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Keywords = high cycle fatigue tests

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14 pages, 3704 KB  
Article
Effects of Grain Boundary Misorientation on the High-Cycle Fatigue Behavior of Nickel-Based Superalloy Bicrystals
by Qinghui Wu, Chenglu Zou, Xiuge Ma, Jianchao Pang, Zengqian Liu, Kailun Luo and Zhefeng Zhang
Materials 2026, 19(13), 2735; https://doi.org/10.3390/ma19132735 - 26 Jun 2026
Viewed by 252
Abstract
Nickel-based single-crystal superalloys are key materials for manufacturing aero-engine turbine blades. Different grain boundaries are inevitably formed during the production of superalloys and weaken the fatigue performance of the alloys. Systematic exploration of the effect of grain boundary misorientation (GBM) on the fatigue [...] Read more.
Nickel-based single-crystal superalloys are key materials for manufacturing aero-engine turbine blades. Different grain boundaries are inevitably formed during the production of superalloys and weaken the fatigue performance of the alloys. Systematic exploration of the effect of grain boundary misorientation (GBM) on the fatigue properties of superalloys is of great significance. Available research cannot fully illustrate the influence of GBM on the high-cycle fatigue (HCF) damage mechanism of superalloys, especially its coupling with inherent casting defects. In this study, bicrystal specimens with misorientations of 4°, 8° and 12° were fabricated from a second-generation nickel-based single-crystal superalloy. The influence mechanism of misorientation variation on HCF performance was systematically investigated. The test results show that the HCF life of the alloy decreases obviously as GBM rises from 4° to 8° and then declines slowly. Fracture analysis indicates that fatigue damage is closely associated with GBM and casting defects. A 4° grain boundary promotes coordinated deformation and inhibits cracking, whereas misorientations over 8° cause dislocation pile-up and speed up crack propagation. Based on the significant effects of GBM and casting defects on fatigue damage behavior, as well as the analysis of the two key parameters in the Basquin model, a linear correlation is established between the fatigue strength coefficient (σf) and misorientation; a coupling relationship is constructed among the fatigue strength exponent (b), misorientation, and defect size. Prediction results confirm that the model achieves higher accuracy by incorporating casting defect parameters. Full article
(This article belongs to the Special Issue Fatigue Behavior, Fracture and Optimization of Alloys and Composites)
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16 pages, 6098 KB  
Article
Tribological Investigation of Wear-Resistant Friction Pairs for Miniature Linear Ultrasonic Motors
by Huajie Qu, Meiqin Liang and Zhongpu Wen
Lubricants 2026, 14(7), 251; https://doi.org/10.3390/lubricants14070251 - 24 Jun 2026
Viewed by 152
Abstract
To solve the drawbacks of conventional long-cycle wear tests for miniature standing- wave linear ultrasonic motors, an accelerated equivalent wear model and test system were proposed in this work. After primary screening of multiple pair materials, graphite and Al2O3 were [...] Read more.
To solve the drawbacks of conventional long-cycle wear tests for miniature standing- wave linear ultrasonic motors, an accelerated equivalent wear model and test system were proposed in this work. After primary screening of multiple pair materials, graphite and Al2O3 were adopted to modify epoxy films. The optimal friction pair is composed of 6061 hard anodic oxidation film and ECA105 composite film. The matched pair exhibits excellent driving stability and low wear loss, with fatigue wear as the main wear form. Graphite and Al2O3 exert synergistic anti-wear and load-bearing effects via forming a stable transfer film on the friction interface. Experimental results confirm that the accelerated test is equivalent to a full-life durability test. The presented method and optimized friction pair can effectively guide the development of high-performance ultrasonic motors. Full article
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12 pages, 11549 KB  
Article
Microstructural Change Due to Aging and Its Effect on Fatigue Properties in Sn-Sb-Ag-Ni-Ge Alloy
by Kohei Mitsui, Hirohiko Watanabe, Kosuke Kimura and Ikuo Shohji
Materials 2026, 19(13), 2710; https://doi.org/10.3390/ma19132710 - 24 Jun 2026
Viewed by 187
Abstract
In this study, the microstructural changes and coarsening behavior of Ag3Sn in Sn-6.4Sb-3.9Ag-0.25Ni-0.003Ge (mass%) during high-temperature aging were investigated. Additionally, low-cycle fatigue tests were conducted to compare the fatigue behavior of Sn-6.4Sb-3.9Ag-0.25Ni-0.003Ge with that of Sn-3.0Ag-0.5Cu. At room temperature, SbSn phases [...] Read more.
