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Keywords = shot peen forming

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58 pages, 4707 KB  
Review
Vision-Based Artificial Intelligence for Adaptive Peen Forming: Sensing Architectures, Learning Models, and Closed-Loop Smart Manufacturing
by Sehar Shahzad Farooq, Abdul Rehman, Fuad Ali Mohammed Al-Yarimi, Sejoon Park, Jaehyun Baik and Hosu Lee
Sensors 2026, 26(8), 2460; https://doi.org/10.3390/s26082460 - 16 Apr 2026
Viewed by 686
Abstract
Peen forming is a dieless manufacturing process used to shape large, thin aerospace panels through controlled shot impacts that induce residual stresses and curvature. Despite long-standing industrial use, process monitoring still depends largely on indirect proxies such as Almen intensity and coverage, limiting [...] Read more.
Peen forming is a dieless manufacturing process used to shape large, thin aerospace panels through controlled shot impacts that induce residual stresses and curvature. Despite long-standing industrial use, process monitoring still depends largely on indirect proxies such as Almen intensity and coverage, limiting spatially resolved deformation assessment and hindering closed-loop control. In parallel, vision-based artificial intelligence (AI) has enabled adaptive monitoring and feedback in smart-manufacturing domains such as welding, additive manufacturing, and sheet forming. This review examines how such sensing and learning strategies can be transferred to adaptive peening forming. We compare six vision sensing modalities and assess major AI model families for surface mapping, temporal prediction, robustness, and deployment maturity. The synthesis shows that progress is primarily constrained by limited validated datasets, harsh in-cabinet sensing conditions, scarce closed-loop demonstrations, and weak validation on curved aerospace geometries. We conclude that the sensing and AI foundations for adaptive peen forming are already emerging, but industrial translation now depends on stronger experimental validation, standardized benchmarking, robust multi-sensor integration, and edge-capable feedback pipelines. Full article
(This article belongs to the Special Issue Artificial Intelligence and Sensing Technology in Smart Manufacturing)
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26 pages, 17902 KB  
Article
Improvement of the Surface Layer Properties of 316L Stainless Steel Produced by DMLS Through the Use of a Shot Peening Process
by Kazimiera Dudek, Dominika Grygier and Lidia Gałda
Materials 2026, 19(7), 1293; https://doi.org/10.3390/ma19071293 - 24 Mar 2026
Cited by 1 | Viewed by 497
Abstract
Additive-manufactured (AM) 316L stainless steel, produced via direct metal laser sintering (DMLS) and characterised by a surface topography of high irregularities and tensile residual stresses with specific anisotropy, was subjected to milling and shot peening. The milling process caused a reduction in surface [...] Read more.
Additive-manufactured (AM) 316L stainless steel, produced via direct metal laser sintering (DMLS) and characterised by a surface topography of high irregularities and tensile residual stresses with specific anisotropy, was subjected to milling and shot peening. The milling process caused a reduction in surface topography parameters, but tensile residual stresses increased significantly. The shot peening process was carried out according to the full factorial design 32 and technological parameters such as a shot diameter in the range of 1-3 mm and an air supply pressure between 0.2 and 0.6 MPa. As a result of the experiments and the analysis, reduced surface topography was achieved, and a favourable residual stress state was formed with compressive stresses. The mechanism of the changes was demonstrated via microstructure observation and statistical models obtained by mathematical analysis. Full article
(This article belongs to the Special Issue High-Strength Lightweight Alloys: Innovations and Advancements)
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17 pages, 10354 KB  
Article
Surface Nanocrystallization and Strengthening Mechanisms of SLM 316L Stainless Steel Induced by Shot Peening
by Hongfeng Luo and Yuxuan Wang
Metals 2026, 16(2), 186; https://doi.org/10.3390/met16020186 - 4 Feb 2026
Viewed by 737
Abstract
To address surface defects and enhance the wear resistance of 316L stainless steel parts fabricated by Selective Laser Melting (SLM), this study applied shot peening (SP) surface treatment to the SLM-processed samples. Ball-on-disk tribological tests were systematically conducted under water-lubricated conditions to investigate [...] Read more.
