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Article

Fiber Orientation Estimation from X-ray Dark Field Images of Fiber Reinforced Polymers Using Constrained Spherical Deconvolution

1
imec—Vision Lab, Department of Physics, University of Antwerp, 2000 Antwerp, Belgium
2
DynXlab: Center for 4D Quantitative X-ray Imaging and Analysis, Department of Physics, University of Antwerp, 2000 Antwerp, Belgium
3
Lab for Equilibrium Investigations and Aerospace, Department of Physics, University of Antwerp, 2000 Antwerp, Belgium
*
Author to whom correspondence should be addressed.
Polymers 2023, 15(13), 2887; https://doi.org/10.3390/polym15132887
Submission received: 1 June 2023 / Revised: 23 June 2023 / Accepted: 28 June 2023 / Published: 29 June 2023

Abstract

The properties of fiber reinforced polymers are strongly related to the length and orientation of the fibers within the polymer matrix, the latter of which can be studied using X-ray computed tomography (XCT). Unfortunately, resolving individual fibers is challenging because they are small compared to the XCT voxel resolution and because of the low attenuation contrast between the fibers and the surrounding resin. To alleviate both problems, anisotropic dark field tomography via grating based interferometry (GBI) has been proposed. Here, the fiber orientations are extracted by applying a Funk-Radon transform (FRT) to the local scatter function. However, the FRT suffers from a low angular resolution, which complicates estimating fiber orientations for small fiber crossing angles. We propose constrained spherical deconvolution (CSD) as an alternative to the FRT to resolve fiber orientations. Instead of GBI, edge illumination phase contrast imaging is used because estimating fiber orientations with this technique has not yet been explored. Dark field images are generated by a Monte Carlo simulation framework. It is shown that the FRT cannot estimate the fiber orientation accurately for crossing angles smaller than 70, while CSD performs well down to a crossing angle of 50. In general, CSD outperforms the FRT in estimating fiber orientations.
Keywords: FRP; dark field; edge illumination; phase contrast imaging; constrained spherical deconvolution FRP; dark field; edge illumination; phase contrast imaging; constrained spherical deconvolution
Graphical Abstract

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MDPI and ACS Style

Huyge, B.; Sanctorum, J.; Jeurissen, B.; De Beenhouwer, J.; Sijbers, J. Fiber Orientation Estimation from X-ray Dark Field Images of Fiber Reinforced Polymers Using Constrained Spherical Deconvolution. Polymers 2023, 15, 2887. https://doi.org/10.3390/polym15132887

AMA Style

Huyge B, Sanctorum J, Jeurissen B, De Beenhouwer J, Sijbers J. Fiber Orientation Estimation from X-ray Dark Field Images of Fiber Reinforced Polymers Using Constrained Spherical Deconvolution. Polymers. 2023; 15(13):2887. https://doi.org/10.3390/polym15132887

Chicago/Turabian Style

Huyge, Ben, Jonathan Sanctorum, Ben Jeurissen, Jan De Beenhouwer, and Jan Sijbers. 2023. "Fiber Orientation Estimation from X-ray Dark Field Images of Fiber Reinforced Polymers Using Constrained Spherical Deconvolution" Polymers 15, no. 13: 2887. https://doi.org/10.3390/polym15132887

APA Style

Huyge, B., Sanctorum, J., Jeurissen, B., De Beenhouwer, J., & Sijbers, J. (2023). Fiber Orientation Estimation from X-ray Dark Field Images of Fiber Reinforced Polymers Using Constrained Spherical Deconvolution. Polymers, 15(13), 2887. https://doi.org/10.3390/polym15132887

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