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Keywords = z-pin reinforcement

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14 pages, 6424 KiB  
Article
Effect of Selective Z-Pinning on the Static and Fatigue Strength of Step Joints between Composite Adherends
by Gabriela Loi, Pasquale Buonadonna, Rayane El Mohtadi, Mauro Carta, Daniele Lai, Mohamad El Mehtedi and Francesco Aymerich
J. Compos. Sci. 2024, 8(3), 84; https://doi.org/10.3390/jcs8030084 - 24 Feb 2024
Cited by 3 | Viewed by 2100
Abstract
The z-pinning reinforcement technique, which involves inserting thin pins through the body of a laminate, has proven highly effective in enhancing the strength of various composite joint configurations. This investigation aims to explore the enhancements achievable through selective z-pinning at very low pin [...] Read more.
The z-pinning reinforcement technique, which involves inserting thin pins through the body of a laminate, has proven highly effective in enhancing the strength of various composite joint configurations. This investigation aims to explore the enhancements achievable through selective z-pinning at very low pin contents on both the static and fatigue performance of composite joints. Single-step joints between carbon/epoxy adherends were reinforced using steel pins arranged in two, three, or four rows of pins parallel to the edges of the overlap, resulting in pin contents ranging from 0.2% to 0.4%. Joint panels were manufactured through co-curing, and coupons were extracted from the panels for static and fatigue tensile testing. The experimental tests show that z-pinning improves the static strength (by about 15%) and extends the fatigue lives of the joints. The ultimate failure of both unpinned and pinned joints is due to the unstable propagation of a crack at the bond line. The superior performances of pinned joints are mainly due to the bridging tractions imposed between the crack faces by z-pins, which delay the growth of the debonding crack. The enhancements in static and fatigue strength achieved by z-pinning were essentially independent of the number of pin rows, and the pins positioned near the joint edges were found to play a dominant role in controlling the structural performance of pinned joints. Full article
(This article belongs to the Special Issue Feature Papers in Journal of Composites Science in 2024)
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16 pages, 7894 KiB  
Article
Dry Friction and Wear Behavior of Laser-Sintered Graphite/Carbon Fiber/Polyamide 12 Composite
by Abdelrasoul Gadelmoula and Saleh Ahmed Aldahash
Polymers 2023, 15(19), 3916; https://doi.org/10.3390/polym15193916 - 28 Sep 2023
Cited by 10 | Viewed by 1916
Abstract
Carbon fiber-reinforced polymers (CFRPs) are being used extensively in modern industries that require a high strength-to-weight ratio, such as aerospace, automotive, motorsport, and sports equipment. However, although reinforcement with carbon fibers improves the mechanical properties of polymers, this comes at the expense of [...] Read more.
Carbon fiber-reinforced polymers (CFRPs) are being used extensively in modern industries that require a high strength-to-weight ratio, such as aerospace, automotive, motorsport, and sports equipment. However, although reinforcement with carbon fibers improves the mechanical properties of polymers, this comes at the expense of abrasive wear resistance. Therefore, to efficiently utilize CFRPs in dry sliding contacts, solid lubricant is used as a filler. Further, to facilitate the fabrication of objects with complex geometries, selective laser sintering (SLS) can be employed. Accordingly, in the present work, graphite-filled carbon fiber-reinforced polyamide 12 (CFR-PA12) specimens were prepared using the SLS process to explore the dry sliding friction and wear characteristics of the composite. The test specimens were aligned along four different orientations in the build chamber of the SLS machine to determine the orientation-dependent tribological properties. The experiments were conducted using a pin-on-disc tribometer to measure the coefficient of friction (COF), interface temperature, friction-induced noise, and specific wear rate. In addition, scanning electron microscopy (SEM) of tribo-surfaces was conducted to specify the dominant wear pattern. The results indicated that the steady-state COF, contact temperature, and wear pattern of graphite-filled CFR-PA12 are orientation-independent and that the contact temperature is likely to approach an asymptote far below the glass transition temperature of amorphous PA12 zones, thus eliminating the possibility of matrix softening. Additionally, the results showed that the Z-oriented specimen exhibits the lowest level of friction-induced noise along with the highest wear resistance. Moreover, SEM of tribo-surfaces determined that abrasive wear is the dominant wear pattern. Full article
(This article belongs to the Special Issue Organic-Inorganic Hybrid Materials III)
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15 pages, 2431 KiB  
Article
Engineered Interleaved Random Glass Fiber Composites Using Additive Manufacturing: Effect of Mat Properties, Resin Chemistry, and Resin-Rich Layer Thickness
by Ahmed M. H. Ibrahim, Mohanad Idrees, Emine Tekerek, Antonios Kontsos, Giuseppe R. Palmese and Nicolas J. Alvarez
Polymers 2023, 15(15), 3189; https://doi.org/10.3390/polym15153189 - 27 Jul 2023
Cited by 3 | Viewed by 2009
Abstract
Standard lay-up fabrication of fiber-reinforced composites (FRCs) suffer from poor out-of-plane properties and delamination resistance. While advanced manufacturing techniques (e.g., interleaving, braiding, and z-pinning) increase delamination resistance in FRCs, they typically result in significant fabrication complexity and limitations, increased manufacturing costs, and/or overall [...] Read more.
