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Crystals 2015, 5(1), 9-13;

Synthesis and Molecular Structure of 2-(Diphenylphosphano)phenyl Benzoate Borane Adduct

Institut für Radiopharmazie, Helmholtz-Zentrum Dresden-Rossendorf, Bautzner Landstraße 400, D-01328 Dresden, Germany
Institut für Chemie, Universität Rostock, Anorganische Festkörperchemie, Albert-Einstein-Straße 3a, D-18059 Rostock, Germany
Author to whom correspondence should be addressed.
Academic Editor: Nikolaus Korber
Received: 5 November 2014 / Accepted: 12 December 2014 / Published: 29 December 2014
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The crystal and molecular structure of 2-(diphenylphosphano)phenyl benzoate borane adduct are reported. The title compound crystallizes from a petroleum ether/ethyl acetate mixture in the triclinic space group P with two molecules in the unit cell. The unit cell parameters are: a = 8.67(1) Å, b = 9.202(1) Å, c = 14.224(2) Å; α = 72.600(7)°, β = 73.577(7)°, γ = 84.349(7)° and V = 1039.5(2) Å3. Bond lengths and angles are typical for this phosphane borane adduct. View Full-Text
Keywords: building block; Lewis acid-base; Staudinger Ligation building block; Lewis acid-base; Staudinger Ligation

Figure 1

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Mamat, C.; Köckerling, M. Synthesis and Molecular Structure of 2-(Diphenylphosphano)phenyl Benzoate Borane Adduct. Crystals 2015, 5, 9-13.

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