Influence of Alcohol Content and Storage Conditions on the Physicochemical Stability of Spirit Drinks
Abstract
:1. Introduction
2. Materials and Methods
2.1. Raw Materials
2.2. Preparation of Samples
2.3. Turbidity Measurement
2.4. Chromatographic Analysis
- 1-propanol (monitored ions: 31 m/z, 59 m/z, 42 m/z).
- Ethyl acetate (monitored ions: 43 m/z, 61 m/z, 45 m/z).
- 2-methyl-1-propanol (monitored ions: 43 m/z, 41 m/z, 42 m/z).
- 3-methyl-1-butanol (monitored ions: 55 m/z, 70 m/z, 42 m/z).
- 2-methyl-1-butanol (monitored ions: 57 m/z, 56 m/z, 41 m/z).
- Isoamyl acetate (monitored ions: 43 m/z, 70 m/z, 55 m/z).
- Ethyl hexanoate (monitored ions: 88 m/z, 43 m/z, 99 m/z).
- Ethyl octanoate (monitored ions: 88 m/z, 101 m/z, 43 m/z).
- Ethyl decanoate (monitored ions: 88 m/z, 101 m/z, 60 m/z).
- Ethyl tetradecanoate (monitored ions: 88 m/z, 101 m/z, 43 m/z).
- Acetaldehyde diethyl acetal (monitored ions: 43 m/z, 103 m/z, 73 m/z).
2.5. Statistical Analysis
3. Results and Discussion
3.1. Turbidity Measurements of the Distillates during Storage
3.2. Chromatographic Analysis of Distillates during Storage
3.2.1. Aldehydes and Alcohols
3.2.2. Acetals and Esters
4. Conclusions
Author Contributions
Funding
Conflicts of Interest
References
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(% v/v) | Temp. (°C) | Time (Weeks) | Formazin Turbidity Unit (FTU) | |
---|---|---|---|---|
Rye Distillate | Plum Distillate | |||
40 | Control sample | 0.00 a ± 0.00 | 0.02 a ± 0.00 | |
20 | 4 | 0.01 b ± 0.00 | 1.37 c ± 0.00 | |
8 | 0.05 c ± 0.00 | 1.70 d ± 0.01 | ||
8 | 4 | 0.02 b ± 0.00 | 3.22 h ± 0.02 | |
8 | 0.15 d ± 0.00 | 4.91 i ± 0.01 | ||
0 | 4 | 0.02 b ± 0.00 | 5.58 k ± 0.02 | |
8 | 0.55 g ± 0.01 | 6.26 l ±0.02 | ||
−18 | 4 | 0.02 b ± 0.00 | 5.41 j ± 0.02 | |
8 | 0.59 h ± 0.00 | 6.39 m ± 0.02 | ||
50 | Control sample | 0.00 a ± 0.00 | 0.00 a ± 0.00 | |
20 | 4 | 0.00 a ± 0.00 | 0.00 a ± 0.00 | |
8 | 0.02 b ± 0.00 | 0.00 a ± 0.00 | ||
8 | 4 | 0.00 a ± 0.00 | 0.02 a ± 0.00 | |
8 | 0.15 d ± 0.00 | 2.55 e ± 0.01 | ||
0 | 4 | 0.00 a ± 0.00 | 0.00 a ± 0.00 | |
8 | 0.38 e ± 0.01 | 2.69 f ± 0.02 | ||
−18 | 4 | 0.00 a ± 0.00 | 0.00 a ± 0.00 | |
8 | 0.44 f ± 0.00 | 2.78 g ± 0.02 | ||
