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Keywords = dew retting

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18 pages, 6078 KiB  
Article
Composites with Flax and Hemp Fibers Obtained Using Osmotic Degumming, Water-Retting, and Dew-Retting Processes
by Wanda Różańska and Szymon Rojewski
Materials 2025, 18(13), 3200; https://doi.org/10.3390/ma18133200 - 7 Jul 2025
Viewed by 343
Abstract
This study presents the application of flax (Linum usitatissimum L.) and hemp (Cannabis sativa L.) fibers into composites with polyethylene matrices. The applied fibers were obtained using osmotic, water-retting, and dew-retting processes. The study determined the impact of the fiber extraction [...] Read more.
This study presents the application of flax (Linum usitatissimum L.) and hemp (Cannabis sativa L.) fibers into composites with polyethylene matrices. The applied fibers were obtained using osmotic, water-retting, and dew-retting processes. The study determined the impact of the fiber extraction method on the properties of the composites obtained from natural filler and polyethylene matrix. These properties included color, tensile strength, thermal stability, adhesion of filler to the polymer, and flammability. It has been shown that the addition of flax and hemp fibers improves the mechanical properties of the composite compared to pure polymer. The tensile strength of the pure polymer samples was 24.64 MPa, while the tensile strength of composites reinforced with flax fibers ranged from 31.26 to 34.45 MPa, and those reinforced with hemp fibers ranged from 31.41 to 33.36 MPa. Studying the composites’ flammability showed that filling them with osmotic degummed hemp fibers reduced the maximum heat release rate by over 34% for hemp compared to pure polymer. This research shows that the composites filled with flax and hemp fibers, regardless of extraction method, are characterized by reduced flammability and improved mechanical properties compared to the pure polyethylene samples. Full article
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34 pages, 2908 KiB  
Article
Geographical and Soil-Based Assessment of Yield and Fiber Quality in Two Flax Varieties in Central–Eastern Poland Using the Flax Value Chain Approach
by Piotr Barbaś, Barbara Sawicka, Dominika Skiba and Piotr Pszczółkowski
Land 2025, 14(6), 1178; https://doi.org/10.3390/land14061178 - 29 May 2025
Viewed by 576
Abstract
Flax cultivation is influenced by geographical conditions and soil properties, affecting yield and fiber quality. This study examines the performance of two fiber flax varieties, Artemida and Hermes, in 2021–2023 in central–eastern Poland’s agroclimatic and soil conditions using a value chain approach. Field [...] Read more.
Flax cultivation is influenced by geographical conditions and soil properties, affecting yield and fiber quality. This study examines the performance of two fiber flax varieties, Artemida and Hermes, in 2021–2023 in central–eastern Poland’s agroclimatic and soil conditions using a value chain approach. Field trials were conducted in soils of varying fertility under a continental climate, employing a randomized block design with four replications. Flax straw underwent dew-retting, and long fibers were extracted through laboratory scutching. Results showed significant differences between the varieties. Artemida achieved higher straw yields, particularly in moderately fertile soils, while Hermes produced a higher proportion of long fibers and adapted better to less-fertile soils. Hermes fibers were thinner and more delicate, whereas Artemida fibers were coarser and stronger. The average straw yield of the Artemida variety was higher by 1.5 t ha−1 than that of the Hermes variety. The yield and quality of fiber were determined by soil fertility and climate, and the genotype–environment interaction was of the greatest importance. These findings provide valuable insights for farmers and stakeholders in selecting suitable flax varieties for different soil and climatic conditions in central–eastern Poland. The value chain approach also supports optimizing cultivation practices and improving the economic sustainability of flax production. Full article
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11 pages, 2024 KiB  
Article
Drying Behavior of Flax Stems at Different Degrees of Dew Retting Under Simulated Rainfall: Implications for Smart Agriculture and Sensor Development
by Ali Reda, Lionel Buchaillot and Steve Arscott
Agriculture 2025, 15(4), 395; https://doi.org/10.3390/agriculture15040395 - 13 Feb 2025
Viewed by 607
Abstract
Dew retting of flax stems is a key agricultural process which facilitates fiber extraction from parent stems. If sensors are to be developed to monitor the degree of retting for optimal fiber extraction, then stem characteristics such as water uptake and loss need [...] Read more.