In this study, the microstructural changes and coarsening behavior of Ag3Sn in Sn-6.4Sb-3.9Ag-0.25Ni-0.003Ge (mass%) during high-temperature aging were investigated. Additionally, low-cycle fatigue tests were conducted to compare the fatigue behavior of Sn-6.4Sb-3.9Ag-0.25Ni-0.003Ge with that of Sn-3.0Ag-0.5Cu. At room temperature, SbSn phases are dispersed in the β-Sn matrix. As the temperature rises, Sb atoms dissolve in the β-Sn phase; thus, the SbSn phases disappear, and some of the atoms aggregate. The activation energy was 45 kJ/mol for the coarsening of Ag3Sn in Sn-6.4Sb-3.9Ag-0.25Ni-0.003Ge due to aging. Ag3Sn coarsening was estimated to be controlled by the lattice diffusion of Ag atoms in the β-Sn phase. Furthermore, it was confirmed that the solid solution of Sb atoms in the β-Sn phase reduces the solubility limit of Ag atoms in the β-Sn phase, which delays the coarsening of Ag3Sn. Regarding fatigue properties, while both alloys exhibited comparable low-cycle fatigue behavior at room temperature, the fatigue ductility exponent’s increase was confirmed to be suppressed for the Sn-6.4Sb-3.9Ag-0.25Ni-0.003Ge alloy at 175 °C. This trend suggests that the delayed coarsening of Ag3Sn maintains the cyclic strain-hardening exponent, thereby influencing high-temperature fatigue behavior. Full article
(This article belongs to the Section Metals and Alloys)
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21 pages, 15198 KB  
Article
Effects of Slamming-Induced Whipping on Fatigue Damage of an Ultra-Large Container Ship Advancing in Irregular Waves
by Ying Tang, Ziyin Huang, Xiaojun Lv, Yucun Pan, Shili Sun, Huilong Ren and Yiheng Zhang
J. Mar. Sci. Eng. 2026, 14(12), 1125; https://doi.org/10.3390/jmse14121125 - 18 Jun 2026
Viewed by 269
Abstract
Slamming-induced whipping has been recognized as a key contributor to fatigue damage of large ships operating under severe sea states. However, accurate prediction of whipping responses remains challenging because of complex nonlinear fluid–structure interactions. This study aims to investigate the characteristics of slamming-induced [...] Read more.
Slamming-induced whipping has been recognized as a key contributor to fatigue damage of large ships operating under severe sea states. However, accurate prediction of whipping responses remains challenging because of complex nonlinear fluid–structure interactions. This study aims to investigate the characteristics of slamming-induced whipping and quantitatively analyze its influence on the fatigue damage of an ultra-large container ship. A three-dimensional fully nonlinear time-domain hydroelastic method, in which the boundary element model is coupled with a Timoshenko beam model, is employed to predict the slamming-induced whipping responses. Segmented model tests in long-crested irregular waves are conducted to provide wave loads of hull girders under severe sea states. The total and wave-frequency vertical bending moments are separated by the fast Fourier transform, and their statistical characteristics are evaluated through probability distributions. Fatigue damage is assessed on the basis of the rainflow counting method and the Palmgren–Miner cumulative damage rule. The contribution of high-frequency whipping responses to fatigue damage is quantitatively evaluated using a fatigue damage factor. It is demonstrated that slamming-induced whipping can significantly amplify fatigue damage by increasing stress amplitudes and cycle counts, particularly under high forward speeds and severe sea conditions. The findings provide a reliable reference for the fatigue design and safety assessment of ultra-large container ships. Full article
(This article belongs to the Special Issue Advances in Fatigue and Dynamic Response of Marine Structures)
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14 pages, 4225 KB  
Article
Fatigue Behavior of Hybrid Additive/Subtractive Manufactured Ti-6Al-4V
by Nicholas Parolini, Andrew Ikeler, Ryan Kinser, Abhendra Singh, P. G. Allison and J. B. Jordon
Metals 2026, 16(6), 673; https://doi.org/10.3390/met16060673 - 18 Jun 2026
Viewed by 399
Abstract
Additive–subtractive hybrid manufacturing (ASHM) allows for the rapid manufacturing of metal components with complex and precise geometries for ready-to-use or near-ready-to-use applications. Laser wire-directed energy deposition (LW-DED) can be used to quickly manufacture metal components, while CNC machining can achieve precise geometric tolerances. [...] Read more.