70 | Control sample | 0.00 a ± 0.00 | 0.00 a ± 0.00 | |
20 | 4 | 0.00 a ± 0.00 | 0.00 a ± 0.00 | |
8 | 0.00 a ± 0.00 | 0.00 a ± 0.00 | ||
8 | 4 | 0.00 a ± 0.00 | 0.02 a ± 0.00 | |
8 | 0.00 a ± 0.00 | 0.09 b ± 0.00 | ||
0 | 4 | 0.00 a ± 0.00 | 0.00 a ± 0.00 | |
8 | 0.00 a ± 0.00 | 0.11 b ± 0.00 | ||
−18 | 4 | 0.00 a ± 0.00 | 0.00 a ± 0.00 | |
8 | 0.00 a ± 0.00 | 0.11 b ± 0.00 |
ABV (% v/v) | Temp. (°C) | Time (Weeks) | Compound Concentration (mg/L Alcohol 100% v/v) | |||||
---|---|---|---|---|---|---|---|---|
Acetaldehyde | Methanol | 1-Propanol | 2-Methyl- 1-Propanol | 3-Methyl- 1-Butanol | 2-Methyl- 1-Butanol | |||
Control sample | 12.52 k | 300.41 abc | 521.00 i | 699.09 i | 481.46 i | 182.89 h | ||
±0.02 | ±0.65 | ±2.22 | ±0.35 | ±0.51 | ±2.00 | |||
40 | 20 | 4 | 11.30 g | 299.50 ab | 507.60 gh | 698.76 i | 463.27 ef | 177.49 defgh |
±0.04 | ±0.53 | ±3.11 | ±1.66 | ±3.25 | ±2.57 | |||
8 | 10.51 e | 300.70 abc | 483.98 de | 697.71 i | 456.22 cde | 173.64 cdefg | ||
±0.00 | ±1.04 | ±2.48 | ±3.25 | ±2.60 | ±1.42 | |||
8 | 4 | 12.43 k | 300.29 abc | 511.45 ghi | 692.65 i | 463.51 ef | 175.65 cdefgh | |
±0.04 | ±0.87 | ±1.85 | ±0.91 | ±0.92 | ±0.46 | |||
8 | 11.86 i | 303.20 cd | 478.89 bcd | 656.91 bcde | 457.02 cde | 172.94 cdefg | ||
±0.05 | ±0.99 | ±2.69 | ±4.62 | ±2.57 | ±1.48 | |||
0 | 4 | 12.43 k | 299.65 ab | 517.98 hi | 676.07 gh | 448.98 abc | 171.85 cdef | |
±0.02 | ±0.45 | ±5.20 | ±4.31 | ±4.46 | ±0.82 | |||
8 | 11.30 g | 301.67 abc | 491.44 ef | 670.55 fgh | 445.87 ab | 169.33 bcd | ||
±0.07 | ±0.61 | ±2.22 | ±1.48 | ±1.97 | ±2.36 | |||
−18 | 4 | 12.43 k | 299.46 ab | 502.27 fg | 674.98 gh | 449.94 abc | 167.97 bc | |
±0.03 | ±0.58 | ±6.48 | ±3.53 | ±3.82 | ±2.44 | |||
8 | 11.30 g | 300.61 abc | 479.37 cd | 665.19 defg | 444.02 a | 162.06 b | ||
±0.03 | ±0.50 | ±2.43 | ±3.11 | ±0.90 | ±0.72 | |||
50 | 20 | 4 | 10.85 f | 300.44 abc | 485.56 de | 698.58 i | 474.94 ghi | 178.58 efgh |
±0.02 | ±0.76 | ±2.22 | ±1.98 | ±2.34 | ±2.66 | |||
8 | 10.56 e | 300.62 abc | 471.52 abc | 697.64 i | 475.39 ghi | 173.53 cdefg | ||
±0.06 | ±0.28 | ±2.35 | ±1.14 | ±2.84 | ±1.56 | |||
8 | 4 | 12.20 j | 302.16 bc | 478.90 bcd | 666.53 efg | 459.29 de | 174.12 cdefgh | |