Dew retting of flax stems is a key agricultural process which facilitates fiber extraction from parent stems. If sensors are to be developed to monitor the degree of retting for optimal fiber extraction, then stem characteristics such as water uptake and loss need to be accurately known. Here, the moisture uptake and drying behavior of short flax stem samples in different degrees of dew retting is studied. Their drying is characterized in laboratory conditions following simulated light and heavy rainfall. The data were accurately fitted with the Page model of moisture loss. It was observed that the drying rate constant of small flax stem samples is smaller for simulated light rain compared to simulated heavy rain. Also, over-retted stem samples dry more rapidly compared to under-retted samples. The findings suggest that this is due to the degradation of the external tissue of the stems observed in the over-retted samples. The results could be useful for laboratory testing of flax stems and designers of emerging technological sensor-based tools used to monitor the degree of retting in controlled conditions. Full article
(This article belongs to the Topic Crop Ecophysiology: From Lab to Field, 2nd Volume)
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16 pages, 5248 KiB  
Article
The Influence of Dew Retting on the Mechanical Properties of Single Flax Fibers Measured Using Micromechanical and Nanomechanical Approaches
by Ali Reda, Thomas Dargent, Louis Thomas, Sebastien Grec, Lionel Buchaillot and Steve Arscott
Fibers 2024, 12(10), 91; https://doi.org/10.3390/fib12100091 - 18 Oct 2024
Cited by 1 | Viewed by 1210
Abstract
The mechanical properties of single flax fibers are characterized here as a function of dew retting. The fibers are measured using micromechanical and nanomechanical techniques over a large retting period (91 days). Damage-free single flax fibers in various stages of dew retting were [...] Read more.
The mechanical properties of single flax fibers are characterized here as a function of dew retting. The fibers are measured using micromechanical and nanomechanical techniques over a large retting period (91 days). Damage-free single flax fibers in various stages of dew retting were manually extracted from retted flax plant stems. The flexural modulus and strength of the flax fibers were determined using micromechanical methods. The effective modulus of the outer surface of the single fibers was measured using AFM-based nanoindentation. The micromechanical methods revealed that the flexural modulus and strength of the manually extracted single fibers does not vary significantly as the retting progresses. The micromechanical methods revealed two distinct values of flexural strength in the fibers attributed to different failure modes. The values of these strengths do not vary significantly with retting or over-retting. The nanomechanical methods revealed that the effective modulus of the outer surface of the single fibers does evolve with retting. The physical/chemical origin of these observations remains to be established and could be the objective of future work. Full article
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23 pages, 6338 KiB  
Article
The Influence of the Chemical Composition of Flax and Hemp Fibers on the Value of Surface Free Energy
by Barbara Romanowska, Wanda Różańska and Małgorzata Zimniewska
Materials 2024, 17(5), 1104; https://doi.org/10.3390/ma17051104 - 28 Feb 2024
Cited by 11 | Viewed by 1854
Abstract
The article presents the exploration of flax and hemp fibers’ surface free energy depending on the chemical composition of the fiber, which is closely related to the plant variety and the method of extracting the fiber. For this purpose, tests of the surface [...] Read more.
