Search Results (70)

Buildings of historic neighborhoods of Santiago de Chile are protected by a coating system composed of different layers of earth-based mortars, as part of a building culture that has been neglected and forgotten since the introduction of industrialized materials but still exists in many buildings. This study presents preliminary results from ongoing research that explores the hygroscopic capacity of this vernacular coating system and the impact of incorporating recent finishing layers into traditional construction practices. The investigation focuses on identifying materials and techniques typical of traditional Chilean coatings, highlighting their role in enhancing the durability of historic buildings, improving user comfort, and promoting environmental sustainability. It contributes to the conservation of historic buildings and their reuse, as well as to the health of its inhabitants, due to its contribution to hygrometric regulation. This article focuses on this last purpose, through the identification and characterization of the coating system and its finishing layer materials, and a comparative sorption/desorption test of four case studies with these vernacular coatings. This study began with the sample extraction in situ, followed by its observation and cataloguing. Stratigraphic and stereo microscope analysis of the finishing layers were carried out to identify them. The characterization of the finishing materials was performed using FTIR-ATR and SEM-EDX tests. The sorption/desorption test was performed with a set of original complete samples of the four case studies. Subsequently, another set was prepared with the removal of the finishing layers in order to compare their influence on the hygroscopicity of the coating systems. The results elucidate the variety of materials employed on the finishing layer of these coatings, which are often superimposed, revealing renovations and reparations over time. The influence of these finishing materials on sorption properties of the coating system (the scratch and base coats) is exposed by comparing the samples with and without them. Full article

Since composite materials are light and corrosion-resistant, they have replaced many traditional materials in the aviation and marine industries. Composite materials have the advantages of a much higher strength–weight ratio, lower maintenance requirements, and the ability to form complex shapes, such as bodies, compared to carbon steel. In this study, the mechanical properties of glass fiber reinforced (GFRP) and carbon fiber reinforced (CFRP) composite materials were investigated in marine applications in which composite materials had been used. In this study, 0/90 oriented twill weave eight-ply GFRP and eight-ply CFRP composite materials were used, incorporating the hand lay-up method and hot-pressing method. Seawater was taken from the Aegean Sea, Izmir Province (Balçova/İnciraltı), and had an average temperature of 22.43 °C. This seawater was kept in different containers for 30 days and 60 days (a total of 1440 h of keeping in seawater) with the intent to test the GFRP and CFRP composite samples separately. The produced CFRP and GFRP sheets were then cut with a wet (circular) saw in accordance with the standard procedure in the Composite Research and Testing Laboratory of the Dokuz Eylul University Department of Mechanical Engineering. Moisture retention percentages and Charpy impact tests were carried out. Then, three-point bending tests were carried out according to TS EN ISO 14125. The damage in the material was examined using a ZEISS Stereo Discovery.V12 imaging microscope (Oberkochen, Germany). The mechanical properties of CFRP- and GFRP-reinforced composite samples before and after aging were investigated using the Charpy impact test and three-point bending test. Then, the effects of the seawater environment on the mechanical properties of the CFRP and GFRP composite materials were evaluated by comparing the results. The aim was to better understand what kind of damage would occur in GFRP and CFRP composite materials given the effects of seawater and at what stages changes would occur in the mechanical properties of these materials. Moisture retention rates (%) in the tested samples after the Charpy impact test were 2.56% in GFRP and 0.47% in CFRP after 30 days. In the tested samples after the three-point bending test, these values were 1.41% in GFRP and 0.31% in CFRP after 30 days. Subsequent to the Charpy impact tests, the fracture toughness values of the CFRP samples tested at the 30 J impact energy level before aging in seawater conditions for 30 days or 60 days were found to be increased by 15.79% and 21.08%, respectively. The fracture toughness values of the GFRP tested at the 30 J impact energy level in dry conditions and kept in seawater for 30 days or 60 days were found to be 27.69% and 29.23%, respectively. The energy absorbed during the impact tests by the GFRP samples was higher than in the CFRP samples. This showed that the GFRP samples were more brittle. Subsequent to the three-point bending tests, the CFRP composite samples kept in seawater for periods of 30 days and 60 days showed changes in the modulus of elasticity of 7.48% and 7.46%, respectively, compared to the dry samples. The GFRP composite samples kept in seawater for periods of 30 days and 60 days showed changes in the modulus of elasticity of 7.015% and 11.53%, respectively, compared to the dry samples. The change in the modulus of elasticity was less in the CFRP samples than in GFRP. All of these results showed that the mechanical properties of CFRP were better than those of GFRP. Full article

