Search Results (71)

This study takes limestone crushed stone concrete as the research object and systematically investigates its mechanical property changes and microstructural damage characteristics under different confining pressures using triaxial compression tests, scanning electron microscope (SEM) tests, and digital image processing techniques. The results show that, in terms of macro-mechanical properties, as the confining pressure increases, the peak strength increases by 192.66%, the axial peak strain increases by 143.66%, the elastic modulus increases by 133.98%, and the ductility coefficient increases by 54.61%. In terms of microstructure, the porosity decreases by 64.35%, the maximum pore diameter decreases by 75.69%, the fractal dimension decreases by 19.56%, and the interfacial transition zone cracks gradually extend into the aggregate interior. The optimization of the microstructure makes the concrete more compact, reduces stress concentration, and thereby enhances the macro-mechanical properties. Additionally, the failure characteristics of the specimens shift from diagonal shear failure to compressive flow failure. According to the Mohr–Coulomb strength criterion, the calculated cohesion is 6.96 MPa, the internal friction angle is 38.89°, and the breakage angle is 25.53°. A regression analysis established a quantitative relationship between microstructural characteristics and macro-mechanical properties, revealing the significant impact of microstructural characteristics on macro-mechanical properties. Under low confining pressure, early volumetric expansion and rapid volumetric strain occur, with microcracks mainly concentrated at the aggregate interface that are relatively wide. Under high confining pressure, volumetric expansion is delayed, volumetric strain increases slowly, and microcracks extend into the interior of the aggregate, becoming finer and more dispersed. Full article

Polyaryletherketone (PAEK) materials, including polyetheretherketone (PEEK) and polyetherketoneketone (PEKK), possess excellent mechanical properties and biocompatibility; however, their inherently low surface energy limits effective bonding with resin cements. This study investigated the effects of hydrofluoric acid (HF) etching and handheld nonthermal plasma (HNP) treatment on enhancing the adhesive performance of PAEK surfaces. Disk-shaped PEEK (BP) and PEKK (PK) specimens were divided into four groups: APA (airborne-particle abrasion), PLA (nonthermal plasma treatment), LHF (5.0% HF), and HHF (9.5% HF). Surface characterization was performed using a thermal field emission scanning electron microscope (FE-SEM). Surface wettability was evaluated using contact angle goniometry. Cytotoxicity was evaluated using HGF-1 cells exposed to conditioned media and analyzed via PrestoBlue assays. Shear bond strength (SBS) was measured after three aging conditions—NT (no aging), TC (thermocycling), and HA (highly accelerated aging)—using a light-curing resin cement. Failure modes were categorized, and statistical analysis was performed using one-way and two-way ANOVA with Tukey’s HSD test (α = 0.05). Different surface treatments did not affect surface characterization. PLA treatment significantly improved surface wettability, resulting in the lowest contact angles among all groups, followed by HF etching (HHF > LHF), while APA showed the poorest hydrophilicity. Across all treatments, PK exhibited better wettability than BP. Cytotoxicity results confirmed that all surface treatments were nontoxic to HGF-1 cells, indicating favorable biocompatibility. SBS testing demonstrated that PLA-treated specimens achieved the highest and most stable bond strength across all aging conditions. Although HF-treated groups exhibited lower bond strength overall, BP samples treated with HF showed relatively less reduction following aging. Failure mode analysis revealed a shift from mixture and cohesive failures in the NT aging condition to predominantly adhesive failures after TC and HA aging conditions. Notably, the PLA-treated groups retained mixture failure patterns even after aging, suggesting improved interfacial durability. Among the tested methods, PLA treatment was the most effective strategy, enhancing surface wettability, bond strength, and aging resistance without compromising biocompatibility. In summary, the PLA demonstrated the greatest clinical potential for improving the adhesive performance of PAEK when used with light-curing resin cements. Full article

