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20 pages, 1448 KiB  
Article
In Vitro Evaluation of Chemical and Microhardness Alterations in Human Enamel Induced by Three Commercial In-Office Bleaching Agents
by Berivan Laura Rebeca Buzatu, Atena Galuscan, Ramona Dumitrescu, Roxana Buzatu, Magda Mihaela Luca, Octavia Balean, Gabriela Vlase, Titus Vlase, Iasmina-Mădălina Anghel, Carmen Opris, Bianca Ioana Todor, Mihaela Adina Dumitrache and Daniela Jumanca
Dent. J. 2025, 13(8), 357; https://doi.org/10.3390/dj13080357 - 6 Aug 2025
Abstract
Background/Objectives: In-office bleaching commonly employs high concentrations of hydrogen peroxide (HP) or carbamide peroxide (CP), which may compromise enamel integrity. This in vitro paired-design study aimed to compare the chemical and mechanical effects of three commercial bleaching agents—Opalescence Boost (40% HP), Opalescence [...] Read more.
Background/Objectives: In-office bleaching commonly employs high concentrations of hydrogen peroxide (HP) or carbamide peroxide (CP), which may compromise enamel integrity. This in vitro paired-design study aimed to compare the chemical and mechanical effects of three commercial bleaching agents—Opalescence Boost (40% HP), Opalescence Quick (45% CP), and BlancOne Ultra+ (35% HP)—on human enamel. The null hypothesis assumed no significant differences between the control and treated samples. Given the ongoing debate over pH, active ingredients, and enamel impact, comparing whitening systems remains clinically important. Methods: Forty-two extracted teeth were assigned to three experimental groups (n = 14) with matched controls. Each underwent a single bleaching session per manufacturer protocol: Opalescence Boost (≤60 min), Opalescence Quick (15–30 min), and BlancOne Ultra+ (three light-activated cycles of 8–10 min). Enamel chemical changes were analyzed by Fourier transform infrared (FTIR) spectroscopy (phosphate and carbonate bands), and surface hardness by Vickers microhardness testing. Paired t-tests (α = 0.05) assessed statistical significance. Results: FTIR analysis revealed alterations in phosphate and carbonate bands for all agents, most notably for Opalescence Boost and BlancOne Ultra+. Microhardness testing showed significant reductions in enamel hardness for Opalescence Boost (control: 37.21 ± 1.74 Hv; treated: 34.63 ± 1.70 Hv; p = 0.00) and Opalescence Quick (control: 45.82 ± 1.71 Hv; treated: 39.34 ± 1.94 Hv; p < 0.0001), whereas BlancOne Ultra+ showed no significant difference (control: 51.64 ± 1.59 HV; treated: 51.60 ± 2.34 Hv; p = 0.95). Conclusions: HP-based agents, particularly at higher concentrations, caused greater enamel alterations than CP-based products. While clinically relevant, the results should be interpreted cautiously due to in vitro limitations and natural enamel variability. Full article
(This article belongs to the Special Issue Advances in Esthetic Dentistry)
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16 pages, 5162 KiB  
Article
Kernel-FastICA-Based Nonlinear Blind Source Separation for Anti-Jamming Satellite Communications
by Xiya Sun, Changqing Li, Jiong Li and Qi Su
Sensors 2025, 25(12), 3743; https://doi.org/10.3390/s25123743 - 15 Jun 2025
Viewed by 381
Abstract
Satellite communication systems, as a core component of global information infrastructure, have undergone unprecedented development. However, the open nature of satellite channels renders them vulnerable to electromagnetic interference, making anti-jamming techniques a persistent research focus in this domain. Satellite transponders contain various power-sensitive [...] Read more.
