Search Results (22)

This study analyzed the effect of a processing sequence comprising precision casting, heat treatment, and high-temperature plastic deformation on the microstructure and mechanical properties of the Haynes 282 nickel superalloy. The starting material was prepared in an industrial VIM IC induction furnace under vacuum conditions; the quality of the resulting castings, phase composition, thermal effects, and the alloy’s behavior during uniaxial compression were then evaluated. Castings in the form of rods with diameters of 10, 12, and 16 mm were produced at a molten alloy temperature of 1550 °C and a ceramic mold temperature of 1250 °C. The lowest porosity values, ranging from approximately 0.036–0.16%, were obtained for the vacuum furnace cooling variant, which was selected for further testing. DTA analysis revealed characteristic thermal effects in the range of 935.9–1379.8 °C, which enabled the selection of supersaturation parameters and a safe range for deformation tests. After supersaturation and aging, the samples were compressed at temperatures of 700–1200 °C at strain rates of 0.001 s⁻¹ and 0.008 s⁻¹. An increase in temperature caused a systematic decrease in maximum stress and yield stress, with the highest plastic resistance observed at temperatures of 700–800 °C. In this range, the microstructure exhibited characteristics of strong strain hardening, high dislocation density, and strain localization. At temperatures of 850–1000 °C, a transition to conditions of intense dynamic recovery and dynamic recrystallization was observed, whereas above 1050 °C, grain growth following recrystallization dominated. The most favorable compromise between reducing deformation resistance, minimizing the risk of cracking, and maintaining a finer microstructure was achieved in the 900–1000 °C range. The results indicate that the combination of precision casting and controlled thermomechanical working can serve as the basis for further optimization of the manufacturing technology for Haynes 282 superalloy semi-finished products. Full article

We investigate TiAlZrTaNb nitride coatings deposited on Haynes 282 nickel superalloy substrates via high-power impulse magnetron sputtering (HiPIMS) under varying substrate bias voltages (0 V to −75 V). The influence of substrate bias on the microstructure, morphology, hardness, and wear resistance was systematically analyzed using X-ray diffraction (XRD), scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS), nanoindentation, and ball-on-disk tribometry. The coatings exhibited a near equiatomic chemical composition with a face-centered cubic (FCC) crystal structure preferentially oriented along the (200) and (111) planes. Increasing the bias voltage reduced the grain size (3.65 nm to 2.84 nm) and lattice parameter (0.442 nm to 0.440 nm); meanwhile, the hardness (>45 GPa) and wear resistance were improved. The interplay between the deposition parameters and coating-substrate interactions are discussed in order to optimize HiPIMS-derived coatings for industrial applications. Full article

This work explores technical feasibility in hot isostatic pressing (HIP) manufacturing of an integral bimetallic component using steel and Ni alloy powder for supercritical carbon dioxide (sCO₂) turbomachinery. Lab-scale bimetallic HIP specimens using HAYNES^® 282^® and SS316L or SS415 powder are investigated in powder configuration, heat treatment, microstructure, and tensile properties up to 400 °C. Interdiffusion profiles at dissimilar alloy interfaces caused by HIP cycle is predicted by DICTRA simulations and validated by electron probe microanalysis (EPMA). The interdiffusion distance of most elements is around 100 μm, while C and N have a higher interdiffusion distance. Dense distribution of Ti-rich carbonitrides and alumina particles are found to decorate prior particle boundaries near joining interface on the 282 side, affecting tensile strength across interface as well as tensile failure location. A higher amount of excessive carbonitride formation near interface is observed in SS316L/282 than in SS415/282, which is consistent with the predicted greater degree of interdiffusion effect in SS316L/282. Typical HAYNES^® 282^® heat treatment condition is applicable to 282/SS316L and 282/SS415 combinations, resulting in a higher strength than cast CF8M and CA6NM. A pilot-scale bimetallic SS415/282 pipe is then demonstrated to show the promise of scaleup. Full article

