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Authors = Elsa Díaz-Montes ORCID = 0000-0002-3016-9937

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32 pages, 2361 KiB  
Review
Advances in the Preservation of Plant-Based Pigments via Spray Drying—A Systematic Review
by Elsa Díaz-Montes
Processes 2025, 13(3), 663; https://doi.org/10.3390/pr13030663 - 26 Feb 2025
Cited by 3 | Viewed by 2106
Abstract
Natural pigments derived from plant sources are notable not only for their vibrant colors but also for their nutritional value and proven biological activities. Spray drying has emerged as an efficient and cost-effective encapsulation technique, offering significant advantages such as enhanced stability, improved [...] Read more.
Natural pigments derived from plant sources are notable not only for their vibrant colors but also for their nutritional value and proven biological activities. Spray drying has emerged as an efficient and cost-effective encapsulation technique, offering significant advantages such as enhanced stability, improved handling properties, and protection against degradation. The diverse range of natural wall materials (e.g., polysaccharides, proteins, and lipids) and the variability in spray drying operating conditions provide numerous possibilities to optimize encapsulation processes. The aim of this systematic review was to evaluate and compare the key factors influencing spray drying encapsulation of plant-based pigments. ResearchGate, Scopus, and Google Scholar were searched between July and December 2024. Data extraction was performed manually using a standardized form to collect information on plant source, pigment type, wall materials (type and concentration), spray drying conditions (in-let/outlet temperatures and feed flow rate), and process results (encapsulation efficiency, process yield, and total pigment content). Future advances in spray drying should focus on the optimization of spray drying conditions. Furthermore, innovations in spray drying formulations, such as customized combinations of polysaccharides and proteins or the incorporation of emulsifiers, could lead to more effective and scalable encapsulation processes, supporting the development of high-performance stable pigments for food, cosmetic, and pharmaceutical applications. Full article
(This article belongs to the Special Issue Advanced Drying Technologies in Food Processing)
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26 pages, 1941 KiB  
Review
Wall Materials for Encapsulating Bioactive Compounds via Spray-Drying: A Review
by Elsa Díaz-Montes
Polymers 2023, 15(12), 2659; https://doi.org/10.3390/polym15122659 - 12 Jun 2023
Cited by 41 | Viewed by 10454
Abstract
Spray-drying is a continuous encapsulation method that effectively preserves, stabilizes, and retards the degradation of bioactive compounds by encapsulating them within a wall material. The resulting capsules exhibit diverse characteristics influenced by factors such as operating conditions (e.g., air temperature and feed rate) [...] Read more.
Spray-drying is a continuous encapsulation method that effectively preserves, stabilizes, and retards the degradation of bioactive compounds by encapsulating them within a wall material. The resulting capsules exhibit diverse characteristics influenced by factors such as operating conditions (e.g., air temperature and feed rate) and the interactions between the bioactive compounds and the wall material. This review aims to compile recent research (within the past 5 years) on spray-drying for bioactive compound encapsulation, emphasizing the significance of wall materials in spray-drying and their impact on encapsulation yield, efficiency, and capsule morphology. Full article
(This article belongs to the Collection Polymer/Biopolymer Stabilization and Degradation)
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15 pages, 1925 KiB  
Review
Polysaccharide-Based Biodegradable Films: An Alternative in Food Packaging
by Elsa Díaz-Montes
Polysaccharides 2022, 3(4), 761-775; https://doi.org/10.3390/polysaccharides3040044 - 25 Nov 2022
Cited by 15 | Viewed by 7928
Abstract
Packaging can mitigate the physical, chemical, and microbiological phenomena that affects food products’ quality and acceptability. However, the use of conventional packaging from non-renewable fossil sources generates environmental damage caused by the accumulation of non-biodegradable waste. Biodegradable films emerge as alternative biomaterials which [...] Read more.
Packaging can mitigate the physical, chemical, and microbiological phenomena that affects food products’ quality and acceptability. However, the use of conventional packaging from non-renewable fossil sources generates environmental damage caused by the accumulation of non-biodegradable waste. Biodegradable films emerge as alternative biomaterials which are ecologically sustainable and offer protection and increase food product shelf life. This review describes the role of biodegradable films as packaging material and their importance regarding food quality. The study emphasizes polysaccharide-based biodegradable films and their use in foods with different requirements and the advances and future challenges for developing intelligent biodegradable films. In addition, the study explores the importance of the selection of the type of polysaccharide and its combination with other polymers for the generation of biodegradable films with functional characteristics. It also discusses additives that cause interactions between components and improve the mechanical and barrier properties of biodegradable films. Finally, this compilation of scientific works shows that biodegradable films are an alternative to protecting perishable foods, and studying and understanding them helps bring them closer to replacing commercial synthetic packaging. Full article
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22 pages, 1471 KiB  
Review
Polysaccharides: Sources, Characteristics, Properties, and Their Application in Biodegradable Films
by Elsa Díaz-Montes
Polysaccharides 2022, 3(3), 480-501; https://doi.org/10.3390/polysaccharides3030029 - 27 Jun 2022
Cited by 64 | Viewed by 13403
Abstract
Biodegradable films emerge as alternative biomaterials to conventional packaging from fossil sources, which, in addition to offering protection and increasing the shelf life of food products, are ecologically sustainable. The materials mostly used in their formulation are based on natural polysaccharides, plasticizing agents, [...] Read more.