This study investigated the enhancement of the mechanical and tribological properties of MWCNT-reinforced bio-based epoxy composites through systematic experiments and analysis. Composites incorporating MWCNTs at varying weight percentages were evaluated for hardness, wear rate, interfacial shear strength, and friction coefficient under diverse load, sliding speed, and distance conditions. An optimal MWCNT content of 0.3–0.4% resulted in a maximum hardness of 4 GPa and a minimum wear rate of 0.0058 mm³/N·m, demonstrating a substantial improvement over the non-reinforced system. FTIR and XRD analyses confirmed robust interfacial bonding between the MWCNTs and epoxy matrix, while molecular dynamics simulations revealed cohesive energy density and stress distribution profiles. The Taguchi optimization identified the MWCNT weight percentage as the most influential parameter, contributing over 85% to wear rate reduction. Contour plots and correlograms further illustrate the parameter interdependencies, emphasizing the role of MWCNT dispersion in enhancing the composite properties. These findings establish that MWCNT-reinforced bio-based epoxy composites are promising candidates for high-performance and sustainable tribological applications. Full article

Flexible pipe end fittings (EFs) transfer axial loads by embedding tensile armor within epoxy matrices. The integrity of bonding between the armor and resin profoundly influences the EF load-bearing capacity. This study investigated the debonding failure mechanism at the epoxy-resin–tensile-armor interface in flexible pipe end fittings through integrated experimental and numerical approaches. Combining tensile tests with digital image correlation (DIC) and cohesive zone modeling (CZM), the research quantified the impacts of interfacial defects and adhesive properties on structural integrity. Specimens with varying bond lengths (40–60 mm) and defect diameters (0–4 mm) revealed that defects significantly reduced load-bearing capacity, with larger defects exacerbating strain localization and accelerating failure. A dimensionless parameter, the defect-size-to-bond-length ratio ($\lambda =D/2L$), was proposed to unify defect impact analysis, demonstrating its nonlinear relationship with failure load reduction. High-toughness adhesives, such as Sikaforce^® 7752, mitigated defect sensitivity by redistributing stress concentrations, outperforming brittle alternatives like Araldite^® AV138. DIC captured real-time strain evolution and crack propagation, validating strain concentrations up to 3.2 at defect edges, while CZM simulations achieved high accuracy (errors: 3.0–7.2%) in predicting failure loads. Critical thresholds for λ (λ < 0.025 for negligible impact; λ > 0.05 requiring defect control or high-toughness adhesives) were established, providing actionable guidelines for manufacturing optimization and adhesive selection. By bridging experimental dynamics with predictive modeling, this work advances the design of robust deepwater energy infrastructure through defect management and material innovation, offering practical strategies to enhance structural reliability in critical applications. Full article

Current research on soil–structure interface properties mainly focuses on sand, clay, and silt, with little attention given to sandy gravel. In order to study the effects of relative density and interface materials on the shear behavior of the sandy gravel–structure interface, a series of large-scale direct shear tests on sandy gravel were carried out, and stress–strain relationships, volume change curves, and shear strengths were investigated. The results show that the angle of internal friction of sandy gravel increases linearly with relative density (R² is 0.998), from 43.0° to 48.0° when the relative density increases from 0.3 to 0.9. The growth trend of cohesion increases, the shear behavior transitions from strain hardening to strain softening, and the shear strength increases linearly with the increase in relative density. The interfacial shear strengths and interface adhesion of sandy gravel with steel and concrete interfaces increase linearly with relative density, and the shear curves are strain hardening. Furthermore, the interface friction angle of concrete increases linearly with relative density (R² is 0.985), from 30.2° to 34.2°, while the interface friction angle of the steel interface remains relatively constant around 28.9°. Finally, relative density was introduced into the Mohr–Coulomb shear strength formula, and the relationship equations of relative density and normal pressure with the shear strength and interfacial shear strength of sandy gravel were established. The validation results show that the error margin of the formula is within 4%. This formula can be used to evaluate changes in the mechanical properties of sandy gravel formations and the bearing capacity of pile foundations after they have been disturbed by factors such as construction. Full article

