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Keywords = luzhou block

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18 pages, 4480 KiB  
Article
Prediction of Horizontal in Situ Stress in Shale Reservoirs Based on Machine Learning Models
by Wenxuan Yu, Xizhe Li, Wei Guo, Hongming Zhan, Xuefeng Yang, Yongyang Liu, Xiangyang Pei, Weikang He, Longyi Wang and Yaoqiang Lin
Appl. Sci. 2025, 15(12), 6868; https://doi.org/10.3390/app15126868 - 18 Jun 2025
Viewed by 284
Abstract
To address the limitations of traditional methods in modeling complex nonlinear relationships in horizontal in situ stress prediction for shale reservoirs, this study proposes an integrated framework that combines well logging interpretation with machine learning to accurately predict horizontal in situ stress in [...] Read more.
To address the limitations of traditional methods in modeling complex nonlinear relationships in horizontal in situ stress prediction for shale reservoirs, this study proposes an integrated framework that combines well logging interpretation with machine learning to accurately predict horizontal in situ stress in shale reservoirs. Based on the logging data from five wells in the Luzhou Block of the Sichuan Basin (16,000 samples), Recursive Feature Elimination (RF-RFE) was used to identify nine key factors, including Stoneley wave slowness and caliper, from 30 feature parameters. Bayesian optimization was employed to fine-tune the hyperparameters of the XGBoost model globally. Results indicate that the XGBoost model performs optimally in predicting maximum horizontal principal stress (SHmax) and minimum horizontal principal stress (SHmin). It achieves R2 values of 0.978 and 0.959, respectively, on the test set. The error metrics (MAE, MSE, RMSE) of the XGBoost model are significantly lower than those of SVM and Random Forest, demonstrating its precise capture of the nonlinear relationships between logging parameters and in situ stress. This framework enhances the model’s adaptability to complex geological conditions through multi-well data training and eliminating redundant features, providing a reliable tool for hydraulic fracturing design and wellbore stability assessment in shale gas development. Full article
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15 pages, 1786 KiB  
Article
Comparison and Application of Pore Pressure Prediction Methods for Carbonate Formations: A Case Study in Luzhou Block, Sichuan Basin
by Wenzhe Li, Pingya Luo, Yatian Li, Jinghong Zhou, Xihui Hu, Qiutong Wang, Yiguo He and Yi Zhang
Energies 2025, 18(10), 2647; https://doi.org/10.3390/en18102647 - 20 May 2025
Viewed by 349
Abstract
The Luzhou Block in the Sichuan Basin hosts a widely distributed high-quality shale gas reservoir. However, the overlying carbonate strata pose considerable engineering challenges, including severe risks of subsurface fluid loss and wellbore collapse. These challenges are primarily attributed to inaccuracies in pore [...] Read more.
The Luzhou Block in the Sichuan Basin hosts a widely distributed high-quality shale gas reservoir. However, the overlying carbonate strata pose considerable engineering challenges, including severe risks of subsurface fluid loss and wellbore collapse. These challenges are primarily attributed to inaccuracies in pore pressure prediction, which significantly constrains the safety and efficiency of drilling operations in carbonate formations. To address this issue, this study systematically investigates and compares three classical pore pressure prediction approaches—namely, the equivalent depth method, the Eaton method, and the effective stress method—within the geological context of the Luzhou Block. A novel fitting strategy based on laboratory core experimental data is introduced, whereby empirical relationships between field-measured parameters and rock mechanical properties are established to improve model robustness in geologically complex formations. The optimized effective stress model is subsequently applied to the carbonate reservoir interval, and its prediction outcomes are evaluated against measured pore pressure data. The results demonstrate that the effective stress method achieves the highest prediction accuracy, with a maximum deviation of 8.4% and an average deviation of 5.3%. In comparison, the equivalent depth and Eaton methods yield average errors of 12.5% and 12.2%, respectively. These findings suggest that the effective stress method exhibits superior adaptability and reliability for pore pressure prediction in carbonate formations of the Luzhou Block, and holds significant potential for guiding mud density design and improving the operational safety of drilling programs. Full article
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19 pages, 8309 KiB  
Article
Experimental Study on Factors Influencing the Propagation of Hydraulic Fractures in Shale Reservoirs with Developed Natural Weak Planes
by Yitao Huang, Juhui Zhu, Yongming Li, Le He, Zeben Fang and Xiyu Chen
Energies 2025, 18(5), 1100; https://doi.org/10.3390/en18051100 - 24 Feb 2025
Viewed by 474
Abstract
Hydraulic fracturing is a key technology to build productivity in shale reservoirs; however, the evolution mechanism of fractures is extremely complex, especially in reservoirs with natural weak-planes development. There is an urgent need to conduct systematic research on the influence of natural weak [...] Read more.