The article presents the exploration of flax and hemp fibers’ surface free energy depending on the chemical composition of the fiber, which is closely related to the plant variety and the method of extracting the fiber. For this purpose, tests of the surface free energy (SFE), evaluation of the percentage content of individual fiber components and FTIR analyses were conducted. The research was carried out with the use of fibrous materials prepared in three different ways: 1. To analyze the effect of subsequent stages of flax fibers refining process on chemical composition and SFE, 2. to explore the dependence of fiber SFE on hemp variety, the water-retting hemp fibers were used, 3. To evaluate the influence of the retting method of hemp fibers BIAŁOBRZESKIE variety on SFE, the fibers extracted with the use of dew and water retting were used as the research material. The study confirmed that the content of individual components in the fiber influenced its sorption capacity and therefore determined its hydrophilic properties. The values of Pearson’s linear correlation coefficients determined in the statistical analysis proved that the surface free energy was strongly correlated with the content of individual components in the fibers. Understanding the wettability characteristics of bast fibers will allow modeling the properties of products made of these fibers and designing surface modification processes in order to obtain specific functionality of textile products, depending on their intended utilization. Full article
(This article belongs to the Section Polymeric Materials)
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25 pages, 11926 KiB  
Article
The Quantity and Quality of Flax and Hemp Fibers Obtained Using the Osmotic, Water-, and Dew-Retting Processes
by Wanda Różańska, Barbara Romanowska and Szymon Rojewski
Materials 2023, 16(23), 7436; https://doi.org/10.3390/ma16237436 - 29 Nov 2023
Cited by 15 | Viewed by 2557
Abstract
This study presents the quantity and quality of flax (Linum usitatissimum L.) and hemp (Cannabis sativa L.) fibers obtained depending on the fiber extraction method. The extraction methods used in this study were osmotic degumming, dew retting, and water retting. The [...] Read more.
This study presents the quantity and quality of flax (Linum usitatissimum L.) and hemp (Cannabis sativa L.) fibers obtained depending on the fiber extraction method. The extraction methods used in this study were osmotic degumming, dew retting, and water retting. The degummed straw was analyzed for fiber content, while the metrological, chemical, and physical properties were determined for the fibers obtained. It was shown that these properties change based on the method of fiber extraction used. The highest fiber content in the straw was obtained using the osmotic degumming method. These fibers are characterized by a light color, no unpleasant odor, low linear mass, good tenacity, lowest hygroscopicity, and reduced flammability compared to fibers obtained via the dew and water retting of straw. Full article
(This article belongs to the Special Issue Green Textile Materials: Fibers, Processing and Applications)
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17 pages, 4767 KiB  
Article
Production of Long Hemp Fibers Using the Flax Value Chain
by Lola Pinsard, Nathalie Revol, Henri Pomikal, Emmanuel De Luycker and Pierre Ouagne
Fibers 2023, 11(5), 38; https://doi.org/10.3390/fib11050038 - 28 Apr 2023
Cited by 9 | Viewed by 4960
Abstract
Hemp is finding a strong renewal of interest in the production of fine fibers for garment textiles. This resource of long-line fibers would come as a complement to the highly demanded flax fibers, whose large production in the north-west of Europe cannot be [...] Read more.
Hemp is finding a strong renewal of interest in the production of fine fibers for garment textiles. This resource of long-line fibers would come as a complement to the highly demanded flax fibers, whose large production in the north-west of Europe cannot be extended. In Normandy, where a complete industrial value chain exists for flax, it is intended to adapt it to hemp, and this was demonstrated from the field to the scutched fibers with a complete value chain. In this region, early harvesting is necessary to leave enough time for dew-retting and permit dry storage of stems before mid-September. An early-flowering variety (USO-31) was harvested using dedicated hemp equipment to obtain a 1 m parallel and aligned windrow that can be further processed by flax equipment. The scutching process as well as the fiber’s morphological and mechanical properties were particularly studied. Adapted scutching process parameters with reduced advancing speed and beating turbine velocity led to long fiber yields of about 18% of the stem mass. Stem yields were reaching about 6 tons/ha leading to a production of 1.1 tons/ha of long fibers. The tensile properties of the long fibers were highly sufficient for textile applications, and their thickness after hackling was in the range suitable for the production of fine yarns. Compared to other crops grown in Normandy, the hemp as produced in this 2020 case study provides good incomes to the farmer, higher than traditional crops such as wheat or barley, and the results of this study should encourage farmers to grow hemp for textile purposes. Full article
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21 pages, 2616 KiB  
Article
Development of 100% Linseed Flax Yarns with Improved Mechanical Properties and Durability for Geotextiles Applications
by Saif Ullah Khan, Mahadev Bar, Philippe Evon, Laurent Labonne and Pierre Ouagne
Fibers 2022, 10(12), 102; https://doi.org/10.3390/fib10120102 - 23 Nov 2022
Cited by 4 | Viewed by 2585
Abstract
Due to the ever-growing demand for bast fibres for technical and garment textiles, complementary sources to textile flax, whose cultivation in western Europe cannot really be extended, need to be proposed. In this study, the interest in harvesting and processing linseed flax straw [...] Read more.