Additive–subtractive hybrid manufacturing (ASHM) allows for the rapid manufacturing of metal components with complex and precise geometries for ready-to-use or near-ready-to-use applications. Laser wire-directed energy deposition (LW-DED) can be used to quickly manufacture metal components, while CNC machining can achieve precise geometric tolerances. In this study, Ti-6Al-4V alloy specimens were fabricated using an LW-DED process combined with CNC machining and tested to evaluate the effects of ASHM on mechanical performance. Post fabrication, the Ti-6Al-4V material was evaluated through hardness mapping, monotonic tensile testing, and fully reversed axial fatigue testing. Vicker’s micro-hardness mapping showed a range of hardness results from 300 to 350 HV in the ASHM Ti-6Al-4V that remained consistent throughout the build. Tensile results showed a similar response to cast and wrought Ti-6Al-4V, with an average yield stress of 819.4 MPa, ultimate tensile strength of 935.5 MPa, and modulus of 119 GPa. When tested in fatigue, the material had a reduced life compared to wrought Ti-6Al-4V, which is attributed to defects originating from the additive process. While no run-outs were observed from the testing, the fatigue results remain aligned with trends reported for other methods of additively manufactured Ti-6Al-4V. Fully reversed high-cycle fatigue loading revealed that the ASHM-fabricated Ti-6Al-4V fell into a Basquin power-law fit with a fatigue strength coefficient of 1942 MPa with a fatigue strength exponent of −0.115. The fatigue life of the ASHM material is found to be dependent on the resulting porosity of the material that stems from the LW-DED process used in the ASHM process described. Full article
(This article belongs to the Special Issue Research on Fatigue Behavior of Additively Manufactured Materials)
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21 pages, 5325 KB  
Article
Fatigue Analysis of Commercial-Vehicle Lateral Stabilizer Bar Based on Load Decomposition Method
by Jiwei Zhang, Ziting Huang, Liang Li, Jun Zeng, Hui Yuan and Changcheng Yin
Vehicles 2026, 8(6), 133; https://doi.org/10.3390/vehicles8060133 - 16 Jun 2026
Viewed by 256
Abstract
As a core component for restraining cab roll, the lateral stabilizer bar bears continuous complex alternating loads during vehicle operation, making it highly susceptible to fatigue failure that may trigger severe traffic accidents. Therefore, fatigue analysis of the lateral stabilizer bar is of [...] Read more.
As a core component for restraining cab roll, the lateral stabilizer bar bears continuous complex alternating loads during vehicle operation, making it highly susceptible to fatigue failure that may trigger severe traffic accidents. Therefore, fatigue analysis of the lateral stabilizer bar is of great significance. To address the drawbacks of conventional direct load testing, such as difficult sensor arrangement and long test cycles, this paper proposes a fatigue-load decomposition and life evaluation method, combining multi-body dynamics and virtual iteration. Firstly, target signal spectra of the frame are obtained via real-vehicle road tests, and a high-precision system dynamic model is established with key suspension parameters. Subsequently, virtual iteration technology is adopted to accurately inverse-solve load spectra at critical points of the lateral stabilizer bar. Finally, the finite element model of the lateral stabilizer bar is validated through modal tests, and the fatigue life and vulnerable regions of the lateral stabilizer bar are predicted using the material S-N curve. Compared with traditional physical testing methods, the proposed method effectively avoids barriers to direct testing under complex operating conditions. It not only greatly reduces testing difficulty and time costs but also ensures the accuracy of load extraction and system analysis. Full article
(This article belongs to the Section Safety and Security in Vehicles)
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14 pages, 27721 KB  
Article
Experimental Investigation of Microstructural Evolution and Fatigue Damage of Pearlite Wheel Steel During Tread Braking Based on a Full-Size Wheel–Rail Test Rig
by Mingzhe Fan, Guanzhen Zhang, Xiang Li, Guang Li, Shuo Sun, Yi Wu and Pengtao Liu
Metals 2026, 16(6), 662; https://doi.org/10.3390/met16060662 - 15 Jun 2026
Viewed by 261
Abstract
This study investigated the relationship between the surface microstructure of pearlite steel wheels and the formation of fatigue cracks during the braking process by using a full-size wheel braking test rig. After fatigue failure, the surface microstructural evolution and fatigue crack initiation and [...] Read more.