Hydraulic fracturing is a key technology to build productivity in shale reservoirs; however, the evolution mechanism of fractures is extremely complex, especially in reservoirs with natural weak-planes development. There is an urgent need to conduct systematic research on the influence of natural weak planes on the vertical propagation of hydraulic fractures. This article takes the deep shale gas block of Luzhou in Southern Sichuan as the research basis and conducts different conditions of true triaxial large-scale hydraulic fracturing physical simulation experiments as well as the characteristics of natural weak-plane reservoir development and reservoir geological characteristics. This study clarifies the interaction mechanism between hydraulic fractures and natural weak planes and identifies the influence of parameters such as vertical stress difference, natural fracture strength, and approach angle on the propagation path of hydraulic fractures in reservoirs with developed natural weak planes, which help us gain a deeper insight into the interaction mechanism between fracture and weak plane. This study indicates that the widely developed natural weak planes in shale reservoirs significantly affect the initiation, propagation, and final distribution of hydraulic fractures. Based on pressure response characteristics, the fracture initiation types can be categorized into two scenarios: initiation along the direction of the maximum principal stress and initiation along natural weak planes. The propagation modes of fractures can be divided into three types: propagation perpendicular to natural weak planes, propagation parallel to natural weak planes, and multi-fracture propagation. The post-pressure fracture distribution patterns can be classified into four types: through-going fractures, T-shaped fractures, compound fractures, and complex fracture networks. The absence of developed natural weak planes, high vertical stress differences, high natural weak-plane cementation strength, and large intersection angles are favorable conditions for the vertical propagation of hydraulic fractures. The research findings enrich the fundamental theory of vertical propagation of hydraulic fractures in shale reservoirs with developed natural weak planes and provide a scientific basis for the formulation and optimization of stimulation schemes for deep shale reservoirs, contributing to better stimulation effects in the Southern Sichuan shale gas block. Full article
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22 pages, 9608 KiB  
Article
Research and Application of Geomechanics Using 3D Model of Deep Shale Gas in Luzhou Block, Sichuan Basin, Southwest China
by Ye Chen, Wenzhe Li, Xudong Wang, Yuan Wang, Li Fu, Pengcheng Wu and Zhiqiang Wang
Geosciences 2025, 15(2), 65; https://doi.org/10.3390/geosciences15020065 - 13 Feb 2025
Cited by 4 | Viewed by 805
Abstract
The deep shale gas resources of the Sichuan Basin are abundant and constitute an important component of China’s natural gas production. Complicated by fault zones and other geostructures, the in situ stress state of the deep shale gas reservoirs in the Luzhou block [...] Read more.
