents a challenge, particularly at the start of the casting sequence, due to its low melting point. The steel spilling over the tundish bottom cools down rapidly and freezes in the stopper rods, obliging the closure of a strand. Therefore, an additional function of turbulence inhibitors is to induce steel masses at a slow cooling rate. This paper deals with the physical and mathematical modeling of unsteady state-flows using two turbulence inhibitors (TIs) during the sequence start. One of the TIs makes steel spill forming thin layers of liquid on the tundish bottom, while the other forms a thicker layer. Based on the Flow of Volume Model, the mathematical simulation was satisfactorily replicated in the water model. Full article

In recent years, Golden Hard Anodizing (G.H.A.^®) has been developed as a variant of the traditional hard anodizing process with the addition of Ag⁺ ions in the nanoporous structure. The tribological properties of this innovative surface treatment are still not well understood. In this study, ball-on-disk tests were conducted in dry sliding conditions using 100Cr6 (AISI 52100) bearing steel balls as a counterbody and GHA^®-anodized EN AW-6082 aluminum alloy disks. The novelty of this work lies in the mapping of the wear properties of the tribocouple under different test conditions for a better comparison of the results. Three different normal loads (equal to 5, 10, and 15 N) and three different reciprocating frequencies (equal to 2, 3, and 4 Hz) were selected to investigate a spectrum of operating conditions for polished and unpolished G.H.A.^®-anodized EN AW-6082 aluminum alloy. Quantitative wear maps were built based on the resulting wear rate values to define the critical operating limits of the considered tribocouple. The results suggest that the coefficient of friction (COF) was independent of test conditions, while different wear maps were found for polished and non-polished surfaces. Polishing before anodizing permitted the acquisition of lower wear for the anodized disks and the steel balls. Full article

In this study, we analyze the extent to which thin hard coatings can serve as tribological protective layers for the selected plastic substrate materials PA12 (polyamide 12) und PEEK (polyetheretherketone), with and without fiber reinforcement. The approximately 1 µm thick coating variants ta-C, ta-C:N, and ta-C:B, which were applied using the laser arc process, are investigated. In oscillating sliding wear tests against a steel ball in an air atmosphere without lubricant, the wear of the coating and counter body is compared to analogous coating variants applied in parallel to AISI 52100 steel. The ta-C-based coatings show good adhesion strength and basic suitability as wear protection layers on the plastic substrates in the tribological tests. However, there are variations depending on the coating type and substrate material. The use of a Cr interlayer and its thickness also plays an important role. It is demonstrated that by coating under conditions where the uncoated plastic substrate would normally fail, a similarly good performance as with analogously coated steel substrates can be achieved by ta-C:N. Full article

This paper presents a comparison of two-component ammonia-based inlet atmospheres diluted with either hydrogen (NH₃/H₂) or nitrogen (NH₃/N₂). Taking advantage of the features of inlet atmospheres diluted with nitrogen and hydrogen, four two-stage processes were designed and carried out, which were juxtaposed with two single-stage processes carried out only in an NH₃ atmosphere. A common parameter of the processes carried out was the same value of nitrogen availability in each process stage. The gas nitriding process was carried out on ASIS 1085 non-alloy steel and ASIS 52100 alloy steel. It was found that the chemical composition of the steels studied, for the adopted nitriding process parameters, did not affect the kinetics of the growth in the mass of nitrided samples as a function of the nitriding time. However, the additions of alloying elements present in the steels studied significantly affected the nitrogen distribution between the resulting iron nitride layer and the diffusion zone in the nitrided substrate. Because of the presence of chromium in AISI 52100 steel, a larger mass of nitrogen accumulated in the nitriding zone in the solution compared with unalloyed AISI 1085 steel. As a result, with the same increase in the mass of nitrided steel, a thicker layer of iron nitrides formed on AISI 1085 steel than on AISI 52100 steel. Full article

