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Keywords = rubber–clay mixtures

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20 pages, 4701 KB  
Article
Effect of Rubber Particle Size and Content on the Mechanical Properties of Rubber–Clay Mixtures Solidified by EICP
by Qiang Ma, Meng Li, Chen Zeng, Hang Shu, Lei Xi, Yue Tao and Xuesong Lu
Materials 2025, 18(15), 3429; https://doi.org/10.3390/ma18153429 - 22 Jul 2025
Cited by 1 | Viewed by 860
Abstract
Using the enzyme-induced carbonate precipitation (EICP) technique to solidify rubber and clay mixtures as lightweight backfill is a feasible way to reduce waste tire impacts and boost rubber recycling in geotech engineering. In this study, a comprehensive laboratory investigation, including triaxial compression, oedometer, [...] Read more.
Using the enzyme-induced carbonate precipitation (EICP) technique to solidify rubber and clay mixtures as lightweight backfill is a feasible way to reduce waste tire impacts and boost rubber recycling in geotech engineering. In this study, a comprehensive laboratory investigation, including triaxial compression, oedometer, permeability, and nuclear magnetic resonance (NMR) tests, was conducted on EICP-reinforced rubber particle solidified clay (hereafter referred to as EICP-RC solidified clay) to evaluate the effects of rubber particle content and size on the mechanical behavior of the improved soil under various solidification conditions and to elucidate the solidification mechanism. The results show that although rubber particles inhibit EICP, they significantly enhance the mechanical properties of the samples. The addition of 5% rubber particles (rubber A) increased cohesion by 11% and the internal friction angle by 18% compared to EICP-treated clay without rubber. Additionally, incorporating smaller-sized tire particles facilitated pore filling, resulting in lower compression and swelling indices and reduced permeability coefficients, making these materials suitable for use behind retaining walls and in embankment construction. Full article
(This article belongs to the Section Construction and Building Materials)
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19 pages, 5048 KB  
Article
Stabilization of Clay Subgrade Soil by Using Waste Foundry Sand with a Geogrid
by Qais Sahib Banyhussan, Jaafar Abdulrazzaq, Ahmed A. Hussein, Anmar Dulaimi, Jorge Miguel de Almeida Andrade and Luís Filipe Almeida Bernardo
CivilEng 2025, 6(2), 26; https://doi.org/10.3390/civileng6020026 - 10 May 2025
Cited by 1 | Viewed by 2117
Abstract
Various stabilizers, such as jute, gypsum, rice-husk ash, fly ash, cement, lime, and discarded rubber tires, are commonly used to improve the shear strength and overall characteristics of clay subgrade soil. In this study, waste foundry sand (WFS) is utilized as a stabilizing [...] Read more.
Various stabilizers, such as jute, gypsum, rice-husk ash, fly ash, cement, lime, and discarded rubber tires, are commonly used to improve the shear strength and overall characteristics of clay subgrade soil. In this study, waste foundry sand (WFS) is utilized as a stabilizing material to enhance the properties of clay subgrade soil and strengthen the bond between clay subgrade soil and subbase material. The materials employed in this study include Type B subbase granular materials, clay subgrade soil, and 1100 Biaxial Geogrid for reinforcement. The clay subgrade soil was collected from the airport area in the Al-Muthanna region of Baghdad. To evaluate the effectiveness of WFS as a stabilizer, soil specimens were prepared with varying replacement levels of 0%, 5%, 10%, and 15%. This study conducted a Modified Proctor Test, a California Bearing Ratio test, and a large-scale direct shear test to determine key parameters, including the CBR value, maximum dry density, optimum moisture content, and the compressive strength of the soil mixture. A specially designed large-scale direct shear apparatus was manufactured and utilized for testing, which comprised an upper square box measuring 20 cm × 20 cm × 10 cm and a lower rectangular box with dimensions of 200 mm × 250 mm × 100 mm. The findings indicate that the interface shear strength and overall properties of the clay subgrade soil improve as the proportion of WFS increases. Full article
(This article belongs to the Section Geotechnical, Geological and Environmental Engineering)
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15 pages, 3364 KB  
Article
Predictive Modeling of Shear Strength of Enzyme-Induced Calcium Carbonate Precipitation (EICP)-Solidified Rubber–Clay Mixtures Using Machine Learning Algorithms
by Qiang Ma, Meng Li, Hang Shu and Lei Xi
Polymers 2025, 17(7), 976; https://doi.org/10.3390/polym17070976 - 3 Apr 2025
Cited by 1 | Viewed by 879
Abstract
The development of reliable predictive models for soil behavior represents a crucial advancement in geotechnical engineering, particularly for optimizing material compositions and reducing experimental uncertainties. Traditional experimental approaches for determining the optimal rubber particle size and content are often resource-intensive, time-consuming, and subject [...] Read more.