Forging on an industrial scale often involves slow, size-limited cooling rates or high temperature hold times between, or after, deformation. This enables the dynamic recrystallization (DRX) initiated during forging to further progress under static conditions, a phenomenon called meta-dynamic recrystallization (mDRX). As mDRX will influence the final grain size, and thus properties, it is critical to understand and control it during processing. Here, we study the mDRX evolution in Ni-based superalloy Haynes 282 during post-deformation hold times of up to 120 s at 1080 °C after partial DRX. We find that mDRX is the dominating mechanisms responsible for the microstructure evolution the hold time. The very rapid mDRX kinetics in the initial stages suggest that quench delays (the time between the end of the deformation and the onset of the quenching intended to arrest the microstructure evolution) must be kept well below 1 s in order to allow reliable conclusions to be drawn from post-deformation microstructure investigations. A larger prior strain (larger DRX fraction) leads to faster mDRX kinetics and a larger final grain size. Larger strains leads to earlier impingement of the growing grains, which, in combination with smaller remaining deformed regions into which the grains can grow, limits the maximum size of the mDRX grains. We also note a close correlation between static recovery and stress relaxation during the hold time, whereas no such correlation between mDRX and stress relaxation can be observed. Full article

In this study, we examined the effects of an aluminization process on the microstructure and texture of Haynes 282 nickel samples fabricated using the direct metal laser sintering technique. The aluminization process involved the use of chemical vapor deposition with AlCl₃ vapors in a hydrogen atmosphere at a temperature of 1040 °C for 8 h. Following the 3D printing and aluminization steps, we analyzed the microstructure of the Haynes 282 nickel alloy samples using light microscopy and scanning electron microscopy. Additionally, we investigated the texture using X-ray diffractometry. A texture analysis revealed that after the process of direct laser sintering of metals, the texture of the Haynes 282 nickel alloy samples developed a texture typical of cast materials. Then, in the aluminization process, the texture was transformed—from foundry-type components to a texture characteristic of recrystallization. Full article

The paper investigates the influence of the ion-nitriding process on the microstructure, corrosion resistance, and tensile strength at elevated temperatures of Haynes 282 nickel superalloy specimens produced by the Direct Metal Laser Sintering (DMLS) technique. The study was performed for two conditions, i.e., as-built by DMLS method and as-built by DMLS method + covered by a layer containing CrN + Cr₂N phases. An analysis of the surface morphology revealed that the ion-nitriding process significantly affects the physical and chemical phenomena occurring on the specimen’s surface. The XRD measurement of the specimens showed that preparing them with the DMLS method as well as following a nitriding process produced residual tensile stresses. Based on the measurement of the nanohardness distribution through the layer approximatively of 7 μm in width and the superalloys substrate, the results of the nanohardness showed the maximum values of 27 GPa and 13.5 GPa for the nitrided layer and the substrate, respectively. The surface protection from the nitrided layer proved a positive effect on the corrosion resistance of the DMLS specimens in the solution of 0.1 M Na₂SO₄ + 0.1 M NaCl at room temperature. The results of the tensile tests at 750 °C showed that the ion-nitriding process did not significantly affect the elevated-temperature tensile strength of the superalloy specimens produced with the DMLS technique. Full article

Interactions in a multicomponent Ni-Cr-Mo-Al-Re model alloy were determined by ab initio calculations in order to investigate the Re doping effect on Haynes 282 alloys. Simulation results provided an understanding of short-range interactions in the alloy and successfully predicted the formation of a Cr and Re-rich phase. The Haynes 282 + 3 wt% Re alloy was manufactured using the additive manufacturing direct metal laser sintering (DMLS) technique, in which the presence of the (Cr₁₇Re₆)C₆ carbide was confirmed by an XRD study. The results provide useful information about the interactions between Ni, Cr, Mo, Al, and Re as a function of temperature. The designed five-element model can lead to a better understanding of phenomena that occur during the manufacture or heat treatment of modern, complex, multicomponent Ni-based superalloys. Full article