The deep shale gas resources of the Sichuan Basin are abundant and constitute an important component of China’s natural gas production. Complicated by fault zones and other geostructures, the in situ stress state of the deep shale gas reservoirs in the Luzhou block remains poorly understood. This study integrated multiple datasets, including acoustic logging, diagnostic fracture injection testing (DFIT), imaging logging, and laboratory stress measurements, for calibration and constraint. A high-precision geomechanical model of the Luzhou block was constructed using the finite element method. This model characterizes the geomechanical properties of the reservoir and explores its applications in optimizing shale gas horizontal well placement, drilling processes, and fracture design. The study findings indicate that the Longmaxi Formation reservoir demonstrates abnormally high pore pressure, with gradients ranging from 16.7 to 21.7 kPa/m. The predominant stress regime is strike-slip, with an overburden stress gradient of 25.5 kPa/m and a minimum horizontal principal stress gradient ranging from 18.8 to 24.5 kPa/m. Based on a three-dimensional geomechanical model, a quantitative delineation of areas conducive to density reduction and pressure control drilling was conducted, and field experiments were implemented in well Y65-X. Utilizing an optimized drilling fluid density of 1.85 g/cm3, the deviated horizontal section was completed in a single trip, resulting in a 67% reduction in the drilling cycle compared to adjacent wells. Similarly, the Y2-X well demonstrated a test daily output of 506,900 cubic meters following an optimization of segmentation clustering and fracturing parameters. Studies indicate that 3D geomechanical modeling, informed by multi-source data constraints, can markedly enhance model precision, and such geomechanical models and their results can effectively augment drilling operational efficiency, elevate single-well production, and are advantageous for development. Full article
(This article belongs to the Section Geomechanics)
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23 pages, 8051 KiB  
Article
Mechanism of Casing Deformation of Shale Gas Platform Wells in Luzhou Block Before Fracturing and Countermeasures for Prevention and Control
by Xiaojun Zhang, Jun Li, Yuxuan Zhao, Wei Cao, Wenbo Zhang, Zongyu Lu and Gonghui Liu
Processes 2025, 13(2), 479; https://doi.org/10.3390/pr13020479 - 10 Feb 2025
Viewed by 795
Abstract
The deep shale gas resources in the Luzhou area of the southern Sichuan Basin are abundant and have been identified as a key replacement field for natural gas development following the medium-to-shallow shale gas fields in Changning and Weiyuan. However, the frequent occurrence [...] Read more.
The deep shale gas resources in the Luzhou area of the southern Sichuan Basin are abundant and have been identified as a key replacement field for natural gas development following the medium-to-shallow shale gas fields in Changning and Weiyuan. However, the frequent occurrence of “pre-deformation without fracturing” in horizontal wells has significantly restricted large-scale production. In this study, the Lu203 and Yang101 well areas were analyzed to investigate the characteristics of casing deformation and the correlation with faults and natural fractures (fracture systems). A numerical model of multi-stage fracturing for platform wells was established based on microseismic event data, and the effects of fracturing on the stress and casing stress of adjacent wells were simulated and analyzed. The results indicate that the development of fracture systems is the primary cause of the “pre-deformation without fracturing” phenomenon. The propagation of fracturing fluid through fractures significantly increases the stress and loading around adjacent wells, causing casing stress to exceed its yield strength. To mitigate this issue, a method involving the injection of approximately 10 MPa of internal casing pressure into unfractured wells was proposed, effectively reducing the risk of casing deformation and failure. This provides technical support for the efficient development of deep shale gas. Full article
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17 pages, 9123 KiB  
Article
The Influence of Rock and Natural Weak Plane Properties on the Vertical Propagation of Hydraulic Fractures
by Xuefeng Yang, Cheng Chang, Qiuyang Cheng, Weiyang Xie, Haoran Hu, Yongming Li, Yitao Huang and Yu Peng
Processes 2024, 12(11), 2477; https://doi.org/10.3390/pr12112477 - 7 Nov 2024
Cited by 1 | Viewed by 1105
Abstract
China has abundant shale gas resources with good exploration value and development potential, making it a recent hotspot for exploration and development. It is widely agreed that large-scale hydraulic fracturing is essential for reservoir enhancement in shale formations. However, the evolution of fractures [...] Read more.
