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Keywords = superplastic forming and diffusion bonding

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31 pages, 9460 KB  
Article
Design, Manufacturing and Experimental Validation of an Integrated Wing Ice Protection System in a Hybrid Laminar Flow Control Leading Edge Demonstrator
by Ionut Brinza, Teodor Lucian Grigorie and Grigore Cican
Appl. Sci. 2026, 16(3), 1347; https://doi.org/10.3390/app16031347 - 28 Jan 2026
Cited by 1 | Viewed by 604
Abstract
This paper presents the design, manufacturing, instrumentation and validation by tests (ground and icing wind tunnel) of a full-scale Hybrid Laminar Flow Control (HLFC) leading-edge demonstrator based on Airbus A330 outer wing plan-form. The Ground-Based Demonstrator (GBD) was developed to reproduce a full-scale, [...] Read more.
This paper presents the design, manufacturing, instrumentation and validation by tests (ground and icing wind tunnel) of a full-scale Hybrid Laminar Flow Control (HLFC) leading-edge demonstrator based on Airbus A330 outer wing plan-form. The Ground-Based Demonstrator (GBD) was developed to reproduce a full-scale, realistic wing section integrating into the leading-edge three key systems: micro-perforated skin for the hybrid laminar flow control suction system (HLFC), the hot-air Wing Ice Protection System (WIPS) and a folding “bull nose” Krueger high-lift device. The demonstrator combines a superplastic-formed and diffusion-bonded (SPF/DB) perforated titanium skin mounted on aluminum ribs jointed with a carbon-fiber-reinforced polymer (CFRP) wing box. Titanium internal ducts were designed to ensure uniform hot-air distribution and structural compatibility with composite components. Manufacturing employed advanced aeronautical processes and precision assembly under INCAS coordination. Ground tests were performed using a dedicated hot-air and vacuum rig delivering up to 200 °C and 1.6 bar, thermocouples and pressure sensors. The results confirmed uniform heating (±2 °C deviation) and stable operation of the WIPS without structural distortion. Relevant tests were performed in the CIRA Icing Wind Tunnel facility, verifying the anti-ice protection system and Krueger device. The successful design, fabrication, testing and validation of this multifunctional leading edge—featuring integrated HLFC, WIPS and Krueger systems—demonstrates the readiness of the concept for subsequent aerodynamic testing. Full article
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20 pages, 11713 KB  
Article
Superplastic Forming/Diffusion Bonding of TA15 Titanium Alloy for Manufacturing Integrated Solid/Hollow Four-Layer Grid Lightweight Structure Components
by Zheng Han, Yuhan Xing, Taiying Liu, Ning Zhang, Shaosong Jiang and Zhen Lu
Metals 2025, 15(1), 28; https://doi.org/10.3390/met15010028 - 31 Dec 2024
Viewed by 2833
Abstract
In recent years, the excellent mechanical properties and lightweight characteristics of multi-layer hollow components have led to a surge in research focused on their forming processes. This growing interest has greatly advanced technological progress in aerospace and other related fields. In this paper, [...] Read more.
In recent years, the excellent mechanical properties and lightweight characteristics of multi-layer hollow components have led to a surge in research focused on their forming processes. This growing interest has greatly advanced technological progress in aerospace and other related fields. In this paper, the metal flow behavior of TA15 titanium alloy at different temperatures from 840 °C to 940 °C and different strain rates from 0.001 s−1 to 0.1 s−1 was studied. Utilizing the finite element method, this study examined the local stress concentration, total strain distribution, thickness thinning characteristics, and pressure loading control during the superplastic forming process of the component. The integrated solid/hollow four-layer grid lightweight structural parts were successfully fabricated using the superplastic forming/diffusion bonding (SPF/DB) process. The quality of the components was evaluated using X-ray and ultrasonic C-scan detection methods. The results show that the maximum elongation of the alloy is 1340% at 900 °C/0.001 s−1. When the temperature is too high, the grain size increases remarkably, and the elongation decreases. Based on the finite element simulation results, 900 °C is the best superplastic forming temperature. Under this temperature parameter, the maximum thinning rate of the core sheet is 39.7%, the SPF time is 10,000 s, the maximum thinning rate of the face sheet is 9.8%, and the SPF time is 2400 s. In addition, the solid block has a minimal effect on the thinning of the core sheet. The grid exhibits obvious stress concentration and thinning at its rounded corners, while the thickness distribution in other areas remains relatively uniform. The nondestructive testing results confirmed that the ribs of the component are fully formed, with no missing or broken ribs. The grid exhibits good geometry and high-quality diffusion bonding. The average thickness at key positions of the component is 1.84 mm, with the minimum thickness being 1.7 mm. As the size of the grid cavity decreases, the thickness of the component tends to increase gradually. The maximum error between the simulated and measured values is 4.47%, indicating good accuracy in the simulation. Additionally, the thickness distribution of the component is relatively uniform. Full article
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11 pages, 4172 KB  
Article
Study on SPF/DB Technology for Two-Sheet Hollow Structure of 1420 Al-Li Alloy
by Yaoming Li, Honglin Wang, Tao Niu, Huang Zhang and Meini Yuan
Metals 2022, 12(3), 389; https://doi.org/10.3390/met12030389 - 23 Feb 2022
Cited by 5 | Viewed by 2827
Abstract
The two-sheet hollow structure of the 1420 Al-Li alloy was prepared by the method of superplastic forming and diffusion bonding. The interface combination status of the diffusion bonding region and the microstructure of the superplastic forming region were observed by an optical microscope. [...] Read more.
The two-sheet hollow structure of the 1420 Al-Li alloy was prepared by the method of superplastic forming and diffusion bonding. The interface combination status of the diffusion bonding region and the microstructure of the superplastic forming region were observed by an optical microscope. The thickness distribution of the superplastic forming region was measured by an ultrasonic thickness meter machine, the defect detection was tested by X-ray nondestructive inspection, and the failure modes of the samples were analyzed. The results showed that the two-sheet hollow structure of the 1420 Al-Li alloy was prepared successfully, the structure was integrated, and there were no shape defects such as pit, wrinkle, and collapse. The structure shape was almost attached to the die completely, and the thickness was almost uniform distribution. The no deforming area of the two-sheet hollow structure of the 1420 Al-Li alloy was a long strip, rolled microstructure, while the grains near the round corner area were equiaxed states resulting from dynamic recrystallization. The improper control of the superplastic gas pressure in the forming process would lead to the tearing or the die-attaching failure for the two-sheet hollow structure of the 1420 Al-Li alloy. Full article
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11 pages, 5925 KB  
Article
The Effect of Grain Size on the Diffusion Bonding Properties of SP700 Alloy
by Qianwen Zhang, Jianjun Wu, Shaosong Jiang and Gang He
Metals 2022, 12(2), 237; https://doi.org/10.3390/met12020237 - 26 Jan 2022
Cited by 142 | Viewed by 5117
Abstract
Superplastic forming and diffusion bonding (SPF/DB) has been recognized as a viable manufacturing technology. However, the basic understanding of grain size and its effects on the quality of diffusion bonds is still limited. In this study, a certain type of SP700 alloy with [...] Read more.
Superplastic forming and diffusion bonding (SPF/DB) has been recognized as a viable manufacturing technology. However, the basic understanding of grain size and its effects on the quality of diffusion bonds is still limited. In this study, a certain type of SP700 alloy with different grain sizes is bonded at superplastic temperature. The experimental results indicate that the same materials, if coarse-grained, may not readily bond under identical conditions of pressure, temperature, and time. This type of bonding is possible because of the presence of many grain boundaries in fine-grained materials that act as short-circuit paths for diffusion. In addition, grain-boundary migration is also faster in fine-grained than in coarse-grained materials. Fractographic studies show that the dimples on the coarse-grained specimen have large dimensions compared with that in the fine-grained material, indicating that heterogeneous deformation develops in the coarse-grained specimen during tension. Full article
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17 pages, 115015 KB  
Article
Superplastic Forming and Reaction Diffusion Bonding Process of Hollow Structural Component for Mg-Gd-Y-Zn-Zr Rare Earth Magnesium Alloy
by Peng Peng, Shaosong Jiang, Zhonghuan Qin and Zhen Lu
Metals 2022, 12(1), 152; https://doi.org/10.3390/met12010152 - 14 Jan 2022
Cited by 6 | Viewed by 3547
Abstract
This work fabricated a double hollow structural component of Mg-8.3Gd-2.9Y-0.8Zn-0.2Zr alloy by superplastic forming (SPF) and reaction-diffusion bonding (RDB). The superplastic characteristic and mechanical properties of Mg-8.3Gd-2.9Y-0.8Zn-0.2Zr alloy sheets at 250–450 °C were studied. Tensile tests showed that the maximum elongation of tensile [...] Read more.
This work fabricated a double hollow structural component of Mg-8.3Gd-2.9Y-0.8Zn-0.2Zr alloy by superplastic forming (SPF) and reaction-diffusion bonding (RDB). The superplastic characteristic and mechanical properties of Mg-8.3Gd-2.9Y-0.8Zn-0.2Zr alloy sheets at 250–450 °C were studied. Tensile tests showed that the maximum elongation of tensile specimens was about 1276.3% at 400 °C under a strain rate of 1 × 10−3 s−1. Besides, the effect of bonding temperature and interface roughness on microstructure and mechanical properties of the reaction diffusion-bonded joints with a Cu interlayer was investigated. With the increase of temperature, the diffusion coefficient of Cu increases, and the diffusion transition region becomes wider, leading to tightening bonding of the joint. However, the bonding quality of the joint will deteriorate due to grain size growth at higher temperatures. Shear tests showed that the highest strength of the joints was 152 MPa (joint efficiency = 98.7%), which was performed at 460 °C. Full article
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22 pages, 5591 KB  
Review
Opportunities and Issues in the Application of Titanium Alloys for Aerospace Components
by James C. Williams and Rodney R. Boyer
Metals 2020, 10(6), 705; https://doi.org/10.3390/met10060705 - 27 May 2020
Cited by 527 | Viewed by 46635
Abstract
The metal titanium (Ti) and its alloys have many attributes which are attractive as structural materials, but they also have one major disadvantage, high initial cost. Nevertheless, Ti and Ti alloys are used extensively in airframes, gas turbine engines (GTE), and rocket engines [...] Read more.
The metal titanium (Ti) and its alloys have many attributes which are attractive as structural materials, but they also have one major disadvantage, high initial cost. Nevertheless, Ti and Ti alloys are used extensively in airframes, gas turbine engines (GTE), and rocket engines (RE). The high cost is a deterrent, particularly in airframe applications, in that the other alloys it competes with are, for the most part, significantly lower cost. This is less of a concern for GTE and RE where the cost of titanium is closer to and sometimes even lower than some of the materials it competes with for these applications. In spacecraft the weight savings are so important that cost is a lesser concern. Ti and its alloys consist of five families of alloys; α-Ti, near α-alloys, α + β alloys, β-alloys, and Ti-based intermetallic compounds. The intermetallic compounds of primary interest today are those based on the compound TiAl which, at this time, are only used for engine applications because of their higher temperature capability. These TiAl-based compounds are used in a relatively low, but growing, amounts. The first production application was for low pressure turbine blades in the GE engine (GEnx) used on the Boeing 787, followed by the GE LEAP engine used on A-320neo and B-737MAX. These air foils are investment cast and machined. The next application is for the GE90X which will power the Boeing B-777X. These air foils will be made by additive manufacturing (AM). Unalloyed titanium and titanium alloys are typically melted by vacuum arc melting and re-melted either once (2X VAR) or twice (3X VAR); however a new and very different melting method (cold hearth melting) has recently become favored, mainly for high performance applications such as rotors in aircraft engines. This process resulted in higher quality ingots with a significant reduction in melt-related defects. Once melted and cast into ingots, the alloys can be processed using all the standard thermomechanical working and casting processes used for making components of other types of structural alloys. Because of their limited ductility, the TiAl-based intermetallic compounds are quite difficult to process using ordinary wrought methods. Consequently, the low-pressure turbine blades currently in service are investment cast and machined to net shape. The AM air foils will require minimal machining, which is an advantage. This paper describes some relatively recent developments as well as some issues and opportunities associated with the production and use of Ti and its alloys in aerospace components. Included are new Ti alloys, new applications of Ti alloys, and the current status of several manufacturing processes including a discussion of the promise and current reality of additive manufacturing as a potentially revolutionary method of producing Ti alloy components. Full article
(This article belongs to the Special Issue Titanium Alloys: Processing and Properties)
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12 pages, 3445 KB  
Article
Diffusion Bonding of 1420 Al–Li Alloy Assisted by Pure Aluminum Foil as Interlayer
by Fan Wu, Wei Chen, Bing Zhao, Hongliang Hou, Wenlong Zhou and Zhiqiang Li
Materials 2020, 13(5), 1103; https://doi.org/10.3390/ma13051103 - 2 Mar 2020
Cited by 16 | Viewed by 3358
Abstract
The Al–Li alloy is becoming popular for aerospace application owing to their low density, high specific strength, good corrosion resistance, etc. The diffusion bonding/superplastic forming (DB/SPF) structure of titanium alloy has been widely used in the aerospace industry. In order to broaden the [...] Read more.
The Al–Li alloy is becoming popular for aerospace application owing to their low density, high specific strength, good corrosion resistance, etc. The diffusion bonding/superplastic forming (DB/SPF) structure of titanium alloy has been widely used in the aerospace industry. In order to broaden the application of Al–Li alloy, it is necessary to develop its diffusion bonding and superplastic forming (DB/SPF) technology. In the present study, diffusion bonding of 1420 Al–Li alloy assisted by pure aluminum foil was conducted on Gleeble-3500 thermal simulation system under different bonding parameters, the results show that the bonding temperatures have direct influence on the interface microstructure and bond strength of joints. Meanwhile, when the pure aluminum interlayer was introduced into the diffusion bonding process, the alloying element diffusion across the bond can improve the interface integrity and the mechanical properties. The joint formation mechanism with interlayer was investigated in detail, the development and application of this method was explored. Full article
(This article belongs to the Section Manufacturing Processes and Systems)
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