Standard lay-up fabrication of fiber-reinforced composites (FRCs) suffer from poor out-of-plane properties and delamination resistance. While advanced manufacturing techniques (e.g., interleaving, braiding, and z-pinning) increase delamination resistance in FRCs, they typically result in significant fabrication complexity and limitations, increased manufacturing costs, and/or overall stiffness reduction. In this work, we demonstrate the use of facile digital light processing (DLP) technique to additively manufacture (AM) random glass FRCs with engineered interleaves. This work demonstrates how vat photo-polymerization techniques can be used to build composites layer-by-layer with controlled interleaf material, thickness, and placement. Note that this engineering control is almost impossible to achieve with traditional manufacturing techniques. A range of specimens were printed to measure the effect of interleaf thickness and material on tensile/flexural properties as well as fracture toughness. One important observation was the ≈60% increase in interlaminar fracture toughness achieved by using a tough resin material in the interleaf. The comparison between AM and traditionally manufactured specimens via vacuum-assisted resin transfer molding (VARTM) highlighted the limitation of AM techniques in achieving high mat consolidation. In other words, the volume fraction of AM parts is limited by the wet fiber mat process, and engineering solutions are discussed. Overall, this technique offers engineering control of FRC design and fabrication that is not available with traditional methods. Full article
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14 pages, 4597 KiB  
Article
Optimization of Pin Position and Angle for Z-Pin-Reinforced Foam Core Sandwich Structures
by Eduardo Fischer Kerche, Agnė Kairytė, Sylwia Członka, Amanda Albertin Xavier da Silva, Maikson Luiz Passaia Tonatto, Francisco Luiz Bresolin, Rafael de Avila Delucis and Sandro Campos Amico
Materials 2023, 16(1), 352; https://doi.org/10.3390/ma16010352 - 30 Dec 2022
Cited by 6 | Viewed by 2393
Abstract
Sandwich panels (SP) are very promising components for structures as they ally high levels of specific stiffness and strength. Civil, marine and automotive industries are some examples of the sectors that use SPs frequently. This work demonstrates the potential of manufacturing Z-pin-reinforced foam [...] Read more.
Sandwich panels (SP) are very promising components for structures as they ally high levels of specific stiffness and strength. Civil, marine and automotive industries are some examples of the sectors that use SPs frequently. This work demonstrates the potential of manufacturing Z-pin-reinforced foam core SPs, using a design strategy that indicated optimal values for both pin position and angle, keeping the same pin diameter as determined in a previous study. A simple search algorithm was applied to optimize each design, ensuring maximum flexural stiffness. Designs using optimal pin position, optimal pin angle and optimal values for both parameters are herein investigated using numerical and experimental approaches. The optimal pin position yielded an increase in flexural stiffness of around 8.0% when compared to the non-optimized design. In this same comparison, the optimal pin angle by itself increased the flexural stiffness by about 63.0%. Besides, the highest increase in the maximum load was found for those composites, molded with optimized levels of pin position and pin angle, which synergistically contributed to this result. All results were demonstrated with numerical and experimental results and there was a good agreement between them. Full article
(This article belongs to the Special Issue Lightweight and High-Strength Sandwich Panel)
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19 pages, 76358 KiB  
Article
Powder Epoxy for One-Shot Cure, Out-of-Autoclave Applications: Lap Shear Strength and Z-Pinning Study
by Thomas Noble, James R. Davidson, Christophe Floreani, Ankur Bajpai, William Moses, Thomas Dooher, Alistair McIlhagger, Edward Archer, Conchúr M. Ó Brádaigh and Colin Robert
J. Compos. Sci. 2021, 5(9), 225; https://doi.org/10.3390/jcs5090225 - 24 Aug 2021
Cited by 8 | Viewed by 4021
Abstract
Large composite structures manufactured out-of-autoclave require the assembly and bonding of multiple parts. A one-shot cure manufacturing method is demonstrated using powder epoxy. Lap shear plates were manufactured from powder epoxy and glass fiber-reinforced plastic with four different bonding cases were assessed: secondary [...] Read more.