Addressing the challenge of weak interface strength in 3D-printed mortars, this study introduces a novel technique using sinuous printing trajectories. The self-locking interface is formed by different meandering print trajectories, and the changes in the strength of the test interface are investigated by adjusting the trajectories to form different amplitudes. This ensures alignment of peaks and troughs between layers, aiming for enhanced interfacial cohesion. Experimental tests measured mechanical properties of printed mortar specimens with varying amplitudes. Using Digital Image Correlation technology, strain fields and fracture surfaces were analyzed. Initial results revealed a 28% decrease in shear resistance for side-by-side printed interfaces compared to traditional layered interfaces. As amplitude increased, shear load-bearing capacity improved. Specifically, a 15 mm amplitude saw a 40% rise in interlayer shear strength. However, a 20 mm amplitude led to reduced shear capacity, with even slight forces causing potential fractures. Tensile strength also increased with amplitude. Specimens up to 15 mm amplitude primarily followed the printing interface in fractures, while a 20 mm amplitude cut through mortar strips. Post-fracture analysis showed the highest surface irregularity at a 15 mm amplitude, aligning with tensile load-bearing capacity. Full article

This study evaluates four widely used fracture simulation methods, comparing their computational expenses and implementation complexities within the finite element (FE) framework when employed on heterogeneous solids. Fracture methods considered encompass the intrinsic cohesive zone model (CZM) using zero-thickness cohesive interface elements (CIEs), the standard phase-field fracture (SPFM) approach, the cohesive phase-field fracture (CPFM) approach, and an innovative hybrid model. The hybrid approach combines the CPFM fracture method with the CZM, specifically applying the CZM within the interface zone. The finite element model studied is characterized by three specific phases: inclusions, matrix, and the interface zone. This case study serves as a potential template for meso- or micro-level simulations involving a variety of composite materials. The thorough assessment of these modeling techniques indicates that the CPFM approach stands out as the most effective computational model, provided that the thickness of the interface zone is not significantly smaller than that of the other phases. In materials like concrete, which contain interfaces within their microstructure, the interface thickness is notably small when compared to other phases. This leads to the hybrid model standing as the most authentic finite element model, utilizing CIEs within the interface to simulate interface debonding. A significant finding from this investigation is that within the CPFM method, for a specific interface thickness, convergence with the hybrid model can be observed. This suggests that the CPFM fracture method could serve as a unified fracture approach for multiphase materials when a specific interfacial thickness is used. In addition, this research provides valuable insights that can advance efforts to fine-tune material microstructures. An investigation of the influence of interfacial material properties, voids, and the spatial arrangement of inclusions shows a pronounced effect of these parameters on the fracture toughness of the material. Full article

To investigate the reinforcement–soil interfacial effects in fiber-reinforced soil, this study developed a novel horizontal pullout tester and conducted pullout tests on coarse polypropylene fibers in plain soil, cemented soil, and fine fiber-reinforced cemented soil. Three soil types were analyzed: low liquid limit clay, high liquid limit clay, and clay sand. The pullout tester proved to be both scientifically robust and efficient. Depending on the soil properties, coarse polypropylene fibers were pulled out intact or fractured. The pullout curves displayed distinct multi-peak patterns, with wavelengths closely linked to the fiber’s intrinsic characteristics. The pullout curve wavelength for plain soil matched the fiber’s intrinsic wavelength, while it was slightly greater in cemented soils. The peak pullout force increased with extended curing periods, higher cement content, more excellent compaction, and the addition of fine polypropylene fibers. Among these factors, compaction had the most significant impact on enhancing the soil–fiber interfacial effect. Friction, cohesion, and fiber interweaving created interlocking effects, inhibiting fiber sliding. Cement hydration processes further deformed the fiber, increasing its friction coefficient and sliding resistance. Hydration products also fill soil voids, improving soil compactness, enlarging the fiber–soil contact area, and enhancing frictional and occlusal forces at the interface. Full article

