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Article
Peer-Review Record

Study on the Influence of Saturation on Freeze–Thaw Damage Characteristics of Sandstone

Materials 2023, 16(6), 2309; https://doi.org/10.3390/ma16062309
by Xinlei Zhang 1, Jiaxu Jin 1,2,*, Xiaoli Liu 3,*, Yukai Wang 3 and Yahao Li 1
Reviewer 1: Anonymous
Reviewer 2:
Reviewer 3: Anonymous
Materials 2023, 16(6), 2309; https://doi.org/10.3390/ma16062309
Submission received: 12 February 2023 / Revised: 8 March 2023 / Accepted: 8 March 2023 / Published: 13 March 2023

Round 1

Reviewer 1 Report

In this paper, the authors performed mechanical tests citing uniaxial compression test, electron microscopic scanning and nuclear magnetic resonance to analyze the mechanism of freeze-thaw disaster evolution and the role of water in rock freeze-thaw cycles. The authors actually investigated the law of water migration in the rock, the law of crack growth and the mechanism of damage during freeze-thaw cycles.

In the reviewer opinion, the paper can be recommended for publication in materials journal after addressing the following comments:

- Abstract. Please check the font of the text of line 15

- Authors should highlight the novelty of their manuscript in the abstract

- In the introductory section, the latest publications 2021-2022 should be analyzed more than the oldest references in order to see if the subject remains new or not.

- Line 103-104 the standard reference should be specified

- Lines 114-117 the temperature and drying time of the specimens as well as the saturation pressure and period: are these parameters standardized or arbitrarily chosen? An explanation should be added to the text.

- The authors sometimes use Fig sometimes Figure. The citation of figures should be the same in the whole manuscript.

- Table 1. How is the damage variable noted in the last column calculated?

- Figure 4. The figure legend is unclear; it is difficult to differentiate the curves drawn in this figure.

- The text in Figure 6 is not clear and another color and character should be used.

- Analyzing the same figure 6 what is the better choice or the better saturation condition?

Author Response

Please see the attachment.

Author Response File: Author Response.pdf

Reviewer 2 Report

The article corresponds to the subject of the journal

The article is written in easy language. Well structured. Written clearly and understandably.

Keywords and abstract are consistent with the conclusions

All references are available

Asa result   ­ ­­­ ­­­­ of the ministry of foreign affairs­­­, it­­­­­was established in 1893­­ in the mountains­­, when it was carried out in 1893, when it ­was carried out in 1893. ­ ­For the purpose of­catching mines, as­­­­ well as for the use ­­­­­­­­­­­of­ mines, as well as­for­­the­construction­of supports and pipes on­the construction ­of the Amur River­. ­The first experiment in ­the­artof soil freezing in the­course of ­­fishing for mines was carried out­­­­in 1883 (the ore­nik "Ar­chi­bald" in Ma­where­the burg­ok­ru­ge, Ger­ma­nia). In the USSR there is a study­of the artsof the land.  Freezing of the soil was first­in­the case of me­nyon in 1928–1929 with the­prokhod­ke ka­ka­liy shah you­in the city of Soli­­Kamsk, and­then in 1933 – on the construction­of­the Mosk met­ro­on­the basisof ­­these­me. ­that­house proy­de­ny all na­clone­shah­ty for es­ka­la­to­rov Moskovskogo­ metro­ po ­li­te­na, many iz ­ko­toryh dos­ti­ga­yut glu­bi­­ny 40-70 m.

Freezing of the  ­­­­­­­ soil ­­­­ can­be­­carried out both in the middle­and in the crepe­­­­­ of ­­­­ the ­nos­.­ Guides­to the ­geo­lo­ ­gich usli ­lo­vi yah.  It­­­­is also necessary to build­­­mines, ton­ne­leu, plo­tin, do­kov, fun­da­men­tov zda­nii and so­­­on.