±0.03 | ±0.60 | ±5.27 | ±2.79 | ±4.33 | ±1.45 | |||
8 | 11.75 hi | 301.24 abc | 468.93 abc | 650.51 bc | 449.94 abc | 170.83 bcde | ||
±0.05 | ±1.14 | ±1.01 | ±3.60 | ±1.52 | ±1.71 | |||
0 | 4 | 11.75 hi | 301.08 abc | 466.71 a | 649.65 bc | 470.43 fg | 169.21 bcd | |
±0.02 | ±0.75 | ±2.35 | ±3.41 | ±3.79 | ±2.63 | |||
8 | 11.75 hi | 303.18 cd | 461.04 a | 631.98 a | 450.52 abc | 168.78 bcd | ||
±0.02 | ±0.75 | ±2.21 | ±3.28 | ±3.65 | ±2.47 | |||
−18 | 4 | 12.20 j | 298.46 a | 467.18 ab | 654.77 bcd | 456.43 cde | 170.34 bcde | |
±0.06 | ±0.89 | ±0.87 | ±2.12 | ±2.09 | ±3.08 | |||
8 | 9.94 c | 299.62 ab | 467.15 ab | 648.83 b | 452.70 bcd | 170.34 bcde | ||
±0.03 | ±1.40 | ±1.31 | ±1.07 | ±1.60 | ±2.01 | |||
70 | 20 | 4 | 10.33 d | 302.31 bc | 511.35 ghi | 678.64 h | 475.30 ghi | 180.04 fgh |
±0.04 | ±0.63 | ±3.52 | ±5.98 | ±2.27 | ±1.53 | |||
8 | 10.27 d | 302.65 bc | 510.14 ghi | 671.49 gh | 471.15 fg | 98.58 a | ||
±0.05 | ±0.59 | ±3.56 | ±2.21 | ±1.42 | ±1.05 | |||
8 | 4 | 7.43 a | 303.15 cd | 520.03 i | 671.94 gh | 474.85 ghi | 181.41 gh | |
±0.03 | ±0.91 | ±3.70 | ±1.94 | ±2.67 | ±2.32 | |||
8 | 7.32 a | 306.25 d | 510.21 ghi | 668.09 fgh | 469.88 fg | 98.22 a | ||
±0.04 | ±0.92 | ±1.20 | ±1.31 | ±2.02 | ±2.30 | |||
0 | 4 | 11.62 h | 303.03 cd | 520.01 i | 660.18 cdef | 477.48 ghi | 175.08 cdefgh | |
±0.08 | ±1.16 | ±5.01 | ±1.21 | ±2.15 | ±5.61 | |||
8 | 9.69 b | 303.39 cd | 514.67 hi | 657.07 bcde | 472.82 gh | 98.98 a | ||
±0.07 | ±1.12 | ±2.13 | ±5.21 | ±1.25 | ±0.86 | |||
−18 | 4 | 10.98 f | 302.48 bc | 518.47 hi | 647.04 b | 480.70 hi | 175.28 cdefgh | |
±0.07 | ±1.00 | ±3.47 | ±6.64 | ±1.38 | ±3.20 | |||
8 | 9.69 b | 302.74 bc | 509.39 ghi | 634.49 a | 479.77 hi | 97.49 a | ||
±0.04 | ±1.68 | ±4.34 | ±3.76 | ±1.47 | ±2.01 |
ABV (% v/v) | Temp. (°C) | Time (Weeks) | Compound Concentration (mg/L Alcohol 100% v/v) | |||||
---|---|---|---|---|---|---|---|---|
Acetaldehyde | Methanol | 1-Propanol | 2-Methyl- 1-Propanol | 3-Methyl- 1-Butanol | 2-Methyl- 1-Butanol | |||
Control sample | 146.67 l | 75.92 ab | 127.46 h | 875.14 l | 3098.98 i | 672.28 k | ||
±0.45 | ±0.79 | ±0.78 | ±4.53 | ±15.84 | ±3.80 | |||
40 | 20 | 4 | 128.68 ijk | 75.70 ab | 124.96 gh | 873.64 l | 3003.94 hi | 668.64 jk |