Satellite communication systems, as a core component of global information infrastructure, have undergone unprecedented development. However, the open nature of satellite channels renders them vulnerable to electromagnetic interference, making anti-jamming techniques a persistent research focus in this domain. Satellite transponders contain various power-sensitive components that exhibit nonlinear characteristics under interference conditions, yet conventional anti-jamming approaches typically neglect the nonlinear distortion in transponders when suppressing interference. To address this challenge, this paper proposes a kernel-method-optimized FastICA algorithm (Kernel-FastICA) that establishes a post-nonlinear mixing model to precisely characterize signal transmission and reception processes. The algorithm transforms nonlinear separation tasks into high-dimensional, linear independent-component-analysis problems through kernel learning methodology. Furthermore, we introduce a regularized pre-whitening strategy to mitigate potential ill-conditioned issues arising from dimensional expansion, thereby enhancing numerical stability and separation performance. The simulation results demonstrate that the proposed algorithm exhibits superior robustness against interference and enhanced generalization capabilities in nonlinear jamming environments compared with existing solutions. Full article
(This article belongs to the Section Communications)
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17 pages, 7868 KiB  
Article
The Effectiveness of Different Cleaning Methods for Clear Orthodontic Aligners: Impacts on Physical, Mechanical, and Chemical Properties—An In Vivo Study
by Athar Alweneen and Nasser Alqahtani
Polymers 2025, 17(12), 1620; https://doi.org/10.3390/polym17121620 - 11 Jun 2025
Viewed by 1000
Abstract
Maintaining the cleanliness of orthodontic aligners is crucial for oral hygiene and preserving the optical properties of aligners. In this randomized clinical trial, we compared the effectiveness of different cleaning methods for the maintenance of Invisalign clear aligners. Twelve adult patients received five [...] Read more.
Maintaining the cleanliness of orthodontic aligners is crucial for oral hygiene and preserving the optical properties of aligners. In this randomized clinical trial, we compared the effectiveness of different cleaning methods for the maintenance of Invisalign clear aligners. Twelve adult patients received five aligners, each worn for 10 days. The aligners were divided based on the cleaning method: tooth brushing with whitening toothpaste, vinegar, Fittydent Super Cleansing Tablets, Invisalign cleaning crystals, and only water. Scanning electron microscopy (SEM) was used to detect surface morphology changes; color changes (ΔE) were evaluated using a spectrophotometer. Fourier transform infrared spectroscopy (FTIR) with a diamond hemisphere was used to study the aligners’ chemical compositions. Nanoindentation testing was used to assess changes in the elastic modulus. SEM confirmed the effectiveness of Invisalign cleaning crystals in maintaining cleanliness, revealing a surface similar to that of the control group with no adverse effects. Color stability analysis revealed significant ΔE value differences; whitening toothpaste had significantly lower ΔE values than water and Invisalign cleaning crystals. The elastic modulus and FTIR analyses indicated no significant differences between the cleaning methods. Therefore, Invisalign cleaning crystals and whitening toothpaste are safe for aligner maintenance, showing successful and aesthetically pleasing results. Full article
(This article belongs to the Section Polymer Applications)
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17 pages, 8727 KiB  
Article
Synthesis of Nano-Selenium from Bombyx batryticatus Polypeptide and Exploring Its Antioxidant and Skin Whitening Ability
by Yang Ning, Chen Peng, Li Weihong, Feng Cuiping, Wang Xiaowen and Wang Qiling
Molecules 2025, 30(5), 1153; https://doi.org/10.3390/molecules30051153 - 4 Mar 2025
Viewed by 807
Abstract
To increase the stability of selenium in nano state and further improve its antioxidant and skin whitening ability, Bombyx batryticatus polypeptide (BBPP) was prepared. The optimum synthesis conditions of Bombyx batryticatus polypeptide nano-selenium (BBPP-SeNPs) were determined by a double-peak method. BBPP-SeNPs were characterized [...] Read more.