To address surface defects and enhance the wear resistance of 316L stainless steel parts fabricated by Selective Laser Melting (SLM), this study applied shot peening (SP) surface treatment to the SLM-processed samples. Ball-on-disk tribological tests were systematically conducted under water-lubricated conditions to investigate the evolution of surface morphology, microstructure, microhardness, and tribological performance before and after SP. The results indicate that SP induced severe plastic deformation in the surface layer, effectively refining the coarse columnar crystals and melt pool structures characteristic of SLM, and forming a crystalline hardened layer with a depth of 70–80 μm. Consequently, the surface microhardness increased by 21.97% compared to the un-peened samples. Under loads of 20 N and 30 N, the coefficient of friction (COF) of the SP-treated samples decreased by 16.36% and 12.4%, while the wear rate was reduced by 17.09% and 14.9%, respectively. In this load range, the samples primarily exhibited uniform plowing and localized adhesive wear, demonstrating significantly improved resistance to plastic deformation and crack initiation. However, when the load increased to 40 N, intense stress and thermal effects diminished the strengthening benefits of SP, resulting in no significant difference in tribological performance between the SP-treated and untreated samples. At this stage, the dominant wear mechanism transitioned to severe plastic deformation, extensive delamination, and thermally induced adhesion. Full article
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17 pages, 7895 KB  
Article
Electrolytic-Plasma Nitriding of Austenitic Stainless Steels After Mechanical Surface Treatment
by Bauyrzhan Rakhadilov, Zarina Satbayeva, Almasbek Maulit, Nurlat Kadyrbolat and Anuar Rustemov
Crystals 2025, 15(11), 992; https://doi.org/10.3390/cryst15110992 - 17 Nov 2025
Cited by 2 | Viewed by 1065
Abstract
In this work, the effect of preliminary mechanical surface treatment on the kinetics of formation, phase composition, and functional properties of the nitrided layer during electrolytic-plasma nitriding (EPN) of austenitic stainless steel 12Kh18N10T (AISI 321) was investigated. In contrast to traditional approaches, for [...] Read more.
In this work, the effect of preliminary mechanical surface treatment on the kinetics of formation, phase composition, and functional properties of the nitrided layer during electrolytic-plasma nitriding (EPN) of austenitic stainless steel 12Kh18N10T (AISI 321) was investigated. In contrast to traditional approaches, for the first time, this work establishes a direct correlation between the degree of surface deformation induced by shot peening and the formation of the expanded austenite (γN) phase under low-temperature plasma conditions. Quantitative X-ray phase analysis revealed a lattice parameter expansion of Δa/a0 ≈ 1.4–1.8% and a gradual transformation of γ-Fe → γN without the formation of CrN nitrides at moderate intensity of preliminary treatment. According to SEM/EDS data and microhardness profiles, a multilayer structure was formed, consisting of a thin surface film of CrN/Fe4N, a developed γN zone with a thickness of 12–15 µm, and a stable austenitic γ-Fe matrix. The surface microhardness increases to 880 ± 20 HV, while the friction coefficient decreases to 0.35–0.40, corresponding to a wear reduction of approximately 55% compared to the initial steel. The results provide a mechanistic understanding of nitrogen diffusion through defect-enriched subsurface layers and show that optimal preliminary deformation (d = 6 mm, v = 40 Hz, t = 20 min) promotes controlled formation of the γN phase with minimal lattice instability. The proposed combined approach—shot peening + EPN—is an effective method for producing wear- and corrosion-resistant surfaces of austenitic steels under atmospheric plasma conditions. Full article
(This article belongs to the Section Inorganic Crystalline Materials)
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25 pages, 3250 KB  
Article
A Thermoelastic Plate Model for Shot Peen Forming Metal Panels Based on Effective Torque
by Conor Rowan
J. Manuf. Mater. Process. 2025, 9(8), 280; https://doi.org/10.3390/jmmp9080280 - 15 Aug 2025
Cited by 1 | Viewed by 1625
Abstract
A common technique used in factories to shape metal panels is shot peen forming, where the panel is sprayed with a high-velocity stream of small steel pellets called “shot.” The impacts between the hard steel shot and the softer metal of the panel [...] Read more.