Interfacial adhesion is one of the key factors affecting the reliability of micro–nano systems. The adhesion contact mechanism is still unclear as the time-dependent viscoelasticity of soft materials. To clarify the adhesion interaction, the pull-off detachment between the rigid flat punch and viscoelastic substrate is explored considering the viscoelasticity of soft materials and rate-dependent adhesion. Taking the Lennard-Jones (L-J) potential characterizing interfacial adhesion and the Prony series defining the viscoelasticity of materials as references, the bilinear cohesion zone model (CZM) and standard Maxwell model are employed, and an adhesion analysis framework is established by combining finite element technology. The influence laws of the loading and unloading rates, material relaxation coefficients and size effect on adhesion pull-off behavior are revealed. The results show that the pull-off force is independent of the material relaxation effect and related to the unloading rate. When $\widehat{v}$ ≥ 50 or $\widehat{v}$ < 0.01, the pull-off force has nothing to do with the unloading rate, but when 0.01 < $\widehat{v}$ < 50, the pull-off force increases with the increasing unloading rate. Also, it is controlled by the size effect, and the changing trend conforms to the MD-n model proposed by Jiang. The energy required for interfacial separation (i.e., effective adhesion work) is a result of the comprehensive influence of unloading rates, material properties and the relaxation effect, which is consistent with Papangelo1’s research results. In addition, we derive the critical contact radius of the transition from the Kendall solution to the strength control solution. This work not only provides a detailed solution for the interfacial adhesion behavior but also provides guidance for the application of adhesion in Micro-Electro-Mechanical Systems (MEMSs). Full article

The drain pipe wrapped in steel wire mesh serves a dual purpose of drainage and reinforcement in tailings pond projects. The self-filtering layer that develops upstream of the steel wire mesh influences the reinforcement characteristics of the drainage pipe. This study first conducts interfacial shearing experiments to explore the impact of the self-filtering layer on the shearing properties between tailings and the steel wire mesh. An exponential interface constitutive model is then proposed to delineate the shear stress–displacement relationship. Finally, through finite element simulations, the study assesses the effect of the self-filtering layer on the load-bearing behavior of the drain pipe, considering the interactive dynamics between the tailings and the steel wire mesh. The results reveal that the interfacial shear strength, across varying median particle sizes of the self-filtering layer, adheres to Mohr–Coulomb strength theory. Specifically, as the median particle size of the self-filtering layer increases, interfacial cohesion diminishes while the friction coefficient rises. The initial shear stiffness demonstrates a linear increase with the median particle size. With the presence of the self-filtering layer, the pull-out resistance of the drainage pipe can be enhanced by up to 26%. Moreover, the self-filtering layer significantly affects the distribution of negative skin friction. This research enhances the safety assessment of tailings ponds by providing crucial insights and solutions, emphasizing the influence of the self-filtering layer on the bearing behavior of the drain pipe. Full article

Currently, microscopic research on the tensile fracture properties of recycled brick coarse aggregate concrete has mainly adopted microscopy techniques, which can clearly observe the actual damage situations of each phase material but are unable to individually analyze the effect of a specific material factor on the tensile properties of recycled concrete. This brings much uncertainty to the practical application of recycled concrete. Therefore, this study proposes a cohesive zone model (CZM) for simulating the tensile fracture of recycled brick coarse aggregate (RBCA) concrete. To this end, the study explores the effects of various critical factors on the fracture mode and bearing capacity of recycled brick aggregate concrete, including the replacement rate of recycled brick coarse aggregate, pore structure, interfacial transition zone (ITZ) strength, mortar strength, and volume fraction of brick aggregate. The results indicate that, when the minor to major axis ratio of elliptical pores is 0.5 ≤ K < 1, the following order of influence can be observed: random convex polygonal pores, circular pores, and elliptical pores. Moreover, excessively strengthening the ITZ and mortar does not significantly enhance the tensile performance of RBCA concrete. The distribution location of aggregate has a significant impact on the crack shape of recycled concrete, as does the pore structure, due to their randomness. Therefore, this article also discusses these. These findings contribute to a comprehensive understanding of the tensile properties of recycled brick coarse aggregate and provide insights into optimizing its behavior. Full article