China has abundant shale gas resources with good exploration value and development potential, making it a recent hotspot for exploration and development. It is widely agreed that large-scale hydraulic fracturing is essential for reservoir enhancement in shale formations. However, the evolution of fractures during hydraulic fracturing is highly complex, necessitating research on the influence of various factors on the vertical propagation of hydraulic fractures. Based on geological and engineering parameters from the Luzhou block in southern Sichuan, this study employed the finite element method (FEM) and the cohesive element method to establish a coupled fluid-solid model for the vertical propagation of hydraulic fractures. Numerical simulations were conducted to investigate the interaction between hydraulic fractures and natural weak planes, clarifying the mechanisms involved. This study elucidates how different rock and natural weak plane properties affect the vertical propagation of hydraulic fractures and draws diagrams illustrating these interactions. The research indicated three fracture distribution patterns after the intersection of hydraulic fractures with natural weak planes: passive fractures, ‘I’-shaped fractures, and crossing fractures. The main fractures in these patterns exhibit initial damage and damage evolution characterized by tensile failure. Specifically, in passive fractures, the initial damage and damage evolution of natural weak planes manifest as shear failure. In ‘I’-shaped fractures, the initial damage in natural weak planes is characterized by shear failure, with damage evolution showing tensile failure. Crossing fractures show minimal damage in the weak planes. Under conditions of high natural weak plane cohesive strength, high Young’s modulus, low interlayer rock cohesive strength, high vertical stress difference, low interlayer stress difference, and high intersection angles, crossing fractures tend to form. Conversely, conditions of low natural weak plane cohesive strength, low Young’s modulus, high interlayer rock cohesive strength, low vertical stress difference, high interlayer stress difference, and low intersection angles favor the formation of ‘I’-shaped fractures. Passive fractures form under conditions of low natural weak plane cohesive strength and high vertical stress difference. This study found that Poisson’s ratio has a minimal effect on the vertical expansion of hydraulic fractures under the studied conditions, with natural weak plane strength being the primary control factor for fracture patterns. These findings enhance the theoretical foundation for the vertical propagation of hydraulic fractures in deep shale formations, facilitating the development and implementation of strategies for enhancing production in shale reservoirs with natural weak planes and better optimizing production in different types of shale reservoirs. Full article
(This article belongs to the Special Issue Advances in Enhancing Unconventional Oil/Gas Recovery, 2nd Edition)
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16 pages, 9977 KiB  
Article
Study on Evaluation and Prediction for Shale Gas PDC Bit in Luzhou Block Sichuan Based on BP Neural Network and Bit Structure
by Ye Chen, Yu Sang, Xudong Wang, Xiaoke Ye, Huaizhong Shi, Pengcheng Wu, Xinlong Li and Chao Xiong
Appl. Sci. 2024, 14(11), 4370; https://doi.org/10.3390/app14114370 - 22 May 2024
Cited by 2 | Viewed by 1204
Abstract
Deep and ultra-deep shale gas resources have great potential, but well drilling faces many challenges. The Polycrystalline Diamond Compact (PDC) bit has become the primary rock-breaking instrument for oil and gas drilling. Reasonable bit structure designs can promote rock-breaking efficiency and extend service [...] Read more.
Deep and ultra-deep shale gas resources have great potential, but well drilling faces many challenges. The Polycrystalline Diamond Compact (PDC) bit has become the primary rock-breaking instrument for oil and gas drilling. Reasonable bit structure designs can promote rock-breaking efficiency and extend service life. In this study, reverse modeling technology is used to analyze the structural characteristics of PDC bits collected in the field, and the influence of the structural characteristics of the bit at a specific interval on the rate of penetration (ROP) and drill footage is investigated using the Spearman rank correlation coefficient method. The number of blades, cutting angle of the cutters, crown rotation radius, internal cone angle, and diameter of the cutters are discovered to be the main structural characteristics that affect the ROP and footage of the bits, and the degree of influence varies depending on the formation conditions. The number of blades, crown rotation radius, inner cone angle, and cutting angle of the cutters have a significant impact on the ROP, whereas blade thickness, gauge length, gauge width, nozzle equivalent diameter have a significant impact on the bit footage. In addition, a back propagation (BP) neural network is utilized to build a prediction model of bit footage and ROP over a certain interval based on the structural characteristics of the bit. The goodness of fit of the model is greater than 85%, and its accuracy is high. Based on the usage of the bit, the evaluation and prediction of the bit can provide a reference for the structural design and optimization of the bit in a specific interval, guide the bit selection work, rationally plan the drilling operation, and reduce the drilling cost. Full article
(This article belongs to the Special Issue Development and Application of Intelligent Drilling Technology)
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13 pages, 5131 KiB  
Article
Quantifying the Widths of Fault Damage Zones Based on the Fault Likelihood: A Case Study of Faults in the Fuji Syncline of the Luzhou Block, Sichuan Basin, China
by Lu Zeng, Jinxi Li, Shihu Wu, Kailin Tong and Zhiwu Li
Sustainability 2023, 15(15), 11771; https://doi.org/10.3390/su151511771 - 31 Jul 2023
Viewed by 1897
Abstract
Faults are critical to the preservation or destruction of shale gas concentration. The Lower Silurian Longmaxi Formation in the southern Sichuan Basin hosts relatively developed faults, which pose a huge challenge to the exploration and exploitation of shale gas. An urgent need to [...] Read more.