A common technique used in factories to shape metal panels is shot peen forming, where the panel is sprayed with a high-velocity stream of small steel pellets called “shot.” The impacts between the hard steel shot and the softer metal of the panel cause localized plastic deformation, which is used to improve the fatigue properties of the material’s surface. The residual stress distribution imparted by impacts also results in bending, which suggests that a torque is associated with it. In this paper, we model shot peen forming as the application of spatially varying torques to a Kirchhoff plate, opting to use the language of thermoelasticity in order to introduce these torque distributions. First, we derive the governing equations for the thermoelastic thin plate model and show that only a torque-type resultant of the temperature distribution shows up in the bending equation. Next, to calibrate from the shot peen operation, an empirical “effective torque” parameter used in the thermoelastic model, a simple and non-invasive test is devised. This test relies only on measuring the maximum displacement of a uniformly shot peened plate as opposed to characterizing the residual stress distribution. After discussing how to handle the unconventional fully free boundary conditions germane to shot peened plates, we introduce an approach to solving the inverse problem whereby the peening distribution required to obtain a specified plate contour can be obtained. Given that the relation between shot peen distributions and bending displacements at a finite set of points is non-unique, we explore a regularization of the inverse problem which gives rise to shot peen distributions that match the capabilities of equipment in the factory. In order to validate our proposed model, an experiment with quantified uncertainty is designed and carried out which investigates the agreement between the predictions of the calibrated model and real shot peen-forming operations. Full article
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20 pages, 15551 KB  
Article
Effect of Microstructure and Compressive Residual Stress on the Fatigue Performance of AISI 4140 Steel with QPQ Salt-Bath Nitro-Carburizing
by Hao Chen, Tai-Cheng Chen, Hsiao-Hung Hsu and Leu-Wen Tsay
Materials 2025, 18(9), 1995; https://doi.org/10.3390/ma18091995 - 28 Apr 2025
Cited by 8 | Viewed by 2907
Abstract
Quench–polish–quench (QPQ) nitro-carburizing of AISI 4140 steel in a salt bath was performed in this study. Nitro-carburizing in a salt bath enhanced the formation of Fe-nitride on the outer surface layer. Moreover, the oxidizing treatment formed a thin oxide layer decorated on the [...] Read more.
Quench–polish–quench (QPQ) nitro-carburizing of AISI 4140 steel in a salt bath was performed in this study. Nitro-carburizing in a salt bath enhanced the formation of Fe-nitride on the outer surface layer. Moreover, the oxidizing treatment formed a thin oxide layer decorated on the outermost part of the QPQ-treated sample. The dense compound layer formed after nitro-carburizing in a salt bath consisted of refined granular Fe3N and transformed to Fe2N after post-oxidation treatment. Micro-shot peening (MSP) was adopted before QPQ treatment to increase the treated steel’s fatigue performance. The results indicated that MSP slightly increased the thickness of the compound layer and harden depth, but it had little effect on improving the fatigue strength/life of the QPQ-treated sample (SP-QPQ) compared to the non-peened one (NP-QPQ). A deep compressive residual stress (CRS) field (about 200 μm) and a hard nitrided layer showed a noticeable improvement in the fatigue performance of the QPQ-treated ones relative to the 4140 substrates tempered at 570 °C. The ease of slipping or deforming on the substrate surface was responsible for its poor resistance to fatigue failure. The cracking and spalling of the brittle surface layer were the causes for the fatigue crack initiation and growth of all of the QPQ-treated samples fatigue-loaded at/above 875 MPa. It was noticed that fatigue crack initiation at the subsurface inclusions was more likely to occur in the SP-QPQ sample fatigue-loading at 850 MPa or slightly above the fatigue limit. Full article
(This article belongs to the Special Issue Microstructure Engineering of Metals and Alloys, 3rd Edition)
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24 pages, 7784 KB  
Article
Enhancing the Surface Integrity of a Laser Powder Bed Fusion Inconel 718 Alloy by Tailoring the Microstructure and Microrelief Using Various Finishing Methods
by Dmytro Lesyk, Bohdan Mordyuk, Silvia Martinez, Vitaliy Dzhemelinskyi, Daniel Grochala, Andriy Kotko and Aitzol Lamikiz
Coatings 2025, 15(4), 425; https://doi.org/10.3390/coatings15040425 - 3 Apr 2025
Cited by 8 | Viewed by 3477
Abstract
Heat-performance nickel-based superalloys are commonly applied in various critical industries. In this work, test samples in the form of turbine blades were manufactured by means of laser powder bed fusion (LPBF) 3D technology. This research focused on comparison of the influences of various [...] Read more.