Due to the ever-growing demand for bast fibres for technical and garment textiles, complementary sources to textile flax, whose cultivation in western Europe cannot really be extended, need to be proposed. In this study, the interest in harvesting and processing linseed flax straw is studied for geotextile applications. The main critical stages of fibre-to-yarn production for geotextiles were investigated. Different dew retting levels as well as different all-fibre extraction processes were investigated to achieve this objective. It was demonstrated that the fibres extracted from linseed flax stems subjected to 12 weeks of dew retting using breaking rollers, thresher and a breaking card exhibited the most suitable morphological and mechanical properties. The optimal fibres were converted into 100% linseed flax yarns using a flyer spinning machine, and the mechanical properties as well as the biodegradability of the linseed yarns were evaluated to understand their potential as geotextiles. These linseed flax yarns were further coated with linseed oil or chitosan to enhance their durability. It was observed that the linseed oil coating better preserved the yarn’s integrity and mechanical properties over time, and it permitted doubling their service life potential. Full article
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29 pages, 6139 KiB  
Review
Hemp Fibre Properties and Processing Target Textile: A Review
by Malgorzata Zimniewska
Materials 2022, 15(5), 1901; https://doi.org/10.3390/ma15051901 - 3 Mar 2022
Cited by 128 | Viewed by 17614
Abstract
Over the last several decades, Cannabis sativa L. has become one of the most fashionable plants. To use the hemp potential for the development of a sustainable textile bio-product sector, it is necessary to learn about the effect of the processes creating hemp’s [...] Read more.
Over the last several decades, Cannabis sativa L. has become one of the most fashionable plants. To use the hemp potential for the development of a sustainable textile bio-product sector, it is necessary to learn about the effect of the processes creating hemp’s value chain on fibre properties. This review presents a multi-perspective approach to industrial hemp as a resource delivering textile fibres. This article extensively explores the current development of hemp fibre processes including methods of fibre extraction and processing and comprehensive fibre characteristics to indicate the challenges and opportunities regarding Cannabis sativa L. Presented statistics prove the increasing interest worldwide in hemp raw material and hemp-based bio-products. This article discusses the most relevant findings in terms of the effect of the retting processes on the composition of chemical fibres resulting in specific fibre properties. Methods of fibre extraction include dew retting, water retting, osmotic degumming, enzymatic retting, steam explosion and mechanical decortication to decompose pectin, lignin and hemicellulose to remove them from the stem with varying efficiency. This determines further processes and proves the diversity of ways to produce yarn by employing different spinning systems such as linen spinning, cotton and wool spinning technology with or without the use of the decortication process. The aim of this study is to provide knowledge for better understanding of the textile aspects of hemp fibres and their relationship to applied technological processes. Full article
(This article belongs to the Special Issue Textile Biomaterials and Technology)
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16 pages, 823 KiB  
Article
Continuous Mechanical Extraction of Fibres from Linseed Flax Straw for Subsequent Geotextile Applications
by Saif Ullah Khan, Laurent Labonne, Pierre Ouagne and Philippe Evon
Coatings 2021, 11(7), 852; https://doi.org/10.3390/coatings11070852 - 15 Jul 2021
Cited by 9 | Viewed by 3774
Abstract
Linseed flax is a multipurpose crop. It is cultivated for its seeds and particularly for its oil. The main contributors for this crop are Canada, France and Belgium. In general, straws of linseed flax are buried in the fields or burnt. However, these [...] Read more.