±0.66 | ±0.75 | ±1.20 | ±2.42 | ±37.01 | ±3.15 | |||
8 | 114.61 g | 76.45 ab | 119.92 ef | 808.41 a | 2792.94 def | 649.06 gh | ||
±1.21 | ±0.94 | ±1.18 | ±3.23 | ±40.31 | ±3.69 | |||
8 | 4 | 129.96 jk | 76.28 ab | 120.34 ef | 871.89 l | 2989.13 hi | 660.01 hijk | |
±1.14 | ±0.95 | ±0.67 | ±4.62 | ±59.00 | ±3.60 | |||
8 | 126.41 ij | 75.10 ab | 112.65 bc | 862.07 hijkl | 2836.86 efg | 648.92 gh | ||
±1.60 | ±0.59 | ±0.46 | ±2.84 | ±36.73 | ±3.34 | |||
0 | 4 | 125.86 i | 74.08 ab | 120.81 ef | 866.96 kl | 2982.56 hi | 666.21 ijk | |
±1.24 | ±0.34 | ±0.50 | ±1.88 | ±27.56 | ±2.62 | |||
8 | 120.93 h | 75.09 ab | 114.96 cd | 863.48 ijkl | 2825.16 efg | 658.99 hijk | ||
±0.91 | ±1.21 | ±1.23 | ±2.13 | ±39.98 | ±4.04 | |||
−18 | 4 | 128.87 ijk | 75.76 ab | 117.24 de | 848.44 fgh | 2928.18 gh | 645.99 fgh | |
±1.09 | ±0.86 | ±0.57 | ±3.02 | ±24.54 | ±3.52 | |||
8 | 115.29 g | 75.62 ab | 115.07 cd | 846.76 fg | 2780.53 cdef | 631.06 f | ||
±1.03 | ±1.10 | ±1.23 | ±3.16 | ±43.35 | ±3.73 | |||
50 | 20 | 4 | 130.95 k | 75.57 ab | 126.53 h | 866.64 jkl | 2996.43 hi | 659.69 hijk |
±1.44 | ±0.88 | ±0.70 | ±3.60 | ±34.95 | ±3.55 | |||
8 | 118.46 gh | 77.30 b | 127.84 h | 853.20 fghijk | 2684.76 abcd | 557.09 cde | ||
±1.18 | ±1.05 | ±1.78 | ±4.33 | ±46.84 | ±5.81 | |||
8 | 4 | 116.29 g | 75.37 ab | 108.98 ab | 849.06 fghi | 2983.47 hi | 670.15 jk | |
±1.20 | ±0.60 | ±0.45 | ±3.05 | ±35.97 | ±4.54 | |||
8 | 103.26 f | 75.85 ab | 105.24 a | 846.25 fg | 2719.84 bcde | 571.73 e | ||
±0.83 | ±1.02 | ±1.14 | ±2.85 | ±47.08 | ±3.59 | |||
0 | 4 | 107.02 f | 75.64 ab | 111.15 bc | 849.78 fghi | 2984.04 hi | 655.80 hij | |
±2.32 | ±0.28 | ±1.64 | ±2.15 | ±44.51 | ±2.96 | |||
8 | 90.32 e | 74.37 ab | 110.49 b | 847.12 fgh | 2696.42 bcd | 562.38 de | ||
±0.47 | ±0.91 | ±0.97 | ±5.20 | ±25.19 | ±2.30 | |||
−18 | 4 | 115.48 g | 76.58 ab | 127.07 h | 826.07 bcd | 2893.13 fgh | 635.17 fg | |
±0.87 | ±0.81 | ±0.80 | ±4.39 | ±37.45 | ±4.72 | |||
8 | 105.48 f | 74.23 ab | 126.59 h | 821.58 abc | 2667.55 abcd | 554.44 bcd | ||
±1.29 | ±1.18 | ±0.50 | ±1.74 | ±32.67 | ±3.72 | |||
70 | 20 | 4 | 82.03 d | 74.40 ab | 126.39 h | 854.74 ghijk | 2996.55 hi | 666.53 ijk |
±0.79 | ±0.48 | ±1.88 | ±2.29 | ±34.50 | ±3.01 | |||