To increase the stability of selenium in nano state and further improve its antioxidant and skin whitening ability, Bombyx batryticatus polypeptide (BBPP) was prepared. The optimum synthesis conditions of Bombyx batryticatus polypeptide nano-selenium (BBPP-SeNPs) were determined by a double-peak method. BBPP-SeNPs were characterized by transmission electron microscope (TEM), Fourier transform infrared spectroscopy (FT-IR), and particle size analysis (PSS). The 1,1-Diphenyl-2-picrylhydrazyl (DPPH), 2,2’-azino-bis (3-ethylbenzothiazoline-6-sulfonic acid (ABTS), superoxide anion free radical scavenging rate, and total antioxidant capacity of BBPP, vitamin C (VC), and BBPP-SeNPs were measured for comparison. The inhibitory ability of BBPP and BBPP-SeNPs on tyrosinase was measured. Using mouse modeling, the skin whitening ability of VC and BBPP-SeNPs was measured. The results showed that the optimal conditions were obtained when the concentration of BBPP was 0.16 mg/mL, sodium selenite was 0.01 mol/L, ultrasound was carried out for 30 min, ascorbic acid was added in 0.04 mol/L, and stirring temperature was 20 °C for 4 h. The antioxidant capacity of BBPP-SeNPs has significantly improved. It can be observed that BBPP-SeNPs has obvious scavenging ability on skin-reactive oxygen species through a Reactive Oxygen Species (ROS) staining section. Through Hematoxylin–Eosin (H&E) staining, it can be proven that BBPP-SeNPs has a high security threshold. Full article
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12 pages, 259 KiB  
Review
Laser Technology in Dentistry: From Clinical Applications to Future Innovations
by Liliana Sachelarie, Roxana Cristea, Ecaterina Burlui and Loredana Liliana Hurjui
Dent. J. 2024, 12(12), 420; https://doi.org/10.3390/dj12120420 - 23 Dec 2024
Cited by 10 | Viewed by 4152
Abstract
This narrative review comprehensively synthesizes laser technology’s clinical applications, advantages, and limitations in modern dentistry. The review of 67 articles published between 2018 and 2023 highlights the latest advancements, including photobiomodulation (PBM) for enhanced tissue healing and inflammation control, alongside innovative uses in [...] Read more.
This narrative review comprehensively synthesizes laser technology’s clinical applications, advantages, and limitations in modern dentistry. The review of 67 articles published between 2018 and 2023 highlights the latest advancements, including photobiomodulation (PBM) for enhanced tissue healing and inflammation control, alongside innovative uses in implantology, endodontics, and teeth whitening. The findings underscore the transformative potential of lasers in improving dental treatment precision and patient outcomes while addressing the barriers to their widespread adoption, such as costs and training needs. This review emphasizes the integration of laser technology into routine clinical practice and identifies pathways for future innovations in dentistry. Full article
(This article belongs to the Special Issue Laser Dentistry: The Current Status and Developments)
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14 pages, 3747 KiB  
Article
Investigation of Whitening Mechanism on Cultural Relic Surfaces Treated with Paraloid B72
by Xing Zhao, Xia Li, Siyu Zhang, Qing Niu, Zongmin Li and Cheng Xue
Coatings 2024, 14(10), 1240; https://doi.org/10.3390/coatings14101240 - 26 Sep 2024
Cited by 2 | Viewed by 1493
Abstract
In the conservation of cultural relics, the application of Paraloid B72 in humid environments frequently results in the surface whitening of artifacts, which impairs their appearance and conceals important details. This study investigates the mechanisms underlying this phenomenon by examining the effect of [...] Read more.
In the conservation of cultural relics, the application of Paraloid B72 in humid environments frequently results in the surface whitening of artifacts, which impairs their appearance and conceals important details. This study investigates the mechanisms underlying this phenomenon by examining the effect of ambient humidity, Paraloid B72 mass concentration, solution addition volume, and solvent type. To evaluate the microstructure, transmittance, and composition of the films, a range of analytical techniques were employed, including optical microscopy, scanning electron microscopy, a UV-Visible Spectrophotometer, and Fourier transform infrared spectroscopy. The findings indicate that higher ambient humidity, lower Paraloid B72 mass concentration, smaller solution addition volume, and solvents with higher volatility and water miscibility increase water content during curing, intensifying the whitening effect. These factors modify the interaction between water and solvent, altering the surface structure of Paraloid B72. The whitening mechanism is linked to the cooling effect of solvent volatility, which lowers the dew point temperature at the air–solution interface, causing moisture condensation. Moisture forms droplets that leave irregular pores upon volatility, resulting in surface roughness, optical heterogeneity, and a reduced refractive index, resulting in whitening. This study provides a theoretical basis for understanding and preventing the whitening of Paraloid B72. Full article
(This article belongs to the Special Issue Coatings for Cultural Heritage: Cleaning, Protection and Restoration)
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11 pages, 4274 KiB  
Brief Report
Spectral Detection of a Weak Frequency Band Signal Based on the Pre-Whitening Scale Transformation of Stochastic Resonance in a Symmetric Bistable System in a Parallel Configuration
by Zhijun Qin, Tengfei Xie, Chen Xie and Di He
Electronics 2024, 13(18), 3637; https://doi.org/10.3390/electronics13183637 - 12 Sep 2024
Viewed by 797
Abstract
The spectral detection of weak frequency band signals poses a serious problem in many applications, especially when the target is within a certain frequency band under low signal-to-noise ratio (SNR) conditions. A kind of novel technique based on the pre-whitening scale transformation of [...] Read more.