Drought stress during the reproductive phase of sunflower can significantly reduce achene yield by affecting inflorescence size, nectar quality, and pollinator activity. This study aimed to analyze the morphological characteristics of the reproductive region, quantify nectar sugar components, and evaluate pollinator presence and pollination success in wild Helianthus species as an important genetic resource for breeding cultivated sunflowers under drought conditions. Morphological investigations were conducted during the flowering and achene development phases with a stereo microscope and calipers. Nectar sugar concentrations were analyzed via HPLC, and pollinator presence was monitored twice a week for two months. This study highlights the correlation between evaluated traits, emphasizing their importance as yield indicators. Significant differences were observed in reproductive characters, nectar quality, and pollination success among the species. Helianthus annuus and Helianthus argophyllus exhibited superior reproductive performance with high nectar sugar concentrations and larger inflorescences, enabling successful pollination and higher achene yield. In contrast, Helianthus debilis demonstrated lower reproductive efficiency, with a higher percentage of empty achenes. These findings provide valuable insights for breeding programs, highlighting H. argophyllus and H. annuus as promising genetic resources for developing sunflower genotypes with increased yield and improved floral traits adapted to drought conditions. Full article

Taking the titanium alloy wing–body connection joint at the rear beam of a certain type of aircraft as the research object, this study analyzed the failure mechanism and verified the structural safety of the wing–body connection joint under actual flight loads. Firstly, this study verified the validity of the loading system and the measuring system in the test system through the pre-test, and the repeatability of the test was analyzed for error to ensure the accuracy of the experimental data. Then, the test piece was subjected to 400,000 random load tests of flight takeoffs and landings, 100,000 Class A load tests, and ground–air–ground load tests, and the test piece fractured under the ground–air–ground load tests. Lastly, the mechanism analysis and structural safety verification of the fatigue fracture of the joints were carried out by using a stereo microscope and scanning electron microscope. The results show that fretting fatigue is the main driving force for crack initiation, and the crack shows significant fatigue damage characteristics in the stable growth stage and follows Paris’ law. Entering the final fracture region, the joint mainly experienced ductile fracture, with typical plastic deformation features such as dimples and tear ridges before fracture. The fatigue crack growth behavior of the joint was quantitatively analyzed using Paris’ law, and the calculated crack growth period life was 207,374 loadings. This result proves that the crack initiation life accounts for 95.19% of the full life cycle, which is much higher than the design requirement of 400,000 landings and takeoffs, indicating that the structural design of this test piece is on the conservative side and meets the requirements of aircraft operational safety. This research is of great significance in improving the safety and reliability of aircraft structures. Full article

Synthetic fibers are widely used in daily life due to their durability, elasticity, low cost, and ease of use. The textile industry is the primary source of synthetic microfibers, as these materials are mostly used in production processes. Globally, plastic pollution has been identified as a major environmental threat in this era, since plastics are not degradable but break down into smaller particles such as mesoplastics, microplastics, and microfibers. Synthetic microfiber pollution is a significant issue in aquatic ecosystems, including oceans and rivers, with laundry wastewater being a major source. This problem is particularly pressing in cities like Galle, Sri Lanka, where numerous tourist hotels are located. Despite the urgency, there has been a lack of scientific and systematic analysis to fully understand the extent of the issue. This study addresses this gap by analyzing the generation of microfibers from laundry activities at a selected hotel and evaluating the efficiency of a laundry wastewater filtration system. This study focused on a fully automatic front-loading washing machine (23 kg capacity) with a load of 12 kg of polyester–cotton blend serviettes (black and red). Samples (1 L each) were taken from both treated and untreated wastewater during four wash cycles, with a total of 100 L of water used for the process. The samples were filtered through a 100 μm sieve and catalytic wet oxidation along with density separation were employed to extract the microfibers, which were then collected on a membrane filter paper (0.45 μm). Microfibers were observed and analyzed for shapes, colors and sizes under a stereo microscope. Results revealed that untreated laundry wastewater contained 10,028.7 ± 1420.8 microfibers per liter (n = 4), while treated wastewater samples recorded 191.5 ± 109.4 microfibers per liter (n = 4). Most of the microfibers observed were black and white/transparent colors. Further analysis revealed that 1 kg of polyester–cotton blend fabric can generate 336,833 microfibers per wash, which was reduced to 6367 microfibers after treatment. The filtration unit recorded an impressive efficiency of 98.09%, indicating a remarkably high capacity for removing microfibers from wastewater. These findings highlight the potential of such filtration techniques to significantly reduce microfiber emissions from laundry wastewater, presenting a promising approach to mitigating environmental pollution from microfibers. Full article