Large composite structures manufactured out-of-autoclave require the assembly and bonding of multiple parts. A one-shot cure manufacturing method is demonstrated using powder epoxy. Lap shear plates were manufactured from powder epoxy and glass fiber-reinforced plastic with four different bonding cases were assessed: secondary bonding using standard adhesive film, secondary bonding using powder epoxy, co-curing, and co-curing plus a novel Z-pinning method. This work investigates the lap shear strength of the four cases in accordance with ISO 4587:2003. Damage mechanisms and fracture behavior were explored using digital image correlation (DIC) and scanning electron microscopy (SEM), respectively. VTFA400 adhesive had a load at break 24.8% lower than secondary bonding using powder epoxy. Co-curing increased the load at break by 7.8% compared to powder epoxy secondary bonding, with the co-cured and pinned joint resulting in a 45.4% increase. In the co-cured and co-cured plus pinned cases, DIC indicated premature failure due to resin spew. SEM indicated shear failure of resin areas and a large amount of fiber pullout in both these cases, with pinning delaying fracture phenomena resulting in increased lap joint strength. This highlights the potential of powder epoxy for the co-curing of large composite structures out-of-autoclave. Full article
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15 pages, 3440 KiB  
Article
Tensile Properties of Z-Pin Reinforced Laminates with Circumferentially Notched Z-Pins
by André Knopp and Gerhard Scharr
J. Compos. Sci. 2020, 4(2), 78; https://doi.org/10.3390/jcs4020078 - 23 Jun 2020
Cited by 17 | Viewed by 3370
Abstract
This paper describes experimental investigations on the in-plane tensile properties of unidirectional carbon-fibre/epoxy laminates reinforced with circumferentially notched z-pins with different notch designs. From the results it can be concluded that the application of circumferential notches at the z-pin surface with constant notch [...] Read more.
This paper describes experimental investigations on the in-plane tensile properties of unidirectional carbon-fibre/epoxy laminates reinforced with circumferentially notched z-pins with different notch designs. From the results it can be concluded that the application of circumferential notches at the z-pin surface with constant notch depth of 20 μm and distance of 100 μm has no significant effect on the in-plane tensile strength values, regardless of the notch designs investigated. For circular and rectangular notch designs, no dependence of the tensile strength from the notch depth could be observed. Only changing the notch distances at a constant notch depth and width leads to small increases in the tensile strength values with increasing notch distance. The determined tensile modulus values indicate that there are no substantial deviations between laminates reinforced with unnotched and circumferentially notched z-pins, no matter which notch design is considered. It can be observed that there are no dependencies of the tensile modulus from notch depth and distance. Therefore, it can be assumed that the microstructural changes influencing the in-plane tensile properties will not be changed, or only to a very small extent, by the presence of notches on the pin surface. Full article
(This article belongs to the Special Issue Advanced Fiber Reinforced Polymer Composites)
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15 pages, 2794 KiB  
Article
Experimental Investigations on the Influence of Different Notch Designs on the Pullout Performance of Circumferentially Notched Z-pins
by André Knopp and Gerhard Scharr
J. Compos. Sci. 2020, 4(2), 67; https://doi.org/10.3390/jcs4020067 - 5 Jun 2020
Cited by 4 | Viewed by 2569
Abstract
The results of experimental research on the pullout properties of circumferentially notched z-pins with various notch designs are presented in this paper. Investigations on notched z-pins with four different notch designs—rectangular, circular, triangular, and sinusoidal—inserted into unidirectional (UD) and quasi-isotropic (QI) laminates were [...] Read more.
The results of experimental research on the pullout properties of circumferentially notched z-pins with various notch designs are presented in this paper. Investigations on notched z-pins with four different notch designs—rectangular, circular, triangular, and sinusoidal—inserted into unidirectional (UD) and quasi-isotropic (QI) laminates were carried out in order to assess the influence of notch design and laminate structure on the resulting z-pin pullout properties. It can be shown that the application of circumferential notches at the z-pin surface causes significant increases in pullout forces and consequently, on the resulting pullout energies, regardless of which notch design is considered. The effect of notched z-pins is higher in a quasi-isotropic than in a unidirectional laminate structure. The highest enhancements of the pullout energy were found on quasi-isotropic laminates with circular and sinusoidal notch designs with increases of up to 69%, in comparison to measurements on samples with unnotched z-pins. Full article
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41 pages, 31085 KiB  
Review
Review of Through-the-Thickness Reinforced z-Pinned Composites
by Vassilis Kostopoulos, Nikolaos Sarantinos and Stavros Tsantzalis
J. Compos. Sci. 