The spectral detection of weak frequency band signals poses a serious problem in many applications, especially when the target is within a certain frequency band under low signal-to-noise ratio (SNR) conditions. A kind of novel technique based on the pre-whitening scale transformation of stochastic resonance (SR) in a symmetric bistable system in a parallel configuration is proposed to solve the problem. Firstly, pre-whitening can ensure the Gaussian distribution of the receiving signal fits the requirements for SR processing. Secondly, scale transformation can help to effectively utilize the properties of a weak signal, especially under a low-frequency band. Thirdly, the SR in a symmetric bistable system in a parallel configuration can try to smoothly reduce the variances in the clutter and additive noise. Fourthly, by subtracting the steady state response of the SR in the selected symmetric bistable system from the parallel output, the spectral detection of a weak signal can be realized successfully. Experiment results based on actual sea clutter radar data guarantee the effectiveness and applicability of the proposed symmetric bistable PSR processing approach. Full article
(This article belongs to the Special Issue Nonlinear Circuits and Systems: Latest Advances and Prospects)
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13 pages, 2615 KiB  
Article
Evaluating the Dermatological Benefits of Snowberry (Symphoricarpos albus): A Comparative Analysis of Extracts and Fermented Products from Different Plant Parts
by Chanwoo Lee, Hana Cho, Myunsoo Kim, Boae Kim, Young-Pyo Jang and Junseong Park
Int. J. Mol. Sci. 2024, 25(17), 9660; https://doi.org/10.3390/ijms25179660 - 6 Sep 2024
Cited by 1 | Viewed by 1806
Abstract
Skin ageing is influenced by both intrinsic and extrinsic factors, with excessive ultraviolet (UV) exposure being a significant contributor. Such exposure can lead to moisture loss, sagging, increased wrinkling, and decreased skin elasticity. Prolonged UV exposure negatively impacts the extracellular matrix by reducing [...] Read more.
Skin ageing is influenced by both intrinsic and extrinsic factors, with excessive ultraviolet (UV) exposure being a significant contributor. Such exposure can lead to moisture loss, sagging, increased wrinkling, and decreased skin elasticity. Prolonged UV exposure negatively impacts the extracellular matrix by reducing collagen, hyaluronic acid, and aquaporin 3 (AQP-3) levels. Fermentation, which involves microorganisms, can produce and transform beneficial substances for human health. Natural product fermentation using lactic acid bacteria have demonstrated antioxidant, anti-inflammatory, antibacterial, whitening, and anti-wrinkle properties. Snowberry, traditionally used as an antiemetic, purgative, and anti-inflammatory agent, is now also used as an immune stimulant and for treating digestive disorders and colds. However, research on the skin benefits of Fermented Snowberry Extracts remains limited. Thus, we aimed to evaluate the skin benefits of snowberry by investigating its moisturising and anti-wrinkle effects, comparing extracts from different parts of the snowberry plant with those subjected to fermentation using Lactobacillus plantarum. Chlorophyll-free extracts were prepared from various parts of the snowberry plant, and ferments were created using Lactobacillus plantarum. The extracts and ferments were analysed using high-performance liquid chromatography (HPLC) to determine and compare their chemical compositions. Moisturising and anti-ageing tests were conducted to assess the efficacy of the extracts and ferments on the skin. The gallic acid content remained unchanged across all parts of the snowberry before and after fermentation. However, Fermented Snowberry Leaf Extracts exhibited a slight decrease in chlorogenic acid content but a significant increase in ferulic acid content. The Fermented Snowberry Fruit Extract demonstrated increased chlorogenic acid and a notable rise in ferulic acid compared to its non-fermented counterpart. Skin efficacy tests revealed that Fermented Snowberry Leaf and Fruit Extracts enhanced the expression of AQP-3, HAS-3, and COL1A1. These extracts exhibited distinct phenolic component profiles, indicating potential skin benefits such as improved moisture retention and protection against ageing. These findings suggest that Fermented Snowberry Extracts could be developed into effective skincare products, providing a natural alternative for enhancing skin hydration and reducing signs of ageing. Full article
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21 pages, 3375 KiB  
Article
An Audio Watermarking Algorithm Based on Adversarial Perturbation
by Shiqiang Wu, Jie Liu, Ying Huang, Hu Guan and Shuwu Zhang
Appl. Sci. 2024, 14(16), 6897; https://doi.org/10.3390/app14166897 - 6 Aug 2024
Viewed by 1954
Abstract
Recently, deep learning has been gradually applied to digital watermarking, which avoids the trouble of hand-designing robust transforms in traditional algorithms. However, most of the existing deep watermarking algorithms use encoder–decoder architecture, which is redundant. This paper proposes a novel audio watermarking algorithm [...] Read more.
