Research on Microstructural Characterization and Mechanical Properties of Al-Zn-Mg-Cu Alloy Thick Plate During Rolling
Abstract
1. Introduction
2. Methods
3. Results
3.1. Microstructure
3.2. Texture Analysis
3.3. Precipitate Morphology
3.4. Tensile Properties
3.5. Anisotropy Analysis
4. Conclusions
Author Contributions
Funding
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
- Chao, L.; He, Y.; Heng, L.; Nian, S.; Jin, F.; Lihua, Z. Dependence of creep age formability on initial temper of an Al-Zn-Mg-Cu alloy. Chin. J. Aeronaut. 2016, 29, 1445–1454. [Google Scholar]
- Zheng, G.; Li, H.; Lei, C.; Fu, J.; Bian, T.; Yang, J. Natural aging behaviors and mechanisms of 7050 and 5A90 Al alloys: A comparative study. Mater. Sci. Eng. A 2018, 718, 157–164. [Google Scholar] [CrossRef]
- Dursun, T.; Soutis, C. Recent developments in advanced aircraft aluminium alloys. Mater. Des. (1980–2015) 2014, 56, 862–871. [Google Scholar] [CrossRef]
- Zwolak, M.; Śliwa, R. Analysis of the influence of dies geometry on the process extrusion force and properties of the extrudate obtained in the process of cold extrusion of 7075 aluminum alloy by the KOBO method. Mater. Sci.-Pol. 2024, 42, 92–106. [Google Scholar] [CrossRef]
- Li, H.; Bai, Q.; Li, Y.; Du, Q.; Katgerman, L.; Zhang, J.; Zhuang, L. Mechanical properties and cold cracking evaluations of four 7××× series aluminum alloys using a newly developed index. Mater. Sci. Eng. A 2017, 698, 230–237. [Google Scholar] [CrossRef]
- Kuo, C.-H.; Lin, Z.-Y. Optimizing the high-performance milling of thin aluminum alloy plates using the Taguchi method. Metals 2021, 11, 1526. [Google Scholar] [CrossRef]
- Yashin, V.V.; Beglov, E.D.; Aryshensky, E.V.; Latushkin, I.A. Large size metal-clad ingots rolling process analysis using finite elements method. J. Sib. Fed. Univ. Eng. Technol. 2018, 11, 419–426. [Google Scholar]
- Prabhu, T.R. An overview of high-performance aircraft structural Al alloy-AA7085. Acta Metall. Sin. (Engl. Lett.) 2015, 28, 909–921. [Google Scholar] [CrossRef]
- Zhang, X.; Chen, Y.; Hu, J. Recent advances in the development of aerospace materials. Prog. Aerosp. Sci. 2018, 97, 22–34. [Google Scholar] [CrossRef]
- Zare, M.A.; Taghiabadi, R.; Ghoncheh, M.H. Effect of cooling rate on microstructure and mechanical properties of AA5056 Al-Mg alloy. Int. J. Met. 2022, 16, 1533–1543. [Google Scholar] [CrossRef]
- Dai, Y.; Yan, L.; Hao, J. Review on micro-alloying and preparation method of 7xxx series aluminum alloys: Progresses and prospects. Materials 2022, 15, 1216. [Google Scholar] [CrossRef] [PubMed]
- Zhu, C.; Zhao, Z.; Zhu, Q.; Wang, G.; Zuo, Y.; Li, Q.; Qin, G. Hot-top direct chill casting assisted by a twin-cooling field: Improving the ingot quality of a large-size 2024 Al alloy. J. Mater. Sci. Technol. 2022, 112, 114–122. [Google Scholar] [CrossRef]
- Li, Z.; Li, Y.; Zhou, R.; Xie, L.; Wang, Q.; Zhang, L.; Ji, Q.; Xu, B. Microstructure and properties of semi-solid 7075 aluminum alloy processed with an enclosed cooling slope channel. Crystals 2023, 13, 1102. [Google Scholar] [CrossRef]
- Song, L.; Xie, Z.; Gao, H.; Kong, C.; Yu, H. Microstructure and mechanical properties of ARB-processed AA1050/AA5052 multilayer laminate sheets during cryorolling. Mater. Lett. 2022, 307, 130998. [Google Scholar] [CrossRef]
- Roth, C.C.; Fras, T.; Mohr, D. Dynamic perforation of lightweight armor: Temperature-dependent plasticity and fracture of aluminum 7020-T6. Mech. Mater. 2020, 149, 103537. [Google Scholar] [CrossRef]