Rubber concrete has been applied to a certain extent in fatigue-resistant structures due to its good durability. Based on a cohesive model of rubber composed of a five-phase material containing mortar, aggregate, rubber, aggregate-mortar interfacial transition zone (ITZ), and rubber-mortar ITZ, this paper studies the influence of the cohesive parameters in the rubber-mortar ITZ on the fatigue problem of rubber concrete on the mesoscopic scale. As the weak part of cement-based composite materials, the ITZ has a great influence on the mechanical properties and durability of concrete, but the performance of the ITZ is difficult to test in macro experiments, resulting in difficulties in determining its simulation parameters. Based on the cohesive model with a rubber content of 5%, this study uses Monofactor analysis and the Plackett-Burman test to quickly and effectively determine the primary and secondary influences of the cohesive model parameters in the rubber-mortar ITZ; further, the response surface method is used to optimize the cohesive parameters in the rubber-mortar ITZ, and the numerical simulation results after optimizing the cohesive parameters are compared and analyzed with the simulation results before optimization. The results show that, under the setting of the optimized parameters, the simulation results of each item of the optimal cohesive model parameters in the rubber-mortar ITZ are in line with the reality and closer to the experimental data, and they are also applicable to rubber concrete models with different rubber dosing. Full article

Hydrogels with adhesion properties and a wetted structure are promising alternatives to traditional wound dressing materials. The insufficiency of gelatin hydrogels in terms of their adhesive and mechanical strength limits their application in wound dressings. This work presents the design and preparation of a gelatin-based hydrogel functionalized with dopamine (DA) and layered double hydroxide (LDH). The combination of DA and LDH improves the hydrogel’s adhesion properties in terms of interfacial adhesion and inner cohesion. Hydrogels with 8% DA and 4% LDH attained the highest adhesion strength of 266.5 kPa, which increased to 295.5 and 343.3 kPa after hydrophobically modifying the gelatin with octanoyl and decanoyl aldehydes, respectively. The gelatin-based hydrogels also demonstrated a macroporous structure, excellent biocompatibility, and a good anti-inflammatory effect. The developed hydrogels accelerated wound healing in Sprague Dawley rat skin full-thickness wound models. Full article

Temperature and humidity coupling has a more significant effect on the failure properties of bonded joints than a single factor, and there is not enough research on this. In this paper, joints bonded with strong toughness structural adhesives are selected for the experimental analysis of joints aged for 240 h, 480 h, and 720 h at temperatures of 40 °C and 60 °C and a humidity of 95% and 100%. The sequential double Fick’s model was used to fit the water absorption of the joints, and the comparison yielded that the water absorption of the adhesive was in accordance with Fick’s law. The quasi-static tensile tests revealed that the reduction in mechanical properties of the joints was positively correlated with the moisture content in the environment, while the competing mechanisms of post-temperature curing and hydroplasticization resulted in a slight increase in the failure strength and energy uptake of the aged joints, which is in agreement with the experimental results of the Fourier infrared spectroscopy. A combination of macroscopic failure sections and scanning electron microscope (SEM) images yielded that the failure mode of the joints changed from cohesive failure to interfacial failure with increasing ageing time. In addition, reliability analyses for the fatigue testing of joints are expected to provide guidance for the life design of bonding technology in the vehicle service temperature range. Full article

Semi-aromatic poly (hexamethylene terephthalamide) (PA6T) oligomer (prePA6T) ultrafine powder, with a diameter of <5 μm, was prepared as an emulsion sizing agent to improve the impregnation performance of CF/PA6T composites. The prePA6T hyperfine powder was acquired via the dissolution and precipitation “phase conversion” method, and the prePA6T emulsion sizing agent was acquired to continuously coat the CF bundle. The sized CF unidirectional tape was knitted into a fabric using the plain weave method, while the CF/PA6T laminated composites were obtained by laminating the plain weave fabrics with PA6T films. The interfacial shear strength (IFSS), tensile strength (TS), and interlaminar shear strength (ILSS) of prePA6T-modified CF/PA6T composites improved by 54.9%, 125.3%, and 120.9%, respectively. Compared with the commercial polyamide sizing agent product PA845H, the prePA6T sizing agent showed better interfacial properties at elevated temperatures, especially no TS loss at 75 °C. The SEM observations also indicated that the prePA6T emulsion has an excellent impregnation effect on CF, and the fracture mechanism shifted from adhesive failure mode to cohesive failure mode. In summary, a facile, heat-resistant, undamaged-to-fiber environmental coating process is proposed to continuously manufacture high-performance thermoplastic composites, which is quite promising in mass production. Full article