Recently, deep learning has been gradually applied to digital watermarking, which avoids the trouble of hand-designing robust transforms in traditional algorithms. However, most of the existing deep watermarking algorithms use encoder–decoder architecture, which is redundant. This paper proposes a novel audio watermarking algorithm based on adversarial perturbation, AAW. It adds tiny, imperceptible perturbations to the host audio and extracts the watermark with a pre-trained decoder. Moreover, the AAW algorithm also uses an attack simulation layer and a whitening layer to improve performance. The AAW algorithm contains only a differentiable decoder, so it reduces the redundancy. The experimental results also demonstrate that the proposed algorithm is effective and performs better than existing audio watermarking algorithms. Full article
(This article belongs to the Special Issue Recent Advances in Multimedia Steganography and Watermarking)
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12 pages, 827 KiB  
Review
Improving the Traits of Perilla frutescens (L.) Britt Using Gene Editing Technology
by Sivabalan Karthik, Jia Chae, Seong Ju Han, Jee Hye Kim, Hye Jeong Kim, Young-Soo Chung, Hyun Uk Kim and Jae Bok Heo
Plants 2024, 13(11), 1466; https://doi.org/10.3390/plants13111466 - 25 May 2024
Cited by 3 | Viewed by 2734
Abstract
Plant breeding has evolved significantly over time with the development of transformation and genome editing techniques. These new strategies help to improve desirable traits in plants. Perilla is a native oil crop grown in Korea. The leaves contain many secondary metabolites related to [...] Read more.
Plant breeding has evolved significantly over time with the development of transformation and genome editing techniques. These new strategies help to improve desirable traits in plants. Perilla is a native oil crop grown in Korea. The leaves contain many secondary metabolites related to whitening, aging, antioxidants, and immunity, including rosmarinic acid, vitamin E, luteolin, anthocyanins, and beta-carotene. They are used as healthy and functional food ingredients. It is an industrially valuable cosmetics crop. In addition, perilla seeds are rich in polyunsaturated fatty acids, such as α-linolenic acid and linoleic acid. They are known to be effective in improving neutral lipids in the blood, improving blood circulation, and preventing dementia and cardiovascular diseases, making them excellent crops whose value can be increased through improved traits. This research will also benefit perilla seeds, which can increase their stock through various methods, such as the increased production of functional substances and improved productivity. Recently, significant attention has been paid to trait improvement research involving gene-editing technology. Among these strategies, CRISPR/Cas9 is highly adaptable, enabling accurate and efficient genome editing, targeted mutagenesis, gene knockouts, and the regulation of gene transcription. CRISPR/Cas9-based genome editing has enormous potential for improving perilla; however, the regulation of genome editing is still at an early stage. Therefore, this review summarizes the enhancement of perilla traits using genome editing technology and outlines future directions. Full article
(This article belongs to the Special Issue Plant Transformation and Genome Editing)
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29 pages, 16784 KiB  
Article
Pre-Processing of Simulated Synthetic Aperture Radar Image Scenes Using Polarimetric Enhancement for Improved Ship Wake Detection
by Yanni Jiang, Ziyuan Yang, Ke Li and Tao Liu
Remote Sens. 2024, 16(4), 658; https://doi.org/10.3390/rs16040658 - 11 Feb 2024
Cited by 5 | Viewed by 1923
Abstract
Ship wake detection using synthetic aperture radar (SAR) imagery provides a way to obtain small marine ship information, but it often becomes unavailable and unreliable during a high sea state. Polarimetric information provides a potential way to solve this problem, which can enhance [...] Read more.