Heat-performance nickel-based superalloys are commonly applied in various critical industries. In this work, test samples in the form of turbine blades were manufactured by means of laser powder bed fusion (LPBF) 3D technology. This research focused on comparison of the influences of various surface finishing methods. The mechanical surface post-processing of the LPBF-manufactured Inconel 718 alloy samples consisted of ultrasonic impact treatment (UIT), ultrasonic shot peening (USP), shot peening (SP), and barrel finishing (BF). The surface microrelief was evaluated using a high-precision laser profilometer, while the microstructural features were studied by light optical microscopy (LOM), scanning/transmission electron microscopy (SEM/TEM), and X-ray diffraction (XRD). Potentiodynamic polarization tests were also conducted to compare the surface finishing methods in terms of corrosion resistance improvement of the LPBF-manufactured 718 alloy samples. The effects of the surface microstructure and hardening intensity in combination with residual stresses and surface relief coupled with roughness profile shapes on the room temperature corrosion behavior of plastically deformed 718 alloy specimens manufactured by LPBF were studied. The corrosion rate (CR) of the LPBF-manufactured samples was reduced after post-processing: BF (~16 μm/year), USP (~15 μm/year), SP (~6.5 μm/year), and UIT (~5.5 μm/year). The experimental trends also agreed well with the theoretical trends of uniform corrosion of the studied alloy. Full article
(This article belongs to the Special Issue Laser Surface Engineering: Technologies and Applications)
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16 pages, 4954 KB  
Article
Equal–Additive–Subtractive Remanufacturing Integrated Laser Directed Energy Deposition with Shot Peening and Machining Induced High Performance of Plunger Rod
by Xiaoyu Zhang, Wenping Mou, Dichen Li, Shaowei Zhu, Lianyu Li, Qiaochu Liu and Sheng Huang
Materials 2024, 17(19), 4767; https://doi.org/10.3390/ma17194767 - 28 Sep 2024
Cited by 1 | Viewed by 1816
Abstract
The number of easily destroyed parts with high value is increasing in industry, and green remanufacture engineering is now mainstream in this new and expanding industrial field. Equal–additive–subtractive manufacturing, as a new technology that combines strengthening technology, additive manufacturing, and machining technology has [...] Read more.
The number of easily destroyed parts with high value is increasing in industry, and green remanufacture engineering is now mainstream in this new and expanding industrial field. Equal–additive–subtractive manufacturing, as a new technology that combines strengthening technology, additive manufacturing, and machining technology has great potential for development in the area of remanufacturing. Aiming at the damage characteristics of a plunger rod, this paper carries out a study about the repair technology by equal–additive–subtractive manufacturing of laser-directed energy deposition and shot peening. It was found that the microstructure of the materials repaired by equal–additive–subtractive technology is finer and the tensile strength can reach 100.4% of the base material. The surface residual stress of cladding materials changes from tensile stress to compressive stress, which reduces forming defects. Equal–additive–subtractive manufacturing has great significance in expanding the application of hybrid manufacturing and promoting green remanufacturing of parts with high value. Full article
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17 pages, 6345 KB  
Article
Enhancing the Tribological Properties of Bearing Surfaces in Hip Arthroplasty by Shot-Peening the Metal Surface
by Chavarat Jarungvittayakon, Anak Khantachawana and Paphon Sa-ngasoongsong
Lubricants 2024, 12(8), 278; https://doi.org/10.3390/lubricants12080278 - 3 Aug 2024
Cited by 3 | Viewed by 3056
Abstract
Total hip arthroplasty (THA) is a surgical procedure for patients with pain and difficulty walking due to hip osteoarthritis. In primary THA, the acetabulum and femoral head are replaced by a prosthesis where the modular femoral head and inner liner of the acetabulum [...] Read more.