In this study, shot peening (SP), quenching and tempering (QT) heat treatment, baking heat treatment and Cr-plating technologies were used to enhance the hardness, tribological properties and corrosion resistance of AISI 4340M steel. The purpose of this study is to develop repair process technology for an overhaul of landing gear applied to the MRO process and establish a quality assurance system. The effects of SP, QT heat treatment, Cr-plating, stripping after Cr-plating and Cr-plating after stripping and re-SP on the tribological properties and corrosion resistance of AISI 4340M steel were investigated, and the obtained results were compared with the base AISI 4340M steel. One of the reasons for stripping after Cr-plating is to find out how many times stripping can be done after Cr-plating. Moreover, it is important to investigate the effect of re-SP after Cr-plating on the tribological properties and corrosion resistance. The tribological properties of the specimens were investigated using a ball-on-disk tribometer at room temperature against AISI 52100 steel for 60 min under dry conditions. The corrosion resistance was investigated using a potentiodynamic polarization test in NaCl 3.5% solution. The results showed that the application of SP, QT heat treatment, Cr-plating, stripping after Cr-plating and Cr-plating after stripping and re-SP had a significant effect on the tribological properties and corrosion resistance of AISI 4340M steel. The effects of SP and Cr-plating post-treatment technologies on the wear and corrosion enhancement and mechanisms were discussed based on the microstructural and surface morphology of worn and corroded surfaces. Full article

By combining the ring rolling and roll bonding processes, the product spectrum can be additionally expanded. Since a successful composite ring rolling process requires a higher growth tendency for the inner ring, previous publications commonly included a softer inner ring to reduce the flow resistance of the inner ring or specific geometries for rings and tools. In this work, the material combination of a 100Cr6 (DIN 1.3505, AISI 52100) outer ring and a 42CrMo4 (DIN 1.7225, AISI 4140) inner ring is used to show that the composite ring rolling process is also possible for material combinations with a balanced flow stress ratio and equal wall thicknesses. In earlier publications, the influence of temperature was neglected. As the influence on the yield stress and thus on the success of the process has a significant influence, this should be considered in order to be able to make a reliable statement. For this purpose, the bond formation of the two materials was investigated by bonding experiments, and an existing bond formation model was extended with respect to the temperature dependency. On the basis of this model, the process control parameters were investigated using FE simulations, and a ring rolling experiment was carried out. Full article

Biodegradable metallic materials are gaining attention for medical applications in short-term implants (15–500 days) because of their good mechanical properties, biocompatibility, and generalized corrosion. Most medical applications involve implant wear processes, particularly for bone fractures. Parallelepipedic specimens (dimensions 50 mm × 10 mm × 3 mm) were obtained by cutting the hot-rolled material processed from cast ingots of ZnMgY. To test the tribological performance of these stationary specimens, they were placed at the upper point of the machine’s tribological contact. The rotating lower disk of the AMSLER machine (AMSLER & Co., Schaffhouse, Switzerland) is manufactured from AISI 52100 bearing steel with a 62–65 HRC hardness and a diameter of 59 mm both radially and axially. Frictional torque is the parameter that is measured. Scanning Electron Microscopy (SEM) and Energy Dispersive Spectroscopy (EDS) were used to analyze the worn areas. The material behavior in the normal and wear states upon immersion in simulated body fluid (SBF) was evaluated. Full article

Being a key component of the transmission system, the needle bearing’s performance and service life affects the overall service life of mechanical equipment. This study takes needle bearings composed of AISI 52100 steel as the research object and studies the effect of carbonitriding surface strengthening treatment on the bearing friction, wear, and fatigue life. The carbon and nitrogen co-infiltration surface-strengthening method was employed to prepare cylindrical and disc samples. The surface hardness, residual austenite content, microscopic morphology and organization composition, coefficient of friction, and wear scar were studied to analyze the effect on the wear performance of the material. The bearing fatigue wear comparison test was conducted on a test bench to compare the actual fatigue life and surface damage of the needle bearing through conventional martensitic quenching heat treatment and carbonitriding treatment. The results demonstrate that the carbonitriding strengthening method enhances the toughness of the material while improving its surface hardness. It also improves the wear resistance of the needle roller bearings, and the fatigue life of the bearings is significantly improved. In conclusion, carbon and nitrogen co-infiltration treatment is a strengthening method that effectively extends the service life of needle roller bearings, indicating its high practical value. Full article