Ship wake detection using synthetic aperture radar (SAR) imagery provides a way to obtain small marine ship information, but it often becomes unavailable and unreliable during a high sea state. Polarimetric information provides a potential way to solve this problem, which can enhance the ship target as well as the ship wake features. However, three challenges still exist in ship wake detection in polarimetric SAR imagery: the unwanted influences of bright and singular points on ship wake detection, the lack of performance analysis of wake detection by new-type polarimetric enhancement methods, and the difficulty of using the assessment criteria for ship wake detection. In this paper, we try to solve the above problems. Firstly, fully polarized SAR imagery of both ship turbulent and Kelvin wake is simulated based on the two-scale composite model, and the Polarimetric Whitening Filter (PWF) and Polarimetric Detection Optimization Filter (PDOF) are applied to the simulated fully polarized SAR imagery to enhance the ship wake features. Secondly, since the bright and singular points resulting from the ship echoes and the polarimetric enhancement methods may lead to misdetections, a logarithm process and z-score normalization pre-processing has been applied to the images. Then, a new assessment criterion for wake detection performance has been formulated, and the probability of missing detections (PMDs) and the probability of false alarms (PFAs) have been defined for two different requirements. And a Radon transform-based ship wake detection method for both ship turbulence and Kelvin wake has been carried out in horizontal–horizontal (HH), vertical–vertical (VV), horizontal–vertical (HV), PWF and PDOF SAR imagery. Finally, an analysis of the wake detection performance has been carried out. The PWF and PDOF can improve the wake detection performance by an average of nearly 50 percent compared with the HH and VV. Full article
(This article belongs to the Section Remote Sensing Image Processing)
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12 pages, 290 KiB  
Article
Grey Time Power Model with Caputo Fractional Derivative
by Pan Hu and Chuan-Yun Gu
Fractal Fract. 2024, 8(1), 25; https://doi.org/10.3390/fractalfract8010025 - 28 Dec 2023
Cited by 1 | Viewed by 1437
Abstract
In this paper, the inverse cumulative grey time power model with a Caputo fractional derivative is established, and the solution to the whitening equation is given by the Laplace transform. To improve the prediction accuracy of the model, the linear-tangent-function transformation is used [...] Read more.
In this paper, the inverse cumulative grey time power model with a Caputo fractional derivative is established, and the solution to the whitening equation is given by the Laplace transform. To improve the prediction accuracy of the model, the linear-tangent-function transformation is used to improve the smoothness of the data sequence, and a grey time power model is obtained, which has higher accuracy than the sinusoidal-function transformation, negative-exponential-function transformation and logarithmic-function transformation. The form and application range of the model are generalized. Full article
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7 pages, 1832 KiB  
Proceeding Paper
Toward a Circular Bioeconomy: Extracting Cellulose from Grape Stalks
by Liliana Araújo, Adriana R. Machado, Manuela Pintado, Eduarda Vieira and Patrícia Moreira
Eng. Proc. 2023, 37(1), 86; https://doi.org/10.3390/ECP2023-14746 - 7 Jun 2023
Cited by 4 | Viewed by 1245
Abstract
The purpose of this study was to assess the extraction of cellulose from stalks of vines using auto-hydrolysis and characterize it. As the results obtained, the colorimeter readings displayed a final yellow color of the fiber, demonstrating that the bleaching process was insufficient [...] Read more.