Total hip arthroplasty (THA) is a surgical procedure for patients with pain and difficulty walking due to hip osteoarthritis. In primary THA, the acetabulum and femoral head are replaced by a prosthesis where the modular femoral head and inner liner of the acetabulum form the bearing surface. The most popular bearing surface used in the United States, metal-on-polyethylene, consists of a cobalt–chromium molybdenum (CoCrMo) alloy femoral head that articulates with a polyethylene acetabular liner, typically made of highly cross-linked polyethylene. While successful in most cases, THA sometimes fails, commonly from aseptic loosening due to the wear debris of polyethylene. Fine-particle shot peening (FPSP) is a simple method for enhancing the mechanical properties and surface properties of metal, including reducing friction and enhancing the lubrication properties of the metal surface. In this study, we applied FPSP to the CoCr in the femoral head of a hip prosthesis to improve its surface properties and conducted experiments with pin-on-disc tribometers using CoCr as a pin and highly cross-linked polyethylene as a disc to mimic the THA implant. The results show that FPSP significantly enhances the tribological properties of the CoCr surface, including lubrication; decreases the friction coefficient; and decreases the polyethylene wear volume. Full article
(This article belongs to the Special Issue Biomechanics and Tribology)
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19 pages, 11624 KB  
Article
Effect of Ultrasonic Shot Peening on Microstructure and Corrosion Properties of GTA-Welded 304L Stainless Steel
by Hyunhak Cho, Young-Ran Yoo and Young-Sik Kim
Crystals 2024, 14(6), 531; https://doi.org/10.3390/cryst14060531 - 4 Jun 2024
Cited by 9 | Viewed by 2988
Abstract
Austenitic stainless steels used in structural applications suffer from stress corrosion cracking due to residual stresses during welding. Much research is being conducted to prevent the stress corrosion cracking of austenitic steels by inducing compressive residual stresses. One method is ultrasonic shot peening [...] Read more.
Austenitic stainless steels used in structural applications suffer from stress corrosion cracking due to residual stresses during welding. Much research is being conducted to prevent the stress corrosion cracking of austenitic steels by inducing compressive residual stresses. One method is ultrasonic shot peening (USP), which is used to apply compressive stress by modifying the mechanical properties of the material’s surface. In this study, 304L stainless steel was butt-welded by gas tungsten arc welding (GTAW) and subsequently subjected to compressive residual stress to a depth of 1 mm from the surface by a USP treatment. The influence of USP on microstructural changes in the base metal, the HAZ and weldment, and the corrosion properties was analyzed. A microstructural analysis was conducted using SEM-EDS, XRD, and EBSD methods alongside residual stress measurements. The surface and cross-sectional corrosion behavior was evaluated and analyzed using a potentiodynamic polarization test, electrochemical impedance spectroscopy (EIS) measurements, a double-loop electrochemical potentiokinetic reactivation (DL-EPR) test, and an ASTM A262 Pr. C test. The surface was deformed and roughened by the USP. The deformed areas formed crevices, and the inside of the crevices contained some cracks. The crevices and internal cracks caused pitting, which reduced the resistance of the passivation film. The cross-section was subjected to compressive residual stress to a depth of 1 mm from the surface, and the outermost area of the cross-section had fine grain refinement, forming a solid passivation film that improved the corrosion resistance. Full article
(This article belongs to the Special Issue Plastic Deformation and Welding on Metallic Materials)
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29 pages, 11863 KB  
Review
Effects of Shot Peening and Electropolishing Treatment on the Properties of Additively and Conventionally Manufactured Ti6Al4V Alloy: A Review
by Wojciech Okuniewski, Mariusz Walczak and Mirosław Szala
Materials 2024, 17(4), 934; https://doi.org/10.3390/ma17040934 - 17 Feb 2024
Cited by 32 | Viewed by 6517
Abstract
This literature review indicates that the basic microstructure of Ti6Al4V is bimodal, consisting of two phases, namely α + β, and it occurs after fabrication using conventional methods such as casting, plastic forming or machining processes. The fabrication of components via an additive [...] Read more.