This study investigated the relationship between the surface microstructure of pearlite steel wheels and the formation of fatigue cracks during the braking process by using a full-size wheel braking test rig. After fatigue failure, the surface microstructural evolution and fatigue crack initiation and propagation of the wheel sample were systematically analyzed by optical microscope (OM), scanning electron microscope (SEM), and transmission electron microscope (TEM). The results showed that after braking of 1572 cycles, a large number of fatigue cracks formed at the wheel tread, which caused the wheel to break. After fatigue failure, some dark areas formed at the wheel tread, which were composed of Fe3O4 compounds. This indicates that severe oxidation was produced at the wheel tread during braking due to the high temperature. After fatigue failure, a continuous thermal white etching layer (T-WEL) was formed in some areas of the wheel tread, while crescent-shaped T-WEL was found in other areas. The microstructure of the T-WEL was composed of martensite phase. The rapid increase and decrease in temperature at the wheel tread during the braking process caused martensitic transformation at the wheel tread. The hardness of the sample reached to about 900 HV in WEL and it reduced with the increase in distance from the surface. The cracks were initiated from the surface and gradually propagated into the matrix. However, the crack propagation mode in the continuous T-WEL and crescent-shaped T-WEL was different. In the continuous T-WEL, the continuous T-WEL of the wheel can be peeled off during the braking wear process, and then the crack was gradually propagated into the matrix in the T-WEL peeled area. As for the crescent-shaped T-WEL, due to the large hardness difference between T-WEL and pearlite, the crack initiated at the interface between the T-WEL and pearlite and gradually propagated into the matrix. Full article
(This article belongs to the Special Issue Advances in the Fatigue and Fracture Behaviour of Metallic Materials)
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30 pages, 7654 KB  
Article
Performance-Based Assessment of Pakistani Regional Aggregates for Flexible Pavements Using Macro- and Micro-Characterization
by Fazli Karim, Nasir Khan, Md Arifuzzaman and Muhammad Imran Khan
Materials 2026, 19(12), 2535; https://doi.org/10.3390/ma19122535 - 11 Jun 2026
Viewed by 176
Abstract
Aggregates comprise up to 95% of flexible pavement composition, critically influencing performance based on geological source and processing methods. In Pakistan, where approximately 264,175 km of roads carry 96% of inland freight, premium Margalla aggregates face increasing demand and depleting reserves, necessitating sustainable [...] Read more.