This paper examined the surface morphology of maple and beech cut through by CO₂ laser under different angles relative to the wood grain: 0°, 15°, 30°, 45°, 60°, 75°, and 90°. In the analysis, stylus measurements, stereo-microscopic images, and chemical changes were considered. Laser uncovers more wood anatomical details, with enhanced clarity, when the cutting transitions from along the grain to across the grain. This is particularly noticeable in the earlywood and is more pronounced in maple compared to beech. The first tissue of earlywood was deeply ablated by the laser, leading to a wavy anatomical pattern, which is more visible for higher angles of laser cutting in relation to the wood grain. The anatomical structure of beech was more affected by carbonization in comparison to maple and had a significantly higher core roughness, Rk. For both species, the worst surface roughness occurred when cutting at 15°. In maple, the laser caused more degradation of the polysaccharides compared to beech, and this impact was particularly noticeable parallel to the grain rather than at a 90° angle. The degradation of hemicelluloses occurred in parallel with more advanced cellulose degradation for beech compared to maple and for cutting along the grain compared to across the grain. Structural changes in lignin, such as condensation processes, were observed for both species. Full article

This study aimed to evaluate the fracture resistance of endodontically treated molars restored with ceramic indirect restorations with and without cervical margin relocation. A total of 120 extracted human maxillary molars were used after MOD cavities preparations with the mesial boxes located 2 mm below CEJ. Specimens were randomly assigned to six groups according to the margin location of each indirect restoration type (n = 20); crown without CMR, crown with CMR, endocrown without CMR, endocrown with CMR, onlay without CMR, and onlay with CMR. Mesial proximal boxes of the MOD cavities were elevated with composite resin in cervical margin relocation groups. Each group was further divided according to indirect restoration material (n = 10); CEREC Tessera and Celtra Press. The specimens were subjected to fracture resistance testing in a universal testing machine. Fracture analysis was performed using stereo and scanning electron microscopes. Data were analyzed by using 3-way ANOVA, 1-way ANOVA and the Tukey HSD tests (α = 0.05). The mean fracture resistance values ranged between 2136.57 and 950.47 N. Significantly higher values were detected among Celtra Press than Cerec Tessera in crown restorations. Unrestorable fracture patterns were seen through all study groups. Crown restorations represented the best restorative option in terms of fracture resistance. Cervical margin relocation adversely affected fracture resistance. However, the material of the indirect restorations had no significant impact on fracture resistance. Full article

When calibrating a microscopic fringe projection profile system with a telecentric camera, the orthogonality of the camera causes an ambiguity in the positive and negative signs of its external parameters. A common solution is to introduce additional constraints, which often increase the level of complexity and the calibration cost. Another solution is to abandon the internal/external parameter models derived from the physical imaging process and obtain a numerically optimal projection matrix through the least squares solution. This paper proposes a novel calibration method, which derives a telecentric epipolar constraint model from the conventional epipolar constraint relationship and uses this constraint relationship to complete the stereo calibration of the system. On the one hand, since only the camera’s intrinsic parameters are needed, there is no need to introduce additional constraints. On the other hand, the solution is optimized based on the full consideration of the imaging model to make the parameters confirm to the physical model. Our experiments proved the feasibility and accuracy of the method. Full article

Corner detection is responsible for accurate camera calibration, which is an essential task for binocular three-dimensional (3D) reconstruction. In microscopic scenes, binocular 3D reconstruction has significant potential to achieve fast and accurate measurements. However, traditional corner detectors and calibration patterns (checkerboard) performed poorly in microscopic scenes due to the non-uniform illumination and the shallow depth of field of the microscope. In this paper, we present a novel method for detecting grid junction corners based on image segmentation, offering a robust alternative to the traditional checkerboard pattern. Model fitting was utilized to obtain the coordinates at a sub-pixel level. The procedures of the proposed method were elaborated, including image segmentation, corner prediction, and model fitting. The mathematical model was established to describe the grid junction. The experiment was conducted using both synthetic and real data and the experimental result shows that this method achieves high precision and is robust to image blurring, indicating this method is suitable for microscope camera calibration. Full article