- Chakraborty, P.; Singha, M.K.; Tiwari, V. Anisotropic mechanical response of AA7475-T7351 alloy at different loading rates and temperatures. Thin-Walled Struct. 2023, 188, 110842. [Google Scholar] [CrossRef]
- Wei, L.; Pan, Q.; Huang, H.; Feng, L.; Wang, Y. Influence of grain structure and crystallographic orientation on fatigue crack propagation behavior of 7050 alloy thick plate. Int. J. Fatigue 2014, 66, 55–64. [Google Scholar] [CrossRef]
- Yang, S.; Yang, Y.; Chen, Z. Effects of rolling method on the microstructure and anisotropy of mechanical properties of Cu–15Cr in-situ composites. Mater. Sci. Eng. A 2022, 856, 144000. [Google Scholar] [CrossRef]
- Shin, Y.-C.; Park, Y.-C.; Hong, J.-P.; Cheong, J.Y.; Kim, K.-Y.; Shin, B.; Jeong, D.-Y.; Lee, T.; Kwak, T.; Jung, T.-K.; et al. Cross-rolling induced texture randomization and structural evolution for improved plastic isotropy in Al-Mg alloys with high Mg content. J. Alloys Compd. 2024, 1008, 176530. [Google Scholar] [CrossRef]
- Pang, H.; Lu, L.; Yang, R.; Ma, M.; Wang, X.; Wu, Y.; Jing, L.; Dong, J.; Zhang, S. Investigation into Mg-4.5 Al-2.5 Zn Mg alloy applying cryogenic treatment and cross-rolling at diverse temperatures. J. Mater. Res. Technol. 2025, 37, 4064–4076. [Google Scholar] [CrossRef]
- Ma, Z.; Zhong, T.; Sun, D.; Qian, B.; Turakhodjaev, N.; Betsofen, S.; Wu, R. Microstructure and anisotropy of mechanical properties of Al-3Li-1Cu-0.4 Mg-0.1 Er-0.1 Zr alloys prepared by normal rolling and cross-rolling. Metals 2023, 13, 1564. [Google Scholar] [CrossRef]
- Kazemi-Navaee, A.; Jamaati, R.; Aval, H.J. Effect of single roll drive cross rolling on the microstructure, crystallographic texture, and mechanical behavior of Al-Zn-Mg-Cu alloy. Arch. Civ. Mech. Eng. 2022, 22, 41. [Google Scholar] [CrossRef]
- Mondal, C.; Singh, A.K.; Mukhopadhyay, A.K.; Chattopadhyay, K. Effects of different modes of hot cross-rolling in 7010 aluminum alloy: Part I. Evolution of microstructure and texture. Metall. Mater. Trans. A 2013, 44, 2746–2763. [Google Scholar] [CrossRef]
- Chen, Z.; Yan, K.; Ren, C.; Naseem, S. Precipitation sequence and hardening effect in 7A85 aluminum alloy. J. Alloys Compd. 2021, 875, 159950. [Google Scholar] [CrossRef]
- Zhao, Y.; Liu, J.; Topping, T.D.; Lavernia, E.J. Precipitation and aging phenomena in an ultrafine grained Al-Zn alloy by severe plastic deformation. J. Alloys Compd. 2021, 851, 156931. [Google Scholar] [CrossRef]
- Altuntaş, G.; Özdemir, A.T.; Bostan, B. Investigation of the impacts of artificial ageing, re-ageing and cryogenic cycles on multiplex second phase precipitation and life-time prediction in 7075 alloy. Mater. Today Commun. 2024, 40, 109602. [Google Scholar] [CrossRef]
- Liu, E.; Pan, Q.; Liu, B.; Ye, J.; Wang, W. Microstructure Evolution of the Near-Surface Deformed Layer and Corrosion Behavior of Hot Rolled AA7050 Aluminum Alloy. Materials 2023, 16, 4632. [Google Scholar] [CrossRef] [PubMed]
- Li, J.; Jiang, F.; Li, Y.; Zhang, M.; Chen, C.; Yang, Z.; Zhang, F. Effect of warm-rolling on the strength and ductility of multilayered composite steel. Mater. Sci. Eng. A 2022, 841, 143043. [Google Scholar] [CrossRef]
- Kumar, D.S.; Chakradhar, I.; Rao, S.; Puri, R.; Manjini, S. Analysis of Chip Generation During Bar Rolling. J. Fail. Anal. Prev. 2018, 18, 635–639. [Google Scholar] [CrossRef]