The cost ­­­­­­­­­­of­ freezing the soil is­­­10–30%­ of the cost ­­­of ­the ground from the ­same­level­, with a ­­value­­of 40 or more than 40. up to 60% of ­the­­­­­total cost­per year­.

Freezing of soils, artificial cooling of soils in conditions of natural occurrence to negative temperatures in order to strengthen them and achieve the necessary degree of waterproofness.   Therefore, the topic of the authors' research is relevant.

The article contains a detailed literary analysis.

Full-scale experiments, testing were carried out, the physical and mechanical properties of sandstone were determined. Mesostructural characteristics of sandstone of different saturation during freezing-thawing with different cycles are obtained.

 Исследования подтверждены electron microscope scanning, nuclear magnetic resonance and uniaxial compression tests 

The results are applicable in practice.

 Notes: all transcripts or abbreviations should be taken out separately, and removed or deciphered in keywords

 

Author Response

Please see the attachment

Author Response File: Author Response.pdf

Reviewer 3 Report

Review report for the manuscript entitled

“Study on the Influence of Saturation on Freeze Thaw Damage Characteristics of Sandstone”

 

In this study, the macro mechanical indexes and micro structural characteristics of sandstones with different saturation levels after certain freeze-thaw cycles were analysed using electron microscope scanning, nuclear magnetic resonance, and uniaxial compression tests. The paper is interesting and well-written. However, the authors are required to address the following issues before the manuscript can be accepted for publication:

 

1) There are some editorial and grammatical mistakes throughout the text. I highly recommend the authors to carefully go through the manuscript and correct these mistakes accordingly. (e.g., “ as the increase of saturation” in the abstract, …)

 

2) Are the results presented in this study on the macro-meso freeze-thaw damage consistent with the previous studies which have mostly been carried out based on macro-scale properties? The authors are better present a comparison in this regard between their results and those in the previous studies.

 

3) The literature review is weak. There are a great number of studies on the effect of freeze-thaw cycles on the mechanical properties of soil and rock. I highly suggest the authors to add these studies to the manuscript.

 

Shirmohammadi, S., Ghaffarpour Jahromi, S., Payan, M., & Senetakis, K. (2021). Effect of lime stabilization and partial clinoptilolite zeolite replacement on the behavior of a silt-sized low-plasticity soil subjected to freezing–thawing cycles. Coatings11(8), 994.

 

Ahmadi, S., Ghasemzadeh, H., & Changizi, F. Effects of A Low-Carbon Emission Additive on Mechanical Properties of Fine-grained Soil under Freeze-Thaw Cycles. Journal of Cleaner Production, 2021, 127157.

 

Güllü, H., & Khudir, A. Effect of freeze–thaw cycles on unconfined compressive strength of fine-grained soil treated with jute fiber, steel fiber and lime. Cold Regions Science and Technology, 2014, 106, 55-65.

 

4) Section 2.1: Please summarize the properties of the tested rock in a table.

 

5) Do the authors have the information of the site where the samples have been taken? Any info on the engineering properties? Rock Classification (RMR & Q)?

 

6) “, and the porosity was 9.32%.” What is the definition of porosity here? This should be presented.

 

7) Have the authors followed any standard in applying freeze-thaw cycles (level, temperature, duration, etc.). If so, it should be mentioned.

 

8) Fig. 4: The legends should be modified. (Sr=…)

 

9) Fig. 5: Have the saturation threshold corresponding to the minimum degree of saturation been reported in the previous studies? How about the effect of freeze-thaw cycles on the value?

 

10) Fig. 6: The SEM images should be presented more clearly! The texts are not legible!

 

11) How can the rock discontinuity orientation affect the results obtained in this study?  

 

12) Table 3: Why do the porosity and permeability experience a peak value at the saturation level of 85%.

Comments for author File: Comments.pdf

Author Response

Please see the attachment.

Author Response File: Author Response.pdf

Round 2

Reviewer 3 Report

The authors have properly addressed all the raised issues and the manuscript can now be accepted for publication.

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