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Synthesis of New bis-Bidentate Nitrogen Ligand: 1,4-bis[(3,5-dimethyl-1H-pyrazol-1-yl)methyl]piperazine
Open AccessShort Note

Synthesis of 4-(4-(dimethylamino)phenyl)-5-acetyl-6-phenyl-3,4-dihydropyrimidin-2(1H)-thione

Canakkale Onsekiz Mart University, Department of Chemistry, 17020, Canakkale-Turkey
Molbank 2006, 2006(2), M468;
Received: 1 September 2005 / Accepted: 13 October 2005 / Published: 28 February 2006
Note: In lieu of an abstract, this is an excerpt from the first page.

4-(4-(dimethylamino)phenyl)-5-acetyl-6-phenyl-3,4-dihydropyrimidin-2(1H)-thione was prepared from benzoxyacetone (1) (1.62 g, 10 mmol), N,N-dimethylaniline (2) (1.21 g, 10 mmol) and thiourea (3) (1.140 g, 15 mmol) in dichloromethane (15 mL) as solvent using KF/Al2O3 (5 g) as a catalysis.[...] View Full-Text
Keywords: Biginelli reaction; KF/Al2O3; Benzoxyacetone; thiourea Biginelli reaction; KF/Al2O3; Benzoxyacetone; thiourea
MDPI and ACS Style

Aydin, F. Synthesis of 4-(4-(dimethylamino)phenyl)-5-acetyl-6-phenyl-3,4-dihydropyrimidin-2(1H)-thione. Molbank 2006, 2006, M468.

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