Direct energy deposition with arc and wire (DED-AW) is a versatile, low-cost, and energy-efficient technology for additive manufacturing of medium- and large-sized metallic components. In this study, the effects of arc energy and shielding gas in cold metal transfer (CMT) welding of walls and blocks on cooling time, mechanical properties, and macro- and microstructure have been studied using precipitation-hardenable Ni-based superalloy Haynes^® 282^®. The arc energy and consequently the cooling rate were varied by changing the wire feed rate and the travel speed. As expected, increasing the arc energy leads to higher cooling times for the walls. Due to the 2D thermal conduction, the thin walls cool down much slower than multi-layer welded blocks, but this reduces the strength values only very slightly. While the walls have no sensitivity to the occurrence of unacceptable seam irregularities, the multi-layer blocks show isolated seam defects, such as hot cracks or lack of fusion. Despite shielding gas variation, the as-welded blocks show acceptable strength properties at room temperatures (RT) and impact values at RT and −196 °C. However, the use of an N-containing shielding gas results in lower elongation and notched bar impact energy. Precipitation-hardened specimens tested at 871 °C exhibit a similar strength level to transverse tensile specimens of gas metal arc welding (GMAW) welded joints on 12.7 mm thick plates with fracture in the weld metal. Full article

The article presents the results of research on the influence of plastic deformation on the microstructure and tensile strength of Haynes 282 nickel superalloy produced by direct metal laser sintering (DMLS) and a conventional technique (casting). Samples were tested for dimensional accuracy using a 3D scanner. Then, the samples were subjected to plastic deformation by rolling. The microstructures of the DMLS and the as-cast samples were analysed using a scanning electron microscope. The strength properties of the samples were determined in a static tensile test. Microhardness measurements of the samples were also performed. Based on the analysis of the dimensional accuracy, it was found that the surface quality of the components produced by DMLS is dependent on the input parameters of the 3D printing process. Using the DMLS method, it is possible to produce Haynes 282 with a fine-crystalline microstructure containing dendrites. The fine-crystalline dendritic microstructure and low porosity showed very good tensile strength compared to the as-cast material. It was also found that the increase in the degree of plastic deformation of the as-cast Haynes 282 and the samples produced by the DMLS technique resulted in an increase in the strength of the tested samples, with reduced ductility. Full article

Despite the interest of industry in nickel-based superalloys and its main features (high temperatures resistance, hardness, low thermal conductivity, among others), even today they are still materials that are difficult to cut. Cutting tools withstand both high pressures and temperatures highly localized at the cutting area because of the elevated work hardening of the alloy and the problems for the cutting fluid to access the region, with the consequent strong tool wear. The use of cutting fluids at high pressures improves coolant access and heat removal. This paper analyzed the machining of Haynes 282 alloy by means of coated carbide tools under high-pressure cutting fluids at finishing conditions. Tests were developed at different cutting speeds and feeds quantifying the machining forces, surface roughness, tool wear, and tool life. Values of 45.9 min and R_a between 2 µm and 1 µm were obtained in this study for tool life and roughness, respectively, for the combination of cutting speed 50 m/min and feed 0.1 mm/rev. Likewise, a comparative analysis is included with the results obtained in previous works developed by the authors relating to the finishing turning of Haynes 282 and Inconel 718 under conventional pressure cooling. The comparative analysis with Inconel 718 is included in the study due to its importance within the nickel base superalloys being widely used in industry and widely analyzed in scientific literature. Full article

Haynes 282 has attracted attention for casting applications in AUSC power plants due to its good creep properties. However, the market is primarily comprised of wrought Haynes 282, while the cast version is not commercially available. In this study, the microstructure of a large traditional sand cast Haynes 282 was studied from as-cast condition to long-term heat-treated condition by combining experimental data and thermodynamic calculations. The microstructure of a large cast Haynes 282 includes γ, γ’, two types of MX, M₂₃C₆ and µ phases. After standard post heat treatment, µ phases were dissolved and precipitated as M₆C. The equilibrium state was achieved after 266 h aging at 788 °C, after which γ’ particles began coarsening. These kept to a spherical morphology; the smallest misfit was found with the γ matrix. Once post heat treatment was finished, MX exhibited little morphology and compositional change during the long-term isothermal aging. Grain boundary is covered by discrete M₂₃C₆ and M₆C precipitates and this morphology keeps stable during isothermal aging. No presence of the needle µ phase have been found at grain boundaries after 10,000 h aging at 788 °C. All these microstructural features indicated that cast Haynes 282 could have a high thermal stability and good creep properties. Full article