Faults are critical to the preservation or destruction of shale gas concentration. The Lower Silurian Longmaxi Formation in the southern Sichuan Basin hosts relatively developed faults, which pose a huge challenge to the exploration and exploitation of shale gas. An urgent need to quickly determine the widths of fault damage zones (FDZs) arises in locating horizontal shale gas wells. In this study, FDZs were estimated using the fault likelihood. The results are as follows: (1) It is rational to constrain the FDZ width using a fault likelihood greater than 0.2. The six major NEE-trending faults in the Fuji syncline of the Luzhou block have complex structures and varying FDZ widths from about 240–1220 m. (2) The degree of influence of FDZs is negatively correlated with their distance from the faults. In other words, a greater distance from a fault is associated with a weaker influence and a smaller fault likelihood. (3) Based on the ratio of the fault throw to the FDZ width, we propose that the width of seismic-scale fault damages can be directly constrained using a ratio value of 3.5. This method is fast and accurate and can provide support for the evaluation of the shale gas preservation conditions and well placement in the Longmaxi Formation of the southern Sichuan Basin. Full article
(This article belongs to the Special Issue Basin Tectonic Analysis and Geoenergy Exploration)
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19 pages, 12943 KiB  
Article
Research on Casing Deformation Prevention Technology of a Deep Shale Gas Well Based on Cementing Slurry System Optimization
by Jing Cao, Shangyu Yang, Lihong Han, Jianjun Wang, Yisheng Mou and Caihong Lu
Processes 2022, 10(9), 1678; https://doi.org/10.3390/pr10091678 - 24 Aug 2022
Cited by 8 | Viewed by 2675
Abstract
In the complex fracturing process of shale gas wells, casing is subjected to serious deformation, which can easily to the failure of wellbore integrity and the reduction of well construction productivity. It is particularly important to clarify the casing deformation mechanism and carry [...] Read more.
In the complex fracturing process of shale gas wells, casing is subjected to serious deformation, which can easily to the failure of wellbore integrity and the reduction of well construction productivity. It is particularly important to clarify the casing deformation mechanism and carry out effective control. Based on the logging data of casing deformation from well and full-scale indoor tests, the casing deformation mechanism is mainly considered to be shear and non-uniform extrusion deformation caused by formation slip and displacement control, i.e., the ultimate working conditions. The slip displacement boundary (<40 mm) under complex fracturing conditions is quantified to provide the design and optimization basis. Then, the influence laws of steel grade and wall thickness on the shear and non-uniform extrusion bearing characteristics are studied, using unconventional oil and gas well casing simulation test systems for 110 ksi (φ139.7 × 10.54 mm) and 125 ksi (φ139.7 × 12.7 mm) casings. Furthermore, combined with the full-scale simulation tests and finite-element simulation, the effects of elastic and modified cement slurry with hollow glass beads on casing deformation are compared and studied. The results show that the deformation capacity mitigation of casing is limited by reducing the cement elastic modulus and increasing the elastic cement thickness. By reasonably adding hollow glass beads of modified cement slurry, the maximum geological movement absorption of cement slurry is up to 27 mm. This new method can obviously decrease casing deformation and have an excellent control effect. Combined with the cementing technology of Luzhou blocks, the formula of modified cement slurry is optimized, and the optimization window of the casing deformation control process is formed, which can ensure the smooth progress of engineering fracturing. Full article
(This article belongs to the Special Issue New Challenges in Advanced Process Control in Petroleum Engineering)
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24 pages, 8655 KiB  
Article
Geological Controlling Factors of Low Resistivity Shale and Their Implications on Reservoir Quality: A Case Study in the Southern Sichuan Basin, China
by Xinhua Ma, Hongyan Wang, Tianqi Zhou, Qun Zhao, Zhensheng Shi, Shasha Sun and Feng Cheng
Energies 2022, 15(16), 5801; https://doi.org/10.3390/en15165801 - 10 Aug 2022
Cited by 14 | Viewed by 2594
Abstract
At the Changning block and at the Luzhou block, the genetic mechanism of low-resistivity shale and its impact on reservoir quality are currently a hot topic on a world-wide scale. Shale with resistivity lower than 20 Ω·m is widely developed at the Wufeng-Longmaxi [...] Read more.