Aggregates comprise up to 95% of flexible pavement composition, critically influencing performance based on geological source and processing methods. In Pakistan, where approximately 264,175 km of roads carry 96% of inland freight, premium Margalla aggregates face increasing demand and depleting reserves, necessitating sustainable alternatives. This study comprehensively evaluates aggregates from five key quarries (Margalla, Malakand, Kohat, Swabi, and Besai) for highway suitability. Rigorous laboratory testing encompassed macro-level physical and mechanical properties and micro-characterization using Scanning Electron Microscopy (SEM), Energy Dispersive Spectroscopy (EDS), and Fourier Transform Infrared Spectroscopy (FTIR), alongside performance tests including Indirect Tensile Strength (ITS), rutting resistance, and fatigue analysis. Overall, Margalla aggregates exhibited the best performance, showing the lowest abrasion value (21%), highest Tensile Strength ratio (TSR) (82%), highest conditioned ITS (433.7 kPa), highest dynamic modulus (2120 MPa at 25 Hz), and the lowest rut depth (7.8 mm at 10,000 cycles). These superior properties are attributed to their favorable physical characteristics and high calcium content. Malakand and Kohat aggregates also demonstrated satisfactory performance, with TSR values of 79% and 76%, conditioned ITS values of 408.7 and 377.7 kPa, and rut depths of approximately 8.8 and 10.5 mm, respectively, indicating their suitability for medium-traffic pavements. In contrast, Swabi and Besai aggregates exhibited lower moisture resistance (TSR = 77% and 75%), lower conditioned ITS (355.7 and 337.7 kPa), and higher rut depths (~13.0 and 14.2 mm), making them less suitable for high-stress pavement layers. These findings support Malakand and Kohat aggregates as viable regional alternatives to Margalla. Full article
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29 pages, 1713 KB  
Article
Preparation and Rheological Properties of Waterborne Epoxy Resin Emulsified Asphalt
by Siyu Wu, Huaxin Chen, Suining Zheng, Yonglu Dong and Wenlan Zhang
Materials 2026, 19(12), 2493; https://doi.org/10.3390/ma19122493 - 10 Jun 2026
Viewed by 228
Abstract
To address the lack of systematic quantitative studies on waterborne epoxy resin (WER)-modified emulsified asphalt regarding its rheological optimization and engineering applicability, this study fills the gap by preparing WER-modified emulsified asphalt via a two-step process. New findings reveal that 20% WER content [...] Read more.
To address the lack of systematic quantitative studies on waterborne epoxy resin (WER)-modified emulsified asphalt regarding its rheological optimization and engineering applicability, this study fills the gap by preparing WER-modified emulsified asphalt via a two-step process. New findings reveal that 20% WER content significantly enhances elastic components, creep–recovery, fatigue life, and fracture energy. The main objective is to establish a theoretical basis for high-performance pavement materials. Modified emulsified asphalt specimens with different waterborne epoxy resin contents were prepared using a two-step method of “emulsification followed by compounding”. The stability of the emulsions was quantitatively evaluated by zeta potential, storage stability, particle size distribution, and demulsification time. Their rheological parameters, multi-stress creep–recovery characteristics, fatigue life, and low-temperature crack resistance were systematically tested across the full temperature range using a dynamic shear rheometer and a bending beam rheometer. In addition, the bonding performance, strength development behavior, and water resistance durability were comprehensively assessed through pull-out tests, Marshall stability and splitting strength tests, as well as freeze–thaw cycle tests. These properties were compared with those of unmodified emulsified asphalt (UEA-0) and SBR-modified emulsified asphalt (SBR-EA). With an increase in waterborne epoxy resin content, the elastic component of the modified asphalt improved significantly, and the phase angle continuously decreased. The specimen with 20% waterborne epoxy resin content (WER-EA-20) exhibited the best performance: its phase angle was lower than those of the other groups under high-, medium-, and low-temperature conditions. After seven creep–recovery cycles, its creep–recovery rate remained at 33%, substantially higher than the 8% observed for the unmodified specimen. The fatigue life reached 15,000 cycles under a shear stress of 2.1 MPa. At −10 °C, the fracture strength was 0.92 MPa, and the fracture energy reached 21.4 J. Furthermore, the pull-out strength of WER-EA-20 was 0.86 MPa, with the failure mode identified as asphalt cohesive failure. After 37 days of curing, the Marshall stability reached 22.5 kN, and the splitting strength was 1.36 MPa. After 40 freeze–thaw cycles, the freeze–thaw splitting strength ratio (TSR) of WER-EA-20 remained above 75%, representing an improvement of more than 110% compared to the unmodified UEA-0 (TSR ≈ 35.5%), which highlights the significant enhancement in water resistance imparted by the waterborne epoxy resin. Compared to SBR-EA, WER-EA-20 has a higher softening point, a lower suitable mixing temperature, and better anti-aging properties. Waterborne epoxy resin can effectively improve the viscoelastic properties and overall road performance of emulsified asphalt, and the modification effect increases with increasing dosage. Full article
(This article belongs to the Special Issue Mechanical Dynamics and Rheological Insights in Advanced Materials)
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27 pages, 9477 KB  
Article
Low-Cycle Fatigue Behavior and Microstructural Damage Mechanisms of 316L Austenitic Stainless Steel in Cryogenic Environments
by Sujuan Guo, Guolong Zhang, Junnan Chen, Lei Li, Hui Zhang, Qicong Li and Jian Zhao
Materials 2026, 19(12), 2494; https://doi.org/10.3390/ma19122494 - 10 Jun 2026
Viewed by 330
Abstract
This study focuses on the low-cycle fatigue behavior and microstructural damage mechanisms of 316L austenitic stainless steel in cryogenic environments to enhance understanding of its fatigue performance and failure mechanisms over a wide temperature range. Uniaxial tensile and strain-controlled low-cycle fatigue tests were [...] Read more.