Linseed flax is a multipurpose crop. It is cultivated for its seeds and particularly for its oil. The main contributors for this crop are Canada, France and Belgium. In general, straws of linseed flax are buried in the fields or burnt. However, these solutions are not good practices for the environment and from an economical point of view. In this study, straws of linseed flax (six batches in total) with different dew retting durations and harvesting techniques were studied to possibly use them for producing innovative geotextiles. Two different fibre extraction processes were investigated. A first process (A) involved horizontal breaker rollers and then a breaking card. A second one (B) consisted in using vertical breaker rollers, and an “all fibre” extraction device (fibre opener) followed by sieving. The chemical composition of fibres in parietal constituents appeared to be globally equivalent to the one of textile flax with a pectic content decreasing as a function of the dew retting duration. This contributed to an increase in the cellulose content. The fibre content was situated in a range from 29% to 33%, which corresponds to a good yield for linseed flax fibre. The level of purity can reach values of up to 90% for method A (without extra-sieving) and 96% for method B (with extra-sieving), and the length of the fibres (larger for method A than for method B) and their tensile properties make them suitable for structural geotextile yarn manufacturing. Full article
(This article belongs to the Special Issue Natural Fiber Based Composites)
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18 pages, 7587 KiB  
Article
Thermal and Mechanical Characteristics of Okra (Abelmoschus esculentus) Fibers Obtained via Water- and Dew-Retting
by Dawid Stawski, Ebru Çalişkan, Nazire Deniz Yilmaz and Izabella Krucińska
Appl. Sci. 2020, 10(15), 5113; https://doi.org/10.3390/app10155113 - 25 Jul 2020
Cited by 20 | Viewed by 5707
Abstract
In this research, fibers were extracted from different parts of the okra plant (Abelmoschus esculentus) via water- and dew-retting methods. The fibers were subjected to physical and thermal analyses. The fibers obtained from the upper part of the okra plant showed [...] Read more.
In this research, fibers were extracted from different parts of the okra plant (Abelmoschus esculentus) via water- and dew-retting methods. The fibers were subjected to physical and thermal analyses. The fibers obtained from the upper part of the okra plant showed higher breaking strength and lower linear density. Fibers obtained via water-retting exhibited higher breaking strength, higher elongation at break rates, and lower linear density values. The paper also presents the results of thermogravimetric analysis of the okra fibers. Tests were carried out in oxygen and inert gas atmospheres. Slight differences were found in the thermal resistance of the tested fibers, which was confirmed by an analysis using the αsr methodology. The calculated activation energy showed a widespread range of values. Full article
(This article belongs to the Special Issue Innovative Textiles in the Era of Circular Economy)
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25 pages, 4276 KiB  
Article
An Alternative to Field Retting: Fibrous Materials Based on Wet Preserved Hemp for the Manufacture of Composites
by Hans-Jörg Gusovius, Carsten Lühr, Thomas Hoffmann, Ralf Pecenka and Christine Idler
Agriculture 2019, 9(7), 140; https://doi.org/10.3390/agriculture9070140 - 3 Jul 2019
Cited by 13 | Viewed by 6579
Abstract
A process developed at the Leibniz Institute for Agricultural Engineering and Bioeconomy (ATB) for the supply and processing of wet-preserved fiber plants opens up new potential uses for such resources. The processing of industrial hemp into fiber materials and products thereof is undergoing [...] Read more.
A process developed at the Leibniz Institute for Agricultural Engineering and Bioeconomy (ATB) for the supply and processing of wet-preserved fiber plants opens up new potential uses for such resources. The processing of industrial hemp into fiber materials and products thereof is undergoing experimental research along the value-added chain from the growing process through to the manufacturing of product samples. The process comprises the direct harvesting of the field-fresh hemp and the subsequent anaerobic storage of the entire plant material. Thus, process risk due to unfavorable weather conditions is prevented in contrast to common dew retting procedures. The effects of the anaerobic storage processes on the properties of the bast part of the plant material are comparable to the results of common retting procedures. Harvest storage, as well as further mechanical processing, leads to different geometrical properties compared to the bast fibers resulting from traditional post harvesting treatment and decortication. The fiber raw material obtained in this way is well suited to the production of fiberboards and the reinforcement of polymer or mineral bonded composites. The objective of this paper is to present recent research results on final products extended by a comprehensive overview of the whole supply chain in order to enable further understanding of the result influencing aspects of prior process steps. Full article
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