At the Changning block and at the Luzhou block, the genetic mechanism of low-resistivity shale and its impact on reservoir quality are currently a hot topic on a world-wide scale. Shale with resistivity lower than 20 Ω·m is widely developed at the Wufeng-Longmaxi Formation in the Southern Sichuan Basin, bringing a considerable challenge for reservoir prediction using the electromagnetic method. This paper discusses the genetic mechanisms and reservoir qualities of three low-resistivity shale reservoir types in the Southern Sichuan Basin (the Changning block and Luzhou block). Three primary elements controlling low-resistivity shale distribution in the Southern Sichuan Basin have been deduced: widely distributed gravity flow deposits, poor structural preservation conditions and shale graphitization caused by Emeishan basalt. Specifically, (1) the shale reservoir with a resistivity <12 Ω·m was uniformly distributed with gravity flow deposits in the Southern Sichuan Basin. High clay mineral contents (especially illite) in gravity flow deposits increased cation exchange capacity and irreducible water saturation at shale reservoir, decreasing electrical resistivity. (2) The resistivity of the shale reservoir close to a complex fault-fracture zone was generally lower than 20 Ω·m, indicating that poor structural preservation conditions played an important role in the wide distribution of low-resistivity shale. The resistivity of the shale reservoir near NE-trending faults at the Changning block was significantly lower than that in other areas. (3) Emeishan basalt caused extensive shale graphitization at the west of the Changning block, which was limited at the Luzhou block. The shale resistivity at the Luzhou block was not affected by graphitization. Among three types of low-resistivity shale, type III was characterized by high quartz content, high TOC, high porosity, high gas content and low graphitization. Although the resistivity of type III is generally lower that 20 Ω·m, it is still a favorable exploration target in the Southern Sichuan Basin. Full article
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20 pages, 6347 KiB  
Article
Pore Water and Its Influences on the Nanopore Structures of Deep Longmaxi Shales in the Luzhou Block of the Southern Sichuan Basin, China
by Haitao Gao, Peng Cheng, Wei Wu, Shenyang Liu, Chao Luo, Tengfei Li, Kesu Zhong and Hui Tian
Energies 2022, 15(11), 4053; https://doi.org/10.3390/en15114053 - 31 May 2022
Cited by 9 | Viewed by 1921
Abstract
In the Luzhou Block of the southern Sichuan Basin, the deep Longmaxi shales have become important exploration targets in recent years. However, the water-bearing properties of these shales are still unclear, which significantly limits evaluations of reservoir pore structures and gas-in-place (GIP) contents. [...] Read more.