This literature review indicates that the basic microstructure of Ti6Al4V is bimodal, consisting of two phases, namely α + β, and it occurs after fabrication using conventional methods such as casting, plastic forming or machining processes. The fabrication of components via an additive manufacturing process significantly changes the microstructure and properties of Ti6Al4V. Due to the rapid heat exchange during heat treatment, the bimodal microstructure transforms into a lamellar microstructure, which consists of two phases: α′ + β. Despite the application of optimum printing parameters, 3D printed products exhibit typical surface defects and discontinuities, and in turn, surface finishing using shot peening is recommended. A literature review signalizes that shot peening and electropolishing processes positively impact the corrosion behavior, the mechanical properties and the condition of the surface layer of conventionally manufactured titanium alloy. On the other hand, there is a lack of studies combining shot peening and electropolishing in one hybrid process for additively manufactured titanium alloys, which could synthesize the benefits of both processes. Therefore, this review paper clarifies the effects of shot peening and electropolishing treatment on the properties of both additively and conventionally manufactured Ti6Al4V alloys and shows the effect process on the microstructure and properties of Ti6Al4V titanium alloy. Full article
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29 pages, 5218 KB  
Review
Analyzing the Tribology of High-Entropy Alloys Prepared by Spark Plasma Sintering
by Chika Oliver Ujah, Daramy Vandi Von Kallon and Victor S. Aigbodion
Metals 2024, 14(1), 27; https://doi.org/10.3390/met14010027 - 25 Dec 2023
Cited by 13 | Viewed by 3926
Abstract
High-entropy alloys (HEAs) are prospective advanced materials for the production of components that operate at high, severe friction and in high-temperature environments. This is because they possess unique properties requisite for such applications. Hence, this study was aimed at reviewing most recent publications [...] Read more.
High-entropy alloys (HEAs) are prospective advanced materials for the production of components that operate at high, severe friction and in high-temperature environments. This is because they possess unique properties requisite for such applications. Hence, this study was aimed at reviewing most recent publications on the tribological characteristics of HEAs processed with spark plasma sintering (SPS). The choice of SPS was because it impacts alloys with a homogenous microstructure, high wear resistance, densely packed grains, and nanocrystalline microstructure. The resource materials for this study were obtained from the Scopus-indexed journal/Google Scholar website for articles published within the last five years. From the study, it was observed that HEAs have good tribological properties which permit their prospective usage in the production of strength-demanding, wear-demanding, and temperature-demanding components. The addition of BCC-forming and FCC-forming elements would help in improving the wear properties of HEAs. It was also observed from the literature that the incorporation of post-processing treatment, laser cladding, shot peening, or the coating of SPSed composites would increase the effective performance and durability of HEAs prepared with SPS. Full article
(This article belongs to the Special Issue High Entropy Alloys: Trends and Future Challenges)
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14 pages, 15750 KB  
Article
Mitigating Stress Corrosion Cracking of 304L and 316L Laser Welds in a Salt Spray through Micro-Shot Peening
by Chia-Ying Kang, Tai-Cheng Chen, Ren-Kae Shiue and Leu-Wen Tsay
Metals 2023, 13(11), 1898; https://doi.org/10.3390/met13111898 - 16 Nov 2023
Cited by 6 | Viewed by 3142
Abstract
Two austenitic stainless steel (ASS) plates, 304L and 316L, were cold-rolled (304R and 316R) with a 10% reduction in thickness and then subjected to laser welding. Cold rolling caused slight surface hardening and introduced residual tensile stress into the ASS plates. The susceptibility [...] Read more.
Two austenitic stainless steel (ASS) plates, 304L and 316L, were cold-rolled (304R and 316R) with a 10% reduction in thickness and then subjected to laser welding. Cold rolling caused slight surface hardening and introduced residual tensile stress into the ASS plates. The susceptibility to stress corrosion cracking (SCC) of the welds (304RW and 316RW) was determined using the U-bend test pieces in a salt spray. To highlight the stress concentration at the weld’s fusion boundary (FB), the top weld reinforcement was not ground off before bending. Moreover, micro-shot peening (MSP) was performed to mitigate the SCC of the welds by imposing high residual compressive stress and forming a fine-grained structure. Cold rolling increased the susceptibility of the 304R specimen to pitting corrosion and intergranular (IG) microcracking. Moreover, pitting corrosion and SCC were found more often at the FBs of the 304RW. The corrosion pits of the peened 304RW (304RWSP) were finer but greater in amount than the those of the un-peened one. The results also indicated that the 316L ASS welds with MSP were resistant to the incidence of pitting corrosion and SCC in a salt spray. The better reliability and longer service life of dry storage canisters could be achieved by using 316L ASS for the construction and application of MSP on it. Full article
(This article belongs to the Special Issue Fusion Welding)
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15 pages, 11334 KB  
Article
The Microstructure Evolution and Formation Mechanism of Gradient Nanostructure Prepared on CrCoNi Medium-Entropy Alloy
by Dou Ning, Wenjie Lu, Xian Luo, Yanqing Yang and Bin Huang
Nanomaterials 2023, 13(13), 1954; https://doi.org/10.3390/nano13131954 - 27 Jun 2023
Cited by 1 | Viewed by 2262
Abstract
An equiatomic CrCoNi medium-entropy alloy was subjected to high-energy shot peening (HESP) to fabricate a gradient nanostructure (GNS) in this work. The microstructures of the GNS samples at different depths within the deformed layer were thoroughly investigated. The microstructure exhibited a transformation from [...] Read more.