This study focuses on the low-cycle fatigue behavior and microstructural damage mechanisms of 316L austenitic stainless steel in cryogenic environments to enhance understanding of its fatigue performance and failure mechanisms over a wide temperature range. Uniaxial tensile and strain-controlled low-cycle fatigue tests were performed at 293 K, 173 K, and 77 K; microstructural evolution and damage mechanisms were explored via interrupted tests combined with multiple microscopic techniques and quantitative martensite analysis. The results show that the room temperature fatigue stress response has three stages, while low temperatures induce continuous cyclic hardening that stabilizes quickly; fatigue life increases with lower temperature and strain amplitude, more notably at high strains. Low temperatures enhance strength, increase hardness, slightly reduce plasticity, but maintain good toughness, suppressing crack initiation and propagation with ductile fracture. The findings clarify cryogenic fatigue damage mechanisms, providing experimental and theoretical support for cryogenic pressure-bearing component design and safety assessment. Full article
(This article belongs to the Section Mechanics of Materials)
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19 pages, 13155 KB  
Article
Influence of a Simulated Marine Atmosphere on the Fatigue Performance of TC25 Alloy
by Guangming Kong, Yichen Jiang, Jianglong Ma, Zhiguo Liu and Ang Tian
Materials 2026, 19(12), 2484; https://doi.org/10.3390/ma19122484 - 10 Jun 2026
Viewed by 248
Abstract
Titanium alloys have been extensively employed in the aerospace industry, and their service performance is largely governed by high-temperature low-cycle fatigue damage. However, investigations into the fatigue behavior of TC25 titanium alloy subjected to corrosion in a marine atmospheric environment remain limited. In [...] Read more.
Titanium alloys have been extensively employed in the aerospace industry, and their service performance is largely governed by high-temperature low-cycle fatigue damage. However, investigations into the fatigue behavior of TC25 titanium alloy subjected to corrosion in a marine atmospheric environment remain limited. In this study, high-temperature low-cycle fatigue tests were conducted on TC25 titanium alloy before and after corrosion. It was found that, after corrosion, the proportion of the structural failure stage increased by approximately 10%. The corrosion pits on the surface led to local stress concentration, resulting in an increase in the number of fatigue crack sources and an acceleration of the fatigue crack growth rate, thus reducing the fatigue life of the material. These findings provide important theoretical and experimental support for the application of TC25 titanium alloy in marine environments. Full article
(This article belongs to the Section Mechanics of Materials)
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21 pages, 6186 KB  
Article
Combined Effects of Fast-Melting SBS (F-SBS) and Crumb Rubber (CR) on Asphalt Mixtures Using the Dry Process Method
by Jinyao Li, Hao Wu, Fengqi Guo, Weimin Song, Xiaobao Chen, Hongbo Liao and Zhiqiang Cheng
Polymers 2026, 18(12), 1440; https://doi.org/10.3390/polym18121440 - 9 Jun 2026
Viewed by 283
Abstract
Considering the production efficiency and performance limitations inherent in conventional wet process asphalt mixtures, this study investigates the synergistic potential of fast-melting styrene–butadiene–styrene (F-SBS) and crumb rubber (CR) in enhancing the performance of asphalt mixtures when applied through the dry process modification method. [...] Read more.