This study was conducted to determine the indentation behavior of thin AlSi10Mg specimens manufactured using Selective Laser Melting (SLM) in the as-built condition along with two post-treatments, namely solution heat treatment and artificial aging. Four different thicknesses of 1.0 mm, 1.5 mm, 2 mm, and 2.5 mm of SLM specimens, with the different post-treatments, underwent standardized Rockwell hardness tests using a spherical indenter to determine their hardness values and assess the impression using a stereo microscope and scanning electron microscope (SEM). The as-built specimens showed a trend of smaller indentation depths with increasing specimen thickness, and finally creased with 0.1547 mm depth at 2.5 mm. However, the post-treatments altered the behavior of the specimens to a certain degree, giving larger experimental indentation depths of 0.2204 mm, 0.1962 mm, and 0.1798 mm at 1.0 mm, 1.5 mm, and 2.5 mm thickness, respectively, after solution heat treatment. Artificial aging showed a general decrease in indentation depth with increasing specimen thickness in contrast to solution treatment, and resulted in depths of 0.1888 mm and 0.1596 mm at 1.0 mm and 2.5 mm thickness. Furthermore, a material numerical model was made using stress–strain data on ANSYS Workbench to develop a predictive model for the indentation behavior of the specimens in contrast to experimentation. Under multi-linear isotropic hardening, the Finite Element Analysis (FEA) simulation produced indentation geometry with an average accuracy of 95.4% for the artificial aging series. Full article

The family Atyidae is composed of species whose existence has been known since the seventeenth century. Widely found in the Caribbean, Atya lanipes is a freshwater scraper/filter feeder shrimp with an amphidromous complex life cycle. Hunte (1975) described the first larval (zoeal) stage of the species. However, no scientific study has described the early larval development of this species after the first stage. This study aimed to document the early larval development of Atya lanipes under laboratory conditions and compare its larval development with other previously described species of the Atyidae family. Larval development was recorded by taking daily photos and videos of larval (zoeal) growth using a stereo microscope. Larvae were also preserved in ethanol for further morphological analysis. The results revealed that the best conditions for Atya lanipes development were 30 ppm water salinity, constant gentle aeration, and 27 °C water temperature. Nine stages were identified for the description of the early larval development of Atya lanipes. Early larval stages differ primarily in interstage larval size, the appearance and development of the telson, appendage appearance, growth of antennae and antennules, and pigmentation. The present contribution represents the first study that describes the larval development of the Caribbean shrimp Atya lanipes. Full article

Oleogels, which are traditionally utilized to reduce saturated and trans fats in bakery foods, have recently shown promising applications in non-bakery foods, particularly in the enhancement of their food texture and cooking qualities. This study investigates the impact of incorporating stearic acid-containing candelilla wax–groundnut oil oleogel in various proportions on the production of whole wheat pasta. Five different pasta samples were prepared by replacing water with oleogels in varying concentrations (2.5%, 5%, 10%, and 15%), and their physicochemical attributes were evaluated using a range of analytical methods for both cooked and uncooked pasta (like microscopy, colorimetry, dimensional analysis, texture, cooking qualities, moisture content, and FTIR). Significant differences in width, thickness, and color properties were observed between the control sample (0% oleogel) and those containing oleogel, with notable variations in surface texture and color intensities, particularly with the higher oleogel content (p < 0.05). Cooked pasta exhibited lower L* values and higher a* values than uncooked pasta. Stereo zoom microscope and field emission scanning electron microscope (FESEM) micrographs demonstrated a change in the pasta surface topology and microstructures. Dark spots on the pasta with greater oleogel concentrations (samples with 10% and 15% oleogel replacement) suggest the formation of starch–lipid complexes. Cooking induced pore formation, which was more pronounced when the oleogel content was increased, impacted the water absorption capacity, swelling index, and moisture content. The cooked samples exhibited higher moisture content and improved polymer network stability compared to the uncooked ones, indicating the potential of oleogel incorporation to modulate pasta properties in a concentration-dependent manner. These findings underscore the versatility of oleogels when their applications are diversified in non-bakery foods to enhance food texture and quality. Full article