8 | 67.35 b | 73.35 a | 120.67 ef | 851.82 fghij | 2652.90 ab | 541.09 b | ||
±1.77 | ±0.84 | ±1.09 | ±4.06 | ±40.42 | ±4.96 | |||
8 | 4 | 71.65 c | 75.63 ab | 126.08 h | 842.15 efg | 2996.38 hi | 671.17 jk | |
±0.98 | ±0.22 | ±1.38 | ±4.22 | ±31.02 | ±4.07 | |||
8 | 57.47 a | 75.75 ab | 121.77 fg | 838.26 def | 2642.90 ab | 540.92 b | ||
±0.36 | ±0.77 | ±1.43 | ±1.95 | ±30.81 | ±3.82 | |||
0 | 4 | 88.69 e | 74.80 ab | 125.68 gh | 830.47 cde | 2966.11 h | 670.95 jk | |
±1.08 | ±0.84 | ±0.38 | ±3.99 | ±37.32 | ±4.15 | |||
8 | 61.10 a | 74.52 ab | 121.88 fg | 828.92 cde | 2660.12 abc | 541.67 bc | ||
±1.08 | ±0.85 | ±1.09 | ±2.57 | ±23.92 | ±4.88 | |||
−18 | 4 | 81.72 d | 74.51 ab | 126.43 h | 811.57 ab | 2896.95 fgh | 651.13 hi | |
±1.18 | ±0.92 | ±1.35 | ±3.58 | ±25.51 | ±5.50 | |||
8 | 65.91 b | 75.67 ab | 128.52 h | 807.03 a | 2560.56 a | 524.93 a | ||
±1.60 | ±0.69 | ±0.84 | ±1.36 | ±39.14 | ±3.63 |
ABV (% v/v) | Temp. (°C) | Time (Weeks) | Compound Concentration (mg/L Alcohol 100% v/v) | ||||||
---|---|---|---|---|---|---|---|---|---|
Acetaldehyde Diethyl Acetal | Ethyl Acetate | Isoamyl Acetate | Ethyl Hexanoate | Ethyl Octanoate | Ethyl Decanoate | Ethyl Tetradecanoate | |||
Control sample | 0.75 a | 62.12 a | 0.52 a | 0.17 a | 0.08 a | n.d. | n.d. | ||
±0.02 | ±0.78 | ±0.00 | ±0.00 | ±0.00 | |||||
40 | 20 | 4 | 1.09 bcd | 65.88 bc | 0.56 bc | 0.22 defghi | 0.10 a | n.d. | n.d. |
±0.02 | ±0.25 | ±0.00 | ±0.01 | ±0.00 | |||||
8 | 1.68 no | 66.32 bcd | 0.63 de | 0.22 cdefgh | 6.39 d | n.d. | n.d. | ||
±0.05 | ±0.50 | ±0.01 | ±0.02 | ±0.09 | |||||
8 | 4 | 1.08 bcd | 70.58 fgh | 0.57 bc | 0.19 abcd | 0.09 a | n.d. | n.d. | |
±0.03 | ±0.93 | ±0.01 | ±0.01 | ±0.00 | |||||
8 | 1.63 lmno | 74.06 i | 0.58 bc | 0.20 abcdefg | 6.37 d | n.d. | n.d. | ||
±0.05 | ±0.55 | ±0.00 | ±0.00 | ±0.07 | |||||
0 | 4 | 0.98 b | 67.32 cdef | 0.55 ab | 0.20 abcdef | 0.09 a | n.d. | n.d. | |
±0.05 | ±0.76 | ±0.02 | ±0.01 | ±0.00 | |||||
8 | 1.66 mno | 69.46 defg | 0.59 cd | 0.22 defghi | 6.36 d | n.d. | n.d. | ||
±0.05 | ±1.09 | ±0.02 | ±0.01 | ±0.05 | |||||
−18 | 4 | 0.99 bc | 67.22 cde | 0.58 bc | 0.18 abc | 0.10 a | n.d. | n.d. | |
±0.05 | ±0.52 | ±0.01 | ±0.00 | ±0.00 | |||||