Biodegradable films emerge as alternative biomaterials to conventional packaging from fossil sources, which, in addition to offering protection and increasing the shelf life of food products, are ecologically sustainable. The materials mostly used in their formulation are based on natural polysaccharides, plasticizing agents, and bioactive components (e.g., antimicrobial agents or antioxidants). The formulation of biodegradable films from polysaccharides and various plasticizers represents an alternative for primary packaging that can be assigned to specific food products, which opens the possibility of having multiple options of biodegradable films for the same product. This review describes the main characteristics of the most abundant polysaccharides in nature and highlights their role in the formulation of biodegradable films. The compilation and discussion emphasize studies that report on the mechanical and barrier properties of biodegradable films when made from pure polysaccharides and when mixed with other polysaccharides and plasticizing agents. Full article
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12 pages, 1472 KiB  
Review
Dextran: Sources, Structures, and Properties
by Elsa Díaz-Montes
Polysaccharides 2021, 2(3), 554-565; https://doi.org/10.3390/polysaccharides2030033 - 1 Jul 2021
Cited by 205 | Viewed by 30633
Abstract
Dextran is an exopolysaccharide (EPS) synthesized by lactic acid bacteria (LAB) or their enzymes in the presence of sucrose. Dextran is composed of a linear chain of d-glucoses linked by α-(1→6) bonds, with possible branches of d-glucoses linked by α-(1→4), α-(1→3), [...] Read more.
Dextran is an exopolysaccharide (EPS) synthesized by lactic acid bacteria (LAB) or their enzymes in the presence of sucrose. Dextran is composed of a linear chain of d-glucoses linked by α-(1→6) bonds, with possible branches of d-glucoses linked by α-(1→4), α-(1→3), or α-(1→2) bonds, which can be low (<40 kDa) or high molecular weight (>40 kDa). The characteristics of dextran in terms of molecular weight and branches depend on the producing strain, so there is a great variety in its properties. Dextran has commercial interest because its solubility, viscosity, and thermal and rheological properties allow it to be used in food, pharmaceutical, and research areas. The aim of this review article is to compile the latest research (in the past decade) using LAB to synthesize high or low molecular weight dextran. In addition, studies using modified enzymes to produce dextran with specific structural characteristics (molecular weights and branches) are addressed. On the other hand, special attention is paid to LAB extracted from unconventional sources to expose their capacities as dextran producers and their possible application to compete with the only commercial strain (Leuconostoc mesenteroides NRRL B512). Full article
(This article belongs to the Collection Current Opinion in Polysaccharides)
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24 pages, 3237 KiB  
Review
Trends in Chitosan as a Primary Biopolymer for Functional Films and Coatings Manufacture for Food and Natural Products
by Elsa Díaz-Montes and Roberto Castro-Muñoz
Polymers 2021, 13(5), 767; https://doi.org/10.3390/polym13050767 - 1 Mar 2021
Cited by 95 | Viewed by 8196
Abstract
Some of the current challenges faced by the food industry deal with the natural ripening process and the short shelf-life of fresh and minimally processed products. The loss of vitamins and minerals, lipid oxidation, enzymatic browning, and growth of microorganisms have been the [...] Read more.
Some of the current challenges faced by the food industry deal with the natural ripening process and the short shelf-life of fresh and minimally processed products. The loss of vitamins and minerals, lipid oxidation, enzymatic browning, and growth of microorganisms have been the main issues for many years within the innovation and improvement of food packaging, which seeks to preserve and protect the product until its consumption. Most of the conventional packaging are petroleum-derived plastics, which after product consumption becomes a major concern due to environmental damage provoked by their difficult degradation. In this sense, many researchers have shown interest in edible films and coatings, which represent an environmentally friendly alternative for food packaging. To date, chitosan (CS) is among the most common materials in the formulation of these biodegradable packaging together with polysaccharides, proteins, and lipids. The good film-forming and biological properties (i.e., antimicrobial, antifungal, and antiviral) of CS have fostered its usage in food packaging. Therefore, the goal of this paper is to collect and discuss the latest development works (over the last five years) aimed at using CS in the manufacture of edible films and coatings for food preservation. Particular attention has been devoted to relevant findings in the field, together with the novel preparation protocols of such biodegradable packaging. Finally, recent trends in new concepts of composite films and coatings are also addressed. Full article
(This article belongs to the Special Issue Biopolymers: Recent Progress and New Perspectives)
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26 pages, 2244 KiB  
Review
Edible Films and Coatings as Food-Quality Preservers: An Overview
by Elsa Díaz-Montes and Roberto Castro-Muñoz
Foods 2021, 10(2), 249; https://doi.org/10.3390/foods10020249 - 26 Jan 2021
Cited by 310 | Viewed by 25515
Abstract
Food preservation technologies are currently facing important challenges at extending the shelf-life of perishable food products (e.g., meat, fish, milk, eggs, and many raw fruits and vegetables) that help to meet the daily nutrient requirement demand. In addition, food preservation has gone beyond [...] Read more.
Food preservation technologies are currently facing important challenges at extending the shelf-life of perishable food products (e.g., meat, fish, milk, eggs, and many raw fruits and vegetables) that help to meet the daily nutrient requirement demand. In addition, food preservation has gone beyond only preservation; the current techniques are focused on the fulfillment of two additional objectives, the suitability of the used processes and generation of environmentally friendly products with non-presence of any side effect on health. Moreover, they are also looking for additional nutritional properties. One of these preservation protocols deals with the use of edible films and coatings. Therefore, this review shows an overview of synthetic materials (e.g., glass, aluminum, plastic, and paperboard), as well as the regulations that limit their application in food packaging. Further, this review releases the current-state-of-the-art of the use of films and edible coatings as an alternative to conventional packaging, providing the main features that these biodegradable packaging should meet towards specific uses for the conservation and improvement of various food products. Herein, particular attention has been paid to the main used components (e.g., biopolymers, additives, bioactive, and probiotic components), manufacturing methods (for edible films or coatings) and their application to specific products. In addition, an outlook of the application of edible films and coatings as quality indicators of perishable products is shown. Full article
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