Considering the production efficiency and performance limitations inherent in conventional wet process asphalt mixtures, this study investigates the synergistic potential of fast-melting styrene–butadiene–styrene (F-SBS) and crumb rubber (CR) in enhancing the performance of asphalt mixtures when applied through the dry process modification method. Firstly, high- and low-temperature rheological tests were conducted on modified asphalt containing different dosages of F-SBS (1–3%) and CR (1–10%) to determine the optimal dosage of the modifier for the asphalt mixture. Furthermore, a comprehensive comparative analysis was conducted to evaluate the performance of asphalt mixtures modified with conventional SBS/CR against the F-SBS/CR system across both wet and dry modification processes. Finally, microscopic tests were conducted on the modified asphalt and asphalt mixtures to further investigate the synergistic mechanisms and effects of F-SBS and CR. The results indicated that F-SBS (2.5%)/CR (8%)-modified asphalt exhibited superior rheological properties, enhanced compatibility, and improved storage stability. Additionally, the dry process F-SBS/CR asphalt mixture demonstrated a 12.9% improvement in high-temperature stability, a 19.1% improvement in split strength after freeze–thaw cycles, and a 14.4% improvement in fatigue resistance compared to wet process conventional SBS/CR asphalt mixtures. The microscopic test results indicate that F-SBS and CR modify the asphalt primarily through physical blending. Observations further confirm that the dry process enhances interfacial bonding among the modifiers, asphalt binder, and aggregates, promoting closer and more stable interactions and thus improving mixing efficiency and overall performance. This study confirms the advantages of applying F-SBS and CR in dry process asphalt mixtures, thereby providing guidance for establishing a connection between laboratory investigations and field construction practices in the future. Full article
(This article belongs to the Special Issue Mechanical Behaviors of Polymer and Polymer Composites)
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26 pages, 7130 KB  
Article
Failure Mechanism and Engineering Validation of an Improved PEEK–CFRP Stator Shielding Sleeve for High-Speed Permanent Magnet Shielded Motors
by Li Cao, Yan Hu, Jiangning Wang, Bohan Wang, Siyu Wu and Jingshan Zhang
Machines 2026, 14(6), 668; https://doi.org/10.3390/machines14060668 - 8 Jun 2026
Viewed by 201
Abstract
High-speed permanent magnet synchronous motors (PMSMs) used in electric pump-fed liquid rocket engines require stator shielding sleeves to prevent corrosive propellants from causing harm under cyclic pressure. However, metallic sleeves suffer significant losses due to eddy currents. Conversely, pure carbon fiber reinforced polymer [...] Read more.
High-speed permanent magnet synchronous motors (PMSMs) used in electric pump-fed liquid rocket engines require stator shielding sleeves to prevent corrosive propellants from causing harm under cyclic pressure. However, metallic sleeves suffer significant losses due to eddy currents. Conversely, pure carbon fiber reinforced polymer (CFRP) sleeves have failed when exposed to 98% H2O2. Micro-CT analysis of a failed pump sleeve reveals a four-stage failure mechanism. Manufacturing defects caused matrix cracking, which propagated under pressure and thermal cycling. This progression resulted in the formation of through-thickness leakage paths, which ultimately triggered catalytic decomposition and explosion. To address these issues, an improved dual-layer sleeve is proposed, featuring a 2.5 mm PEEK 450G liner and a 2.0 mm T700S/epoxy CFRP overwrap. Finite Element Analysis (FEA) indicates peak von-Mises stresses of 86.25 MPa and 112.16 MPa, yielding Tsai–Wu safety factors of 2.9 and 1.7. Furthermore, various tests, including immersion, fatigue, burst, hydraulic, and thermal evaluations, demonstrate a burst margin of 2.37× at 7.12 MPa, with only 0.19% increase in mass. This design effectively eliminates leakage pathways while preserving zero eddy-current loss and ensuring a low weight. Full article
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22 pages, 549 KB  
Article
Plasma Metabolite Profiles of Exercising American Foxhound Dogs Fed Different Diets
by Sara E. Martini, Maria R. C. de Godoy, Alison N. Beloshapka, Preston R. Buff and Kelly S. Swanson
Metabolites 2026, 16(6), 397; https://doi.org/10.3390/metabo16060397 - 8 Jun 2026
Viewed by 372
Abstract
Background/Objectives: Canine athletes have a higher energy requirement and are more susceptible to nutrient depletion, electrolyte imbalance, and metabolic stress than sedentary pets. The objective of this study was to characterize the plasma metabolome of American Foxhound dogs following a bout of unstructured [...] Read more.