8 | 1.47 ijkl | 73.52 hi | 0.59 cd | 0.22 bcdefgh | 6.36 d | n.d. | n.d. | ||
±0.05 | ±1.03 | ±0.01 | ±0.01 | ±0.04 | |||||
50 | 20 | 4 | 1.26 efgh | 72.46 ghi | 0.80 ij | 0.26 ij | 0.09 a | n.d. | n.d. |
±0.06 | ±0.35 | ±0.02 | ±0.01 | ±0.00 | |||||
8 | 1.78 o | 78.14 kl | 0.80 ij | 0.27 j | 5.11 c | n.d. | n.d. | ||
±0.07 | ±0.51 | ±0.00 | ±0.02 | ±0.09 | |||||
8 | 4 | 1.19 def | 70.11 efg | 0.73 g | 0.18 ab | 0.09 a | n.d. | n.d. | |
±0.05 | ±1.24 | ±0.02 | ±0.00 | ±0.00 | |||||
8 | 1.53 jklmn | 79.21 klm | 0.75 gh | 0.24 hij | 5.12 c | n.d. | n.d. | ||
±0.05 | ±0.92 | ±0.01 | ±0.01 | ±0.05 | |||||
0 | 4 | 1.13 bcde | 63.58 ab | 0.64 ef | 0.19 abcde | 0.09 a | n.d. | n.d. | |
±0.05 | ±1.52 | ±0.01 | ±0.00 | ±0.00 | |||||
8 | 1.57 klmn | 72.40 ghi | 0.65 ef | 0.22 bcdefgh | 5.11 c | n.d. | n.d. | ||
±0.04 | ±0.44 | ±0.01 | ±0.01 | ±0.05 | |||||
−18 | 4 | 1.16 cdef | 67.30 cdef | 0.66 ef | 0.18 abc | 0.10 a | n.d. | n.d. | |
±0.04 | ±1.12 | ±0.00 | ±0.00 | ±0.00 | |||||
8 | 1.43 hijk | 78.08 jk | 0.68 f | 0.24 ghij | 5.12 c | n.d. | n.d. | ||
±0.04 | ±0.79 | ±0.02 | ±0.02 | ±0.02 | |||||
70 | 20 | 4 | 2.64 p | 74.80 ij | 0.87 kl | 0.31 k | 0.09 a | n.d. | n.d. |
±0.08 | ±0.71 | ±0.00 | ±0.02 | ±0.00 | |||||
8 | 5.22 q | 81.67 m | 0.88 lm | 0.31 k | 3.71 b | n.d. | n.d. | ||
±0.04 | ±0.84 | ±0.01 | ±0.00 | ±0.05 | |||||
8 | 4 | 1.40 hijk | 72.11 ghi | 0.90 lm | 0.21 bcdefgh | 0.10 a | n.d. | n.d. | |
±0.05 | ±0.65 | ±0.01 | ±0.01 | ±0.00 | |||||
8 | 1.46 ijk | 81.37 klm | 0.91 m | 0.24 ghij | 3.66 b | n.d. | n.d. | ||
±0.06 | ±0.80 | ±0.01 | ±0.01 | ±0.06 | |||||
0 | 4 | 1.32 fghi | 68.67 cdef | 0.82 ij | 0.21 bcdefgh | 0.09 a | n.d. | n.d. | |
±0.04 | ±0.63 | ±0.00 | ±0.02 | ±0.00 | |||||
8 | 1.49 ijklm | 81.40 lm | 0.84 jk | 0.23 efghij | 3.69 b | n.d. | n.d. | ||
±0.06 | ±0.76 | ±0.02 | ±0.01 | ±0.06 | |||||
−18 | 4 | 1.21 defg | 67.23 cde | 0.79 hi | 0.20 abcdef | 0.09 a | n.d. | n.d. | |
±0.06 | ±1.23 | ±0.00 | ±0.00 | ±0.00 | |||||
8 | 1.37 ghij | 80.67 klm | 0.81 ij | 0.23 fghij | 3.68 b | n.d. | n.d. | ||
±0.04 | ±0.89 | ±0.01 | ±0.01 | ±0.05 |
ABV (% v/v) | Temp. (°C) | Time (Weeks) | Compound Concentration (mg/L Alcohol 100% v/v) | ||||||
---|---|---|---|---|---|---|---|---|---|