The development of reliable predictive models for soil behavior represents a crucial advancement in geotechnical engineering, particularly for optimizing material compositions and reducing experimental uncertainties. Traditional experimental approaches for determining the optimal rubber particle size and content are often resource-intensive, time-consuming, and subject to significant variability. In this study, the shear strength of clay mixed with rubber particles solidified by the Enzyme-Induced Calcium Carbonate Precipitation (EICP) technique was investigated and predictively modeled using a machine learning algorithm. The effects of different rubber contents and particle sizes on the shear strength of the clay were analyzed experimentally, and a hybrid model of a convolutional neural network (CNN) and long short-term memory (LSTM) network optimized based on the crown porcupine optimization (CPO) algorithm was proposed to predict the shear strength of the EICP-treated clay mixed with rubber particles. The superiority of the CPO-CNN-LSTM model in predicting shear strength was verified by comparing multiple machine learning algorithms. The results show that the addition of rubber particles significantly improves the shear strength of the clay, especially at a 5% rubber content. The coefficient of determination (R2) of the CPO-CNN-LSTM model on the training and test datasets reaches 0.98 and 0.97, respectively, which exhibit high prediction accuracy and generalization ability. Full article
(This article belongs to the Section Polymer Physics and Theory)
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17 pages, 5319 KB  
Article
Use of Lignin, Waste Tire Rubber, and Waste Glass for Soil Stabilization
by Süleyman Gücek, Cahit Gürer, Bojan Žlender, Murat V. Taciroğlu, Burak E. Korkmaz, Kürşat Gürkan, Tamara Bračko, Borut Macuh, Rok Varga and Primož Jelušič
Appl. Sci. 2024, 14(17), 7532; https://doi.org/10.3390/app14177532 - 26 Aug 2024
Cited by 8 | Viewed by 3811
Abstract
The complex interactions between soil and additives such as lignin, glass powder, and rubber tires were investigated using principles of material and soil mechanics. Previous research has mainly focused on individual additives in clay soils. In contrast, this study investigates soil improvement with [...] Read more.
The complex interactions between soil and additives such as lignin, glass powder, and rubber tires were investigated using principles of material and soil mechanics. Previous research has mainly focused on individual additives in clay soils. In contrast, this study investigates soil improvement with two different types of waste materials simultaneously. The improvement of soil properties by hybrid waste materials was evaluated using several laboratory tests, including the standard Proctor test, the unconfined compressive strength test, the California Bearing Ratio (CBR) test, and cyclic triaxial tests. The aim of this research is to identify key parameters for the design and construction of road pavements and to demonstrate that improving the subgrade with hybrid waste materials contributes significantly to the sustainability of road construction. The mechanical and physical properties were evaluated in detail to determine the optimal mixtures. The results show that the most effective mixture for the combination of waste glass powder and rubber tires contains 20% glass powder and 3% rubber tires, based on the dry weight of the soil. For the combination of waste glass powder and lignin, the optimum mixture consists of 15% glass powder and 15% lignin, based on the dry weight of the soil. These results provide valuable insights into the sustainable use of waste materials for soil stabilization in road construction projects. Full article
(This article belongs to the Section Civil Engineering)
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36 pages, 8828 KB  
Article
From Bibliometric Analysis to Experimental Validation: Bibliometric and Literature Review of Four Cementing Agents in Soil Stabilization with Experimental Focus on Xanthan Gum
by Jair de Jesús Arrieta Baldovino, Oriana Palma Calabokis and Manuel Saba
Sustainability 2024, 16(13), 5363; https://doi.org/10.3390/su16135363 - 24 Jun 2024
Cited by 8 | Viewed by 3406
Abstract
This article focuses on the search for efficient solutions to enhance the mechanical strength of geomaterials, especially soils, with crucial applications in civil engineering. Four promising materials are explored as soil improvement agents: natural latex (rubber trees), lignosulfonate (paper industry byproduct), xanthan gum [...] Read more.