Background/Objectives: Canine athletes have a higher energy requirement and are more susceptible to nutrient depletion, electrolyte imbalance, and metabolic stress than sedentary pets. The objective of this study was to characterize the plasma metabolome of American Foxhound dogs following a bout of unstructured exercise. Methods: Thirty-nine adult American Foxhound dogs (32 intact males, 7 spayed females; age: 6.2 ± 3.1 yr; BW: 36.3 ± 5.3 kg) were allotted to a standard performance diet (CTRL) or NUTRO® Natural Choice® Adult High Endurance Formula (TEST). After 80 d in the study, blood samples were collected prior to (0 h), and 3 h and 25 h post-exercise (average: 17.7 km run over 2–3 h). Plasma samples of the 10 top performers of each treatment group were analyzed for untargeted metabolite profiling. Results: Of the 566 named metabolites identified, >200 and >185 metabolites were impacted (p < 0.05) by exercise and diet, respectively. Principal component analysis indicated distinct clustering by diet. Random forest analysis highlighted several metabolites having a high degree of predictive accuracy based on diet and exercise, with most related to amino acid, lipid, xenobiotic, and cofactor and vitamin metabolism. Relating to exercise, glycolytic end-products and citric acid cycle intermediates were increased at 3 h post-exercise. Similarly, tocopherols and omega-3 polyunsaturated fatty acids were higher in dogs fed TEST than those fed CTRL during recovery, indicating a lower oxidative stress and anti-inflammatory response. Conclusions: Overall, the data suggest a protective effect (lower susceptibility to oxidative stress and muscle fatigue) of feeding a nutrient-fortified diet for dogs undergoing unstructured exercise. Full article
(This article belongs to the Section Animal Metabolism)
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16 pages, 1916 KB  
Article
Study on the Modification Mechanism and Rheological Properties of Bio-Oil-Based Composite-Modified Material for TOP-DOWN Crack Treatment in Long-Life Pavement
by Haining Wang, Xiangpeng Yan, Qingming Wang, Wenjuan Wu, Yao Tian and Qinsheng Xu
J. Compos. Sci. 2026, 10(6), 298; https://doi.org/10.3390/jcs10060298 - 29 May 2026
Viewed by 278
Abstract
To address the durability limitations of conventional crack sealants under coupled extreme temperatures and traffic loads in long-life pavements, a bio-oil composite-modified patching material was developed using 90# base asphalt as the matrix, synergistically modified with crumb rubber (CR) and epoxidized soybean oil [...] Read more.
To address the durability limitations of conventional crack sealants under coupled extreme temperatures and traffic loads in long-life pavements, a bio-oil composite-modified patching material was developed using 90# base asphalt as the matrix, synergistically modified with crumb rubber (CR) and epoxidized soybean oil (ESO). To resolve the contradictory requirements for high elasticity and thermal expansion/contraction coordination in sealants, ESO was introduced; its polar epoxy groups optimize phase compatibility and promote low-temperature stress relaxation without restricting thermal deformability. Rheological evaluations revealed that the optimal system (OPT) successfully extended the service temperature window from PG 76–−24 °C (baseline) to PG 82–−24 °C, significantly enhancing its adaptability to extreme climatic fluctuations. At −24 °C, OPT exhibited a reduced creep stiffness (S) of 164 MPa and an increased creep rate (m) of 0.312, with a cracking resistance ratio (k) as low as 525.6; the quantitative significance of these metrics lies in granting the sealant superior stress relaxation capacity, enabling it to accommodate dynamic crack widening without interfacial debonding or brittle fracture. Fatigue testing via time sweeps demonstrated that Nf50 reached 2890 cycles, highlighting robust long-term resistance against high-frequency shear strains induced by tire edges. Micro-mechanistic analyses (FTIR, TG/DTG, and DSC) confirmed that the modification is primarily driven by physical blending. The elevation of the thermal decomposition threshold (T5%) to 302.4 °C and the residue at 600 °C to 44.8% provide a critical safety margin for high-temperature construction heating, preventing thermal degradation. Furthermore, the glass transition temperature (Tg) decreased to approximately −35.2 °C. These findings establish a rigorous quantitative and mechanistic framework for designing sustainable, high-performance patching materials for resilient pavement maintenance. Full article
(This article belongs to the Special Issue Advanced Composite Materials for Civil Construction Applications)
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