Acetaldehyde Diethyl Acetal | Ethyl Acetate | Isoamyl Acetate | Ethyl Hexanoate | Ethyl Octanoate | Ethyl Decanoate | Ethyl Tetradecanoate | |||
Control sample | 97.51 a | 189.10 a | 1.82 a | 0.66 a | 2.37 a | 7.09 a ± 0.02 | 0.06 a ± 0.00 | ||
±0.68 | ±0.97 | ±0.02 | ±0.00 | ±0.01 | |||||
40 | 20 | 4 | 102.88 ab | 196.26 ab | 1.88 a | 0.94 c | 3.75 e | 8.55 d ± 0.04 | 0.10 def ± 0.00 |
±1.08 | ±1.90 | ±0.02 | ±0.00 | ±0.02 | |||||
8 | 117.52 d | 198.67 ab | 2.29 b | 1.03 d | 9.78 rs | 9.33 f ± 0.03 | 0.14 i ± 0.00 | ||
±1.32 | ±1.18 | ±0.02 | ±0.01 | ±0.05 | |||||
8 | 4 | 105.42 b | 214.57 efgh | 1.86 a | 0.70 a | 3.26 c | 7.20 a ± 0.06 | 0.09 bcd ± 0.00 | |
±1.33 | ±3.64 | ±0.02 | ±0.00 | ±0.02 | |||||
8 | 110.95 c | 244.65 lmn | 2.29 b | 1.16 fg | 9.58 pq | 7.86 b ± 0.02 | 0.14 hi ± 0.01 | ||
±1.61 | ±3.70 | ±0.02 | ±0.01 | ±0.04 | |||||
0 | 4 | 103.85 b | 204.76 bcdef | 1.90 a | 0.88 b | 3.44 d | 8.17 c ± 0.06 | 0.08 ab ± 0.00 | |
±1.24 | ±2.60 | ±0.02 | ±0.00 | ±0.01 | |||||
8 | 104.90 b | 235.25 jkl | 2.44 cd | 1.14 f | 8.73 m | 8.77 e ± 0.06 | 0.12 gh ± 0.00 | ||
±1.40 | ±3.18 | ±0.02 | ±0.00 | ±0.03 | |||||
−18 | 4 | 101.50 ab | 205.57 bcdefg | 1.84 a | 0.68 a | 2.82 b | 8.05 bc ± 0.06 | 0.08 abc ± 0.00 | |
±1.02 | ±2.33 | ±0.00 | ±0.01 | ±0.01 | |||||
8 | 103.80 b | 211.64 efgh | 1.88 a | 0.69 a | 8.51 l | 8.10 c ± 0.02 | 0.12 fg ± 0.01 | ||
±0.90 | ±1.54 | ±0.01 | ±0.00 | ±0.06 | |||||
50 | 20 | 4 | 180.67 f | 216.57 hi | 2.50 d | 1.08 e | 4.85 h | 11.95 i ± 0.00 | 0.10 def ± 0.00 |
±2.31 | ±2.76 | ±0.04 | ±0.02 | ±0.04 | |||||
8 | 188.25 g | 226.58 ij | 2.62 e | 1.25 jk | 9.89 st | 14.00 k ± 0.13 | 0.20 kl ± 0.00 | ||
±1.53 | ±2.43 | ±0.03 | ±0.01 | ±0.09 | |||||
8 | 4 | 179.13 f | 214.30 efgh | 2.37 bc | 1.02 d | 4.80 h | 11.44 h ± 0.04 | 0.10 cde ± 0.00 | |
±1.57 | ±4.33 | ±0.01 | ±0.00 | ±0.04 | |||||
8 | 187.52 g | 246.64 mn | 2.93 g | 1.21 hi | 9.77 rs | 13.19 j ± 0.04 | 0.20 kl ± 0.01 | ||
±1.49 | ±5.17 | ±0.02 | ±0.01 | ±0.06 | |||||
0 | 4 | 175.29 f | 201.42 bcd | 2.38 bc | 1.23 ij | 4.61 g | 11.26 h ± 0.03 | 0.10 cde ± 0.00 | |
±1.91 | ±1.04 | ±0.03 | ±0.02 | ±0.03 | |||||
8 | 178.96 f | 210.93 defgh | 2.49 d | 1.40 m | 8.95 n | 11.36 h ± 0.05 | 0.19 jk ± 0.00 | ||