- Li, C.-M.; Cheng, N.-P.; Chen, Z.-Q.; Li, X.; Xie, Z.-J.; He, H. Electric field-induced aging phase transformation in Al-Zn-Mg-Cu alloys: A first-principles study. In Proceedings of the 2016 3rd International Conference on Mechatronics and Information Technology, Shenzhen, China, 9–10 April 2016; Atlantis Press: Dordrecht, The Netherlands, 2016; pp. 511–518. [Google Scholar]
- Balaško, T.; Nagode, A.; Li, J.; Medved, J. Microstructure evolution during solution annealing of an Al–Zn–Mg–Cu alloy with La additions. Sci. Rep. 2025, 15, 3845. [Google Scholar] [CrossRef]
- Wang, Z.; Huang, S.; Zhang, W.; Li, S.; Liu, J. Precipitation Thermodynamics in an Al–Zn–Mg Alloy with Different Grain Sizes. Metals 2024, 14, 625. [Google Scholar] [CrossRef]
- Sun, J.-R.; Dong, B.-X.; Yang, H.-Y.; Shu, S.-L.; Qiu, F.; Jiang, Q.-C.; Zhang, L.-C. The Role of Lithium in the Aging Precipitation Process of Al-Zn-Mg-Cu Alloys and Its Effect on the Properties. Materials 2023, 16, 4750. [Google Scholar] [CrossRef] [PubMed]
- Yan, X.; Yang, Y.; Hamada, H. Tensile properties of glass fiber reinforced polypropylene composite and its carbon fiber hybrid composite fabricated by direct fiber feeding injection molding process. Polym. Compos. 2017, 39, 3564–3574. [Google Scholar] [CrossRef]
- Duan, X.; Jiang, H.; Mi, Z.; Cheng, L.; Wang, J. Reduce the Planar Anisotropy of AA6016 Aluminum Sheets by Texture and Microstructure Control. Crystals 2020, 10, 1027. [Google Scholar] [CrossRef]
- Lee, D.N.; Han, H.N. Recrystallization textures of metals and alloys. In Recent Developments in the Study of Recrystallization; InTechOpen: London, UK, 2013; pp. 3–59. [Google Scholar]
- Ryu, J.H.; Lee, D.N. The effect of precipitation on the evolution of recrystallization texture in AA8011 aluminum alloy sheet. Mater. Sci. Eng. A 2002, 336, 225–232. [Google Scholar] [CrossRef]
- Inoue, H.; Takasugi, T. Texture control for improving deep drawability in rolled and annealed aluminum alloy sheets. Mater. Trans. 2007, 48, 2014–2022. [Google Scholar] [CrossRef]











| Si | Fe | Cu | Mg | Zn | Ti | Zr | Al |
|---|---|---|---|---|---|---|---|
| 0.03 | 0.04 | 2.18 | 1.68 | 8.20 | 0.025 | 0.10 | Bal. |
| Texture | Habit Plane | Loading–Habit Plane Angle | ||
|---|---|---|---|---|
| L | LT | ST | ||
| Brass | {111} {11} {1} {} | 70.53° 0° 28.12° 28.12° | 19.47° 90° 19.47° 19.47° | 0° 0° 54.74° 54.74° |
| S | {111} {11} {1} {} | 31.17° 21.69° 73.94° 4.24° | 36.35° 4.53° 16.06° 71.50° | 38.11° 67.79° 0° 17.97° |
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Deng, G.; Wang, Y.; Zheng, X.; Zhang, X.; Ma, K.; Xiao, B.; Ma, Z. Research on Microstructural Characterization and Mechanical Properties of Al-Zn-Mg-Cu Alloy Thick Plate During Rolling. Metals 2026, 16, 535. https://doi.org/10.3390/met16050535
Deng G, Wang Y, Zheng X, Zhang X, Ma K, Xiao B, Ma Z. Research on Microstructural Characterization and Mechanical Properties of Al-Zn-Mg-Cu Alloy Thick Plate During Rolling. Metals. 2026; 16(5):535. https://doi.org/10.3390/met16050535
Chicago/Turabian StyleDeng, Guiying, Yaohui Wang, Xu Zheng, Xinkui Zhang, Kai Ma, Bolu Xiao, and Zongyi Ma. 2026. "Research on Microstructural Characterization and Mechanical Properties of Al-Zn-Mg-Cu Alloy Thick Plate During Rolling" Metals 16, no. 5: 535. https://doi.org/10.3390/met16050535
APA StyleDeng, G., Wang, Y., Zheng, X., Zhang, X., Ma, K., Xiao, B., & Ma, Z. (2026). Research on Microstructural Characterization and Mechanical Properties of Al-Zn-Mg-Cu Alloy Thick Plate During Rolling. Metals, 16(5), 535. https://doi.org/10.3390/met16050535