An equiatomic CrCoNi medium-entropy alloy was subjected to high-energy shot peening (HESP) to fabricate a gradient nanostructure (GNS) in this work. The microstructures of the GNS samples at different depths within the deformed layer were thoroughly investigated. The microstructure exhibited a transformation from unstressed coarse grains to deformed coarse grains, followed by the formation of ultrafine grains, and ultimately reaching a final nanocrystalline structure with a uniform size of approximately 50 nm. Detailed structural analysis indicated that the deformation process was primarily influenced by the interaction between dislocations and deformation twins, which was attributed to the low stacking fault energy (SFE) of the alloy. The nanocrystalline mechanism was divided into three stages. In the coarse-grained deformation stage, the dislocation band divided twin/matrix lamellae into sub-segments, and the cross twin divided coarse grains into ultrafine grains simultaneously. In the ultrafine grain deformation stage, dislocations were arranged around the deformation twins in order to break the twins to form incoherent boundaries, destroying the coherent relationship between the twin and matrix. Finally, in the nanocrystalline deformation stage, the nanocrystalline structure was further divided into smaller segments to accommodate additional strains through the interaction between dislocations and twins. Full article
(This article belongs to the Section Nanofabrication and Nanomanufacturing)
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12 pages, 9288 KB  
Article
Surface Characteristic and Friction Behavior of Plasma Sprayed FeCoNiCrMo0.2 High Entropy Alloy Coatings on BS960 High-Strength Steel with Subsequent Shot Peening Treatment
by Zheng Yang and Chuanhai Jiang
Coatings 2023, 13(2), 303; https://doi.org/10.3390/coatings13020303 - 29 Jan 2023
Cited by 14 | Viewed by 2544
Abstract
The FeCoNiCrMo0.2 high entropy alloy coatings were deposited on BS960 high strength steel by plasma spraying method with four different current intensities (250 A, 350 A, 450 A, 550 A). These coatings were then subjected to a subsequent micro-shot peening treatment. Surface [...] Read more.
The FeCoNiCrMo0.2 high entropy alloy coatings were deposited on BS960 high strength steel by plasma spraying method with four different current intensities (250 A, 350 A, 450 A, 550 A). These coatings were then subjected to a subsequent micro-shot peening treatment. Surface characteristics including surface morphology, microhardness and phase composition were characterized, and the wear resistance of the coatings was assessed by reciprocal friction and wear tests. The results showed that the high entropy alloy coatings had FCC structure. XRD results showed that no new phase was formed during the spraying process. At the same time, shot peening treatment could effectively improve the hardness of the coating surface. Under the four processes, the coating surface prepared with the current intensity of 350 A had the highest microhardness and uniformity before and after shot peening, and the hardness values were 473 ± 10.21 and 504 ± 8.62 HV0.2, respectively. The friction and wear test results showed that the friction coefficients of the four coatings were close to each other at 10 N load, which was about 0.4. When the test load reached 25 N, the friction coefficient of the coating with current intensity of 350 A was lower, and it showed better friction performance. After shot peening, the friction coefficient of the four coatings further decreased to about 0.3 under 10 N loading due to the existence of hardened surface layer. When the test load reached 25 N, the hardened layer would be worn through and the friction coefficient would suddenly rise. Under the 25 N test load, the hardened layer of the high-entropy alloy coating with current intensity of 350 A illustrated better friction resistance. Full article
(This article belongs to the Special Issue Friction, Wear, Lubrication and Mechanics of Surfaces and Interfaces)
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