±1.13 | ±3.25 | ±0.00 | ±0.01 | ±0.06 | |||||
−18 | 4 | 169.40 e | 200.86 bc | 2.32 b | 0.91 bc | 4.07 f | 11.05 g ± 0.04 | 0.10 def ± 0.00 | |
±1.98 | ±3.06 | ±0.03 | ±0.00 | ±0.02 | |||||
8 | 178.07 f | 233.53 jk | 2.67 e | 1.18 gh | 9.18 o | 11.84 i ± 0.03 | 0.18 j ± 0.00 | ||
±1.98 | ±3.01 | ±0.03 | ±0.02 | ±0.03 | |||||
70 | 20 | 4 | 337.39 h | 204.59 bcde | 2.99 g | 1.37 lm | 6.56 k | 16.61 o ± 0.09 | 0.11 efg ± 0.00 |
±1.96 | ±2.92 | ±0.02 | ±0.00 | ±0.05 | |||||
8 | 342.21 hi | 214.67 fgh | 3.12 h | 1.46 n | 10.56 u | 22.25 s ± 0.08 | 0.23 m ± 0.01 | ||
±2.28 | ±2.19 | ±0.04 | ±0.02 | ±0.07 | |||||
8 | 4 | 363.20 k | 219.31 hi | 2.94 g | 1.34 l | 6.64 k | 16.35 n ± 0.01 | 0.11 defg ± 0.00 | |
±1.23 | ±1.08 | ±0.01 | ±0.00 | ±0.04 | |||||
8 | 376.92 l | 250.72 mn | 3.17 h | 1.79 q | 9.97 t | 20.59 r ± 0.07 | 0.21 l ± 0.00 | ||
±1.72 | ±4.82 | ±0.03 | ±0.01 | ±0.04 | |||||
0 | 4 | 360.16 k | 215.05 gh | 2.84 f | 1.28 k | 6.18 j | 15.74 m ± 0.05 | 0.11 efg ± 0.00 | |
±1.87 | ±1.97 | ±0.04 | ±0.01 | ±0.02 | |||||
8 | 377.47 l | 240.80 klm | 2.99 g | 1.50 o | 9.64 qr | 20.04 q ± 0.09 | 0.21 l ± 0.01 | ||
±1.88 | ±3.68 | ±0.00 | ±0.02 | ±0.05 | |||||
−18 | 4 | 345.84 i | 209.75 cdefgh | 2.83 f | 1.22 hij | 5.38 i | 15.21 l ± 0.02 | 0.12 fg ± 0.00 | |
±0.86 | ±2.94 | ±0.03 | ±0.00 | ±0.02 | |||||
8 | 351.96 j | 253.68 n | 3.36 i | 1.55 p | 9.44 p | 19.04 p ± 0.08 | 0.19 jkl ± 0.00 | ||
±1.47 | ±2.59 | ±0.03 | ±0.01 | ±0.06 |
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Różański, M.; Pielech-Przybylska, K.; Balcerek, M. Influence of Alcohol Content and Storage Conditions on the Physicochemical Stability of Spirit Drinks. Foods 2020, 9, 1264. https://doi.org/10.3390/foods9091264
Różański M, Pielech-Przybylska K, Balcerek M. Influence of Alcohol Content and Storage Conditions on the Physicochemical Stability of Spirit Drinks. Foods. 2020; 9(9):1264. https://doi.org/10.3390/foods9091264
Chicago/Turabian StyleRóżański, Mateusz, Katarzyna Pielech-Przybylska, and Maria Balcerek. 2020. "Influence of Alcohol Content and Storage Conditions on the Physicochemical Stability of Spirit Drinks" Foods 9, no. 9: 1264. https://doi.org/10.3390/foods9091264