This article focuses on the search for efficient solutions to enhance the mechanical strength of geomaterials, especially soils, with crucial applications in civil engineering. Four promising materials are explored as soil improvement agents: natural latex (rubber trees), lignosulfonate (paper industry byproduct), xanthan gum (bacterial fermentation), and eggshell lime. While other sustainable options exist, these four were chosen for their distinct characteristics and potential for further study. Natural latex, derived from rubber trees, demonstrates exceptional potential for strengthening the mechanical resistance of soils, offering a path to effective stabilization without compromising environmental sustainability. Lignosulfonate, a paper industry byproduct, emerges as an alternative that can significantly enhance the load-bearing capacity of soils, boosting its applicability in civil engineering projects. Xanthan gum, produced through bacterial fermentation, possesses unique properties that increase soil cohesion and strength, making it a valuable option for geotechnical applications. Finally, despite potential challenges, eggshell lime shows promising potential in enhancing the mechanical resistance of soils. This study highlights the importance of evaluating and comparing these agents in terms of their effectiveness in improving the mechanical strength of soils in civil engineering applications. In the literature review, the impact of stabilizer addition (%) was examined for the four cementing agents studied, along with its influence on key soil properties like optimum moisture content (OMC, %), maximum dry density (MDD, gm/cc), California bearing ratio (CBR, %), uniaxial compressive strength (UCS) at 28 days (MPa), and the change in UCS (ΔUCS, %) among other physicochemical parameters. Appropriate selection of these materials can lead to developing more robust and sustainable geomaterials, promoting significant advancements in geotechnical engineering and civil construction practices. To evaluate their effectiveness, the efficiency of one of them was assessed experimentally. Xanthan gum (XG) was selected to biopolymerize clay soil. Specimens were prepared for strength and stiffness tests, including unconfined compression, scanning electron microscopy (SEM), and ultrasonic wave analysis. The impact of stabilizer concentration was examined (e.g., 1%, 3%, 5% xanthan gum) to assess how dosage affects the soil–stabilizer mixture. The results showed that the rubber increases the unconfined compression and stiffness of the soil, controlled by the XG’s porosity/volumetric quantity ratio. The research demonstrates the potential of XG, but a broader analysis of all four materials with the outlined testing methods paves the way for future advancements in geotechnical engineering. Full article
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18 pages, 7254 KB  
Article
Deformation Characteristics of Rubber Waste Powder–Clay Mixtures
by Davood Akbarimehr, Alireza Rahai, Abolfazl Eslami and Moses Karakouzian
Sustainability 2023, 15(16), 12384; https://doi.org/10.3390/su151612384 - 15 Aug 2023
Cited by 18 | Viewed by 2431
Abstract
With the increasing accumulation of rubber waste, the potential reuse of rubber fillers offers a promising solution to enhance the engineering properties of low-plasticity soils while promoting environmental sustainability. In this study, the effect of rubber waste powders (RWPs) on the consolidation and [...] Read more.
With the increasing accumulation of rubber waste, the potential reuse of rubber fillers offers a promising solution to enhance the engineering properties of low-plasticity soils while promoting environmental sustainability. In this study, the effect of rubber waste powders (RWPs) on the consolidation and deformation properties of low-plasticity clay soil (CS) was investigated using a fully automated consolidation testing procedure for clay–rubber mixtures. The study involved adding 2% up to 30% RWPs to Tehran clay, and various parameters were evaluated through consolidation, compaction, and uniaxial strength tests. The results revealed that the consolidation volume of the mixture differed from that of the CS due to the elastic nature of the rubber wastes (RWs). To achieve higher precision, a new equation was proposed to determine the void ratio, along with modified e-log p’ curves for the clay–rubber mixture. Furthermore, the addition of RWPs to the CS resulted in moderated free swelling of the soil while enhancing ductility, compression index (Cc), swelling index (Cs), and recompression index (Cr). However, it was observed that the strength and modulus of elasticity of the mixture decreased with the increase in rubber content. Considering the variations in geotechnical parameters with different rubber contents, the appropriate rubber content can be selected based on specific applications in soil and rubber mixtures, considering the required geotechnical parameters. This study highlights the potential applications of RWPs as a material in civil and geotechnical engineering projects, providing valuable insights for sustainable and eco-friendly engineering practices. Full article
(This article belongs to the Special Issue Waste Management and Recycling: Towards a Sustainable Future)
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22 pages, 3809 KB  
Article
Strength Characteristics of Clay–Rubber Waste Mixtures in Low-Frequency Cyclic Triaxial Tests
by Małgorzata Jastrzębska and Krzysztof Tokarz
Minerals 2021, 11(3), 315; https://doi.org/10.3390/min11030315 - 18 Mar 2021
Cited by 18 | Viewed by 4411
Abstract
This paper presents the results of consolidated and undrained (CU) triaxial cyclic tests related to the influence of tire waste addition on the strength characteristics of two different soils from Southern Poland: unswelling kaolin and swelling red clay. The test procedure included the [...] Read more.