This study investigated the microstructural evolution of the weld interface and creep fracture behavior of 10% Cr martensitic steel welds using Haynes 282 filler metal. The welded joints were subjected to post-weld heat treatment (PWHT) at temperatures of 738 °C for 4, 8, and 15 h. Creep tests were carried out at 600 °C under stress of 200 MPa. The creep rupture life increased with an increase in holding time for PWHT up to 8 h compared to the as-welded condition. However, when the holding time for PWHT was further increased to 15 h, creep properties (i.e., rupture life and creep strain) decreased considerably, and the failure location was found to shift from the ICHAZ to the weld interface. The microstructural investigation revealed that Type I carbides precipitated at the weld interface and recrystallized grains with Cr depletion were formed near Type I carbides in the partially mixed zone during creep exposure. The creep failure at the weld interface began on the surface and propagated inward through the recrystallized grains of the weld-interface region. Full article

This study investigated the effect of postweld heat treatment (PWHT) conditions on Type IV failure behavior of 10% Cr martensitic steel welds using Haynes 282 filler. The welded joints were subjected to PWHT at temperatures of 688, 738, and 788 °C for 4 and 8 h. Creep tests were carried out at 600 °C under a stress of 200 MPa. The as-welded joint without PWHT showed Type IV cracking due to growth of voids around Laves phase by localized creep deformation in the intercritical heat-affected zone (ICHAZ). The creep properties of the PWHTed joints at 688 °C were similar to those of the as-welded joints without PWHT. On the other hand, the PWHTed joints at 738 °C exhibited a significantly longer creep life by a lower amount of Laves phase in the ICHAZ than those at 688 °C; this could be a result of the homogenization of ICHAZ microstructure during PWHT at 738 °C. However, the PWHT at 688 and 738 °C showed the same Type IV creep failure mode. Meanwhile, the PWHTed joints at 788 °C exhibited the shortest creep life in this study. The failure location was shifted to the base metal away from the HAZ, and severe plastic deformation occurred due to the softened matrix by excessive tempering. Full article

Thermomechanical processes, such as forging, are important steps during manufacturing of superalloy components. The microstructural development during processing, which controls the final component properties, is complex and depends on e.g., applied strain, strain rate and temperature. In this study, we investigate the effect of process parameters on the dynamic and post-dynamic recrystallization during hot compression of Ni-base superalloy Haynes 282. Specifically, we address the effect of deformation below the grain boundary carbide solvus temperature. During deformation, discontinuous and continuous dynamic recrystallization was observed at the grain boundaries, and particle-stimulated nucleation occurred at primary carbides. Strain rate was determined to be the governing factor controlling the recrystallization fraction for strain rates up to 0.5 s⁻¹ above which adiabatic heating became the dominating factor. Careful examination of the temperature development during deformation showed that the response of the closed-loop temperature control system to adiabatic heating can have important effects on the interpretation of the observed behavior. During a 90 s post-deformation hold, grain growth and an increasing fraction of twin boundaries significantly changed the deformation-induced microstructure and texture. The microstructure developed during post-dynamic recrystallization was mainly controlled by the temperature and only weakly coupled to the prior deformation step. Full article

A novel repair strategy based on decoupled heat source for increasing the productivity of wire-assisted pulsed laser cladding of the γ’-precipitation strengthening nickel-base superalloys Inconel 738 low carbon (IN 738 LC, base material) and Haynes 282 (HS 282, filler material) is presented. The laser beam welding process is supported by the hot-wire technology. The additional energy is utilized to increase the deposition rate of the filler material by increasing feeding rates and well-defining the thermal management in the welding zone. The simultaneous application of laser pulse modulation allows the precise control of the temperature gradients to minimize the hot-crack formation. Accompanying investigations such as high-speed recordings and numerical simulations allow a generalized statement on the influence of the adapted heat management on the resulting weld seam geometry (dilution, aspect ratio and wetting angle) as well as the formation of hot-cracks and lack of fusion between base and filler material. Statistical analysis of the data—the input parameters like laser pulse energy, pulse shape, hot-wire power and wire-feeding rate in conjunction with the objectives like dilution, aspect ratio, wetting angle and hot-cracking behavior—revealed regression functions to predict certain weld seam properties and hence the required input parameters. Full article