The purpose of this study was to assess the extraction of cellulose from stalks of vines using auto-hydrolysis and characterize it. As the results obtained, the colorimeter readings displayed a final yellow color of the fiber, demonstrating that the bleaching process was insufficient and that multiple bleaching processes might be required. According to the FTIR (Fourier-transform infrared spectroscopy) data, there were stretching and deformation vibrationsof characteristic peak that represent cellulose (2900, 1500, and 1200 cm−1). Although lignin and hemicellulose were partially removed according to the FTIR, distinct cellulose yields were achieved for each fraction, including fractions 500, 300, 250, 150 µm, and retain, with values of 21.98, 12.70, 7.20, 5.74, and 3.11%, respectively. In sum, we were able to extract cellulose from the stalk vine, although the last step still needs to be optimized for better whitening. Full article
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21 pages, 4302 KiB  
Article
Extraction Optimization, Characterization and Biological Activities of Polysaccharide Extracts from Nymphaea hybrid
by Hui-Min Liu, Wei Tang, Sheng-Nan Lei, Yun Zhang, Ming-Yan Cheng, Qing-Lei Liu and Wei Wang
Int. J. Mol. Sci. 2023, 24(10), 8974; https://doi.org/10.3390/ijms24108974 - 18 May 2023
Cited by 13 | Viewed by 2829
Abstract
In this study, polysaccharide–rich Nymphaea hybrid extracts (NHE) were obtained using the ultrasound-assisted cellulase extraction (UCE) method optimized by response surface methodology (RSM). The structural properties and thermal stability of NHE were characterized by Fourier-transform infrared (FT–IR), high–performance liquid chromatography (HPLC) and thermogravimetry–derivative [...] Read more.
In this study, polysaccharide–rich Nymphaea hybrid extracts (NHE) were obtained using the ultrasound-assisted cellulase extraction (UCE) method optimized by response surface methodology (RSM). The structural properties and thermal stability of NHE were characterized by Fourier-transform infrared (FT–IR), high–performance liquid chromatography (HPLC) and thermogravimetry–derivative thermogravimetry (TG–DTG) analysis, respectively. Moreover, the bioactivities of NHE, including the antioxidant, anti–inflammatory, whitening and scratch healing activities were evaluated by different in vitro assays. NHE conveyed a good ability to scavenge against the 2,2-diphenyl-1-picrylhydrazyl (DPPH) free radicals and inhibit the hyaluronidase activity. NHE can effectively protect the HaCaT cells against oxidative damage by inhibiting the intracellular reactive oxygen species (ROS) production in the H2O2 stimulation assays and promoting the proliferation and migration in the scratch assays. In addition, NHE was proven to inhibit melanin production in B16 cells. Collectively, the above results seem to be the evidence needed to promote the potential of NHE to be regarded as a new functional raw material in the cosmetics or food industries. Full article
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14 pages, 12203 KiB  
Article
Novelty Cosmetic Filters Based on Nanomaterials Composed of Titanium Dioxide Nanoparticles
by Marta Bartoszewska, Elżbieta Adamska, Agata Kowalska and Beata Grobelna
Molecules 2023, 28(2), 645; https://doi.org/10.3390/molecules28020645 - 8 Jan 2023
Cited by 23 | Viewed by 3830
Abstract
The following work describes the synthesis of new physical filters based on TiO2/SiO2 and TiO2/Ag nanostructures. Titanium dioxide nanoparticles (TiO2 NPs) were applied as control material and a popular physical UV filter. The advantage of using materials [...] Read more.
The following work describes the synthesis of new physical filters based on TiO2/SiO2 and TiO2/Ag nanostructures. Titanium dioxide nanoparticles (TiO2 NPs) were applied as control material and a popular physical UV filter. The advantage of using materials on the nanometer scale is the elimination of the skin whitening effect that occurs when using photoprotective cosmetics containing titanium dioxide on a macro scale. In addition, the silica coating makes the material less harmful, and the silver coating enriches the material with antibacterial properties. Nanoparticles and nanostructures have been characterized by Energy Dispersive X-Ray Analysis (EDX), the Scanning Electron Microscope (SEM), Transmission Electron Microscopy (TEM), and Fourier-Transform Infrared Spectroscopy (FT-IR) methods. Due to the use of physical filters in anti-radiation protection cosmetics, water-in-oil (W/O) emulsion has been prepared. All cosmetic formulations have been tested for stability. The sun protection research with the Sun Protection Diagnostic SP37 was carried out. These studies made it possible to determine the natural sun protection time and to compare the synthesized materials. Furthermore, one of the most important parameters when describing this type of cosmetic is water resistance, which has also been measured. The results show that the new type of material of TiO2/Ag used as a new physical filter in emulsion W/O shows the best sun protection compared with other obtained nanomaterials. It is most likely due to the improved optical properties of the combination of noble metals, for example, silver with TiO2. Full article
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