This paper presents the results of consolidated and undrained (CU) triaxial cyclic tests related to the influence of tire waste addition on the strength characteristics of two different soils from Southern Poland: unswelling kaolin and swelling red clay. The test procedure included the normally consolidated remolded specimens prepared from pure red clay (RC) and kaolin (K) and their mixtures with two different fractions of shredded rubber powder (P) and granulate (G) in 5%, 10%, and 25% mass proportions. All samples were subjected to low-frequency cyclic loading carried out with a constant stress amplitude. Analysis of the results includes consideration of the effect of rubber additive and number of load cycles on the development of excess pore pressure and axial strain during the cyclic load operation and on the maximum stress deviator value. A general decrease in the shear strength due to the cyclic load operation was observed, and various effects of shear strength depended on the mixture content and size of the rubber waste particles. In general, the use of soil–rubber mixtures, especially for expansive soils and powder, should be treated with caution for cyclic loading. Full article
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8 pages, 860 KB  
Proceeding Paper
Natural Rubber Composites for Paper Coating Applications
by Pieter Samyn, Frank Driessen and Dirk Stanssens
Mater. Proc. 2020, 2(1), 29; https://doi.org/10.3390/CIWC2020-06832 - 13 May 2020
Cited by 7 | Viewed by 5019
Abstract
Natural rubbers are characterized by extremely high molecular weight that might be beneficial in the formation of a protective barrier layer on paper substrates, providing good cohesive properties but limited adhesion to the substrate. In parallel, the low glass transition temperature of natural [...] Read more.
Natural rubbers are characterized by extremely high molecular weight that might be beneficial in the formation of a protective barrier layer on paper substrates, providing good cohesive properties but limited adhesion to the substrate. In parallel, the low glass transition temperature of natural rubber might give the opportunity for good sealability, in contrast with severe problems of tack. Therefore, natural rubbers can be good candidates to serve as an alternative ecological binder in paper coatings for water and grease barrier resistance. In order to tune the surface properties of the paper coating, the effect of different fillers in natural rubber coatings are evaluated on rheological, thermo–mechanical and surface properties. The fillers are selected according to common practice for the paper industry, including talc, kaolinite clay and a type of organic nanoparticle, which are all added in the range of 5 to 20 wt.-%. Depending on the selected natural rubber, the dispersibility range (i.e., dispersive and distributive mixing) of the fillers in the latex phase highly varies and filler/matrix interactions are the strongest for nanoparticle fillers. An optimum selection of viscosity range allows us to obtain homogeneous mixtures without the need of surface modification of the additives. After bar-coating natural rubber latex composites on paper substrates, the drying properties of the composite coatings are followed by spectroscopy, illustrating the influences of selected additives on the vulcanization process. In particular, the latter most efficiently improves in the presence of nanoparticle fillers and highly increases the coating hydrophobicity in parallel, reducing the adhesive tack surface properties, as predicted from calculated work of adhesion. Full article
(This article belongs to the Proceedings of 2nd Coatings and Interfaces Web Conference (CIWC-2 2020))
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16 pages, 4126 KB  
Article
Strength Characteristics of Clay-Rubber Waste Mixtures in UU Triaxial Tests
by Małgorzata Jastrzębska
Geosciences 2019, 9(8), 352; https://doi.org/10.3390/geosciences9080352 - 10 Aug 2019
Cited by 16 | Viewed by 5279
Abstract
This paper presents results of undrained and unconsolidated (UU) triaxial tests related to the influence of tire waste addition on strength characteristics of red clay from Patoka in Southern Poland. Angle of internal friction and cohesion values were estimated for 30 specimens prepared [...] Read more.
This paper presents results of undrained and unconsolidated (UU) triaxial tests related to the influence of tire waste addition on strength characteristics of red clay from Patoka in Southern Poland. Angle of internal friction and cohesion values were estimated for 30 specimens prepared from pure red clay (RC), its mixtures with two different fractions of shredded rubber in 5%, 10%, and 25% mass proportions as well as for pure powder (P) and granulate (G). It has been observed that the addition of granulate contributes more to the increase in the angle of friction than the addition of powder (ΔΦuu = +1% (G-5) / +16% (G-10) / +31% (G-25), ΔΦuu = +1% (P-5) / +10% (P-10) / +19% (P-25)). On the other hand, rubber additions reduce cohesion in mixtures, and the effect is enhanced with increases in their grain size and percentage composition (Δcuu = −31% (G-5) / −63% (G-10) / −87% (G-25), Δcuu = −67% (P-5) / −58% (P-10) / −58% (P-25)). It has been noticed that a change of parameters Φuu and cuu causes a decline of shear stresses at increasing granulate content. There is an inverse relationship for powder. At the same time, it has been shown that the failure strain, hence a change in red clay-rubber (RCR) mixtures plasticity, is related to the level of confining stress σ3 and the type of rubber waste. Results of tests and their comparison with results of other researchers show that each time it is necessary to experimentally verify a given soil with specific rubber waste. Full article
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