In the Luzhou Block of the southern Sichuan Basin, the deep Longmaxi shales have become important exploration targets in recent years. However, the water-bearing properties of these shales are still unclear, which significantly limits evaluations of reservoir pore structures and gas-in-place (GIP) contents. In this study, twelve fresh shale core samples were collected at the well site, and the pore water (CPW) and equilibrium water (CEW) contents, as well as the pore structures of the shales, were analyzed under both as-received and dried conditions. The results indicate that the deep shales have low water-bearing extents with a pore water content (CPW) of 3.82–16.67 mg/g, and that both the organic matter (OM) and inorganic matter (IM) pores can be used for pore water storage. The extent of influence of pore water on nonmicropores and IM pore structures is more significant than that on micropores and OM pore structures. Meanwhile, the pore water obviously reduces the retention effects of nanopores and may block nanopores with pore widths < 0.5 nm. An average of 40% of pore spaces were taken up by pore water in the studied deep shales in the Luzhou Block, and the residual pore surface area and pore volume of the shales were mainly contributed from micropores and nonmicropores, respectively. Full article
(This article belongs to the Special Issue New Challenges in Shale Gas and Oil)
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18 pages, 5259 KiB  
Article
Influence of Particle Size on the Low-Temperature Nitrogen Adsorption of Deep Shale in Southern Sichuan, China
by Hongming Zhan, Xizhe Li, Zhiming Hu, Xianggang Duan, Wei Guo and Yalong Li
Minerals 2022, 12(3), 302; https://doi.org/10.3390/min12030302 - 27 Feb 2022
Cited by 15 | Viewed by 3038
Abstract
Pore characteristics are one of the most important elements in the study of shale reservoir properties and are a key parameter for the evaluation of the potential of shale oil and gas resources. Low-temperature nitrogen adsorption is a common laboratory method that is [...] Read more.
Pore characteristics are one of the most important elements in the study of shale reservoir properties and are a key parameter for the evaluation of the potential of shale oil and gas resources. Low-temperature nitrogen adsorption is a common laboratory method that is used to characterize the pore structure of shale. However, the effect of shale’s particle size on the experimental results of the nitrogen adsorption of deep shale samples is still unclear. In this paper, using deep shale samples of different mesh sizes from the Luzhou Block as an example, we studied the effect of particle size on the pore structure of deep shale, as characterized by nitrogen adsorption experiments. The results showed that the pore volume of deep shale is mainly distributed in the mesoporous range, with a pore size ranging from 2 to 20 nm. The pore volume, as measured by nitrogen adsorption, increases slowly as the particle size decreases and then it increases rapidly. The particle size of shale has no obvious effect on the measurement of the specific surface area. The fractal dimension of deep shale gradually increases as the particle size of the shale samples increases and the smaller the particle size, the higher the correlation coefficient, R2, of the fractal dimension fitting. In this paper, different recommended sizes are given for selecting suitable particle sizes in nitrogen adsorption experiments on deep shale with different structural parameters, which will increase the accuracy of the study of the pore structure of deep shale. Full article
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14 pages, 4075 KiB  
Article
Shale Reservoir Heterogeneity: A Case Study of Organic-Rich Longmaxi Shale in Southern Sichuan, China
by Hongming Zhan, Feifei Fang, Xizhe Li, Zhiming Hu and Jie Zhang
Energies 2022, 15(3), 913; https://doi.org/10.3390/en15030913 - 27 Jan 2022
Cited by 10 | Viewed by 2249
Abstract
Shale reservoir heterogeneity is strong, which seriously affects shale gas reservoir evaluation and reserves estimation. The Longmaxi Formation shale of the Luzhou block in southern Sichuan was taken as an example to characterize the pore distribution of shale over the full scale using [...] Read more.
Shale reservoir heterogeneity is strong, which seriously affects shale gas reservoir evaluation and reserves estimation. The Longmaxi Formation shale of the Luzhou block in southern Sichuan was taken as an example to characterize the pore distribution of shale over the full scale using micro-computed tomography (CT), focusing on ion beam scanning electron microscopy (FIB-SEM) and small-angle neutron scattering (SANS); further, the heterogeneity of the shale pore distribution over the full scale was explored quantitatively within different scales. The results show that shale micropores are dominated by microfractures that are mainly developed along the bedding direction and associated with organic matter, contributing 1.24% of porosity. Shale nanopores are more developed, contributing 3.57–4.72% porosity and have strong heterogeneity locally at the microscale, but the pore distribution characteristics show lateral homogeneity and vertical heterogeneity at the macroscale. In the same layer, the porosity difference is only 0.1% for the sheet samples with 2 cm adjacent to each other. Therefore, in shale core experiments in which parallel samples are needed for comparison, parallel samples should be in the same bedding position. This paper explores the extent of heterogeneity over the full scale of pore distribution from macro to micro, which has important significance for accurately characterizing the pore distribution of shale and further carrying out reservoir evaluation and estimation of reserves. Full article
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