The purpose of this study was to characterize in detail the reproductive strategy, course of embryogenesis, and development of larvae in three species of fishes of the genus Cichlasoma: the green terror (Andinoacara rivulatus), the red discus (Symphysodon discus), and the jaguar cichlid (Parachromis managuensis). Eggs for the study were obtained from five pairs of each species (300 eggs from each female) and incubated at 26 °C. The developing eggs were observed under a microscope (Carl Zeiss Stereo Discovery. V12 and Nikon 2000SE software (NIS-Elements F 4.30.01 64-bit) from fertilization to larval hatching until complete yolk-sac resorption. The largest average number of eggs per female was found in the jaguar cichlid ($\overline{\mathrm{x}}$ = 2991 eggs), a smaller average number of eggs was shown in the green terror ($\overline{\mathrm{x}}$ = 922 eggs), and the red discus showed the smallest average number of eggs ($\overline{\mathrm{x}}$ = 300 eggs). There were significant differences in the sizes of the eggs of the studied species: jaguar cichlid eggs were the smallest (1.060 ± 0.05 mm³), red discus eggs were larger (1.070 ± 0.07 mm³), and green terror eggs were the largest (1.365 ± 0.16 mm³). The embryogenesis time in the red discus was 2132 °H (82 Hpf), in the green terror it was 2158 °H (83 Hpf), and the longest in the jaguar cichlid was 2470 °H (87 Hpf). At the end of embryogenesis, the average size of the larvae after hatching was measured (red discus $\overline{\mathrm{x}}$ = 4.346 mm, green terror $\overline{\mathrm{x}}$ = 5.203 mm, and jaguar cichlid $\overline{\mathrm{x}}$ = 5.301 mm) and the time of yolk-sac resorption from the moment of hatching to the transition from endogenous to exogenous feeding was determined (jaguar cichlid 5 days, green terror 6 days, and red discus 3 days). The results of this study may contribute to the development of reproductive biotechnology for the studied fishes that could be used in aquaculture and, thus, help protect them in their natural habitats. Full article

Aluminum nitride (AlN) crystals with areas ranging from 1 mm² to 2 mm² were successfully grown through spontaneous nucleation at 1700 °C using a modified vapor transport method. In this approach, Cu–Al alloy served as the source of aluminum (Al), and nitrogen (N₂) was employed as the nitrogen source. The morphology and crystalline quality of the AlN crystals were characterized by a stereo microscope, Raman spectrometer, photoluminescence (PL) and secondary-ion mass spectrometry (SIMS). Deposited on the graphite lid, the as-grown AlN crystals exhibited both rectangular and hexagonal shapes, identified as m-plane and c-plane AlN, respectively, based on Raman spectroscopy. The full width half maximum (FWHM) values of E₂ (high) for the rectangular and hexagonal grains were measured to be 6.00 cm⁻¹ and 6.06 cm⁻¹, respectively, indicating high crystalline quality. However, PL and SIMS analysis indicated the presence of impurities associated with oxygen in the crystals. This paper elucidates the growth mechanism of the modified vapor transport method and highlights the role of the Cu–Al alloy in sustaining reactions at lower temperatures. The addition of copper (Cu) not only facilitates sustainable reactions, but also provides a novel perspective for the growth of AlN single crystals. Full article

This research aims to evaluate the physical and mechanical performance of three types of hybrid composites made of date palm (Phoenix dactylifera L.) (DP), additional layers of cotton (DP/C) and Kevlar fibres (DP/K). The fibres were formed into flat sheets and employed as reinforcement layers embedded in a polyester matrix. Three-layer and five-layer hybrid composites were created using the hand layup method. The layers have alternative longitudinal–transversal orientation. The composites were investigated for density, thickness swelling (TS), water absorption (WA), flexural strength and modulus of elasticity (MOE) properties. Moreover, the composites were subjected to cycles of water immersion, freezing and drying, and the changes in mass and mechanical performance were analysed before and after the cyclic testing. The hybrid composite with Kevlar as the inner layers displayed better physical and mechanical properties when compared to the other two hybrid composites. A stereo-microscopic investigation revealed that poor adhesion between the layers of composites contributed to a reduction in the mechanical properties of DP/C and DP hybrid composites. The DP/C composite had the highest thickness swelling and water absorption, with the water uptake more pronounced than in the cases of the other composites. The hybridisation of date palms with Kevlar fibres improved the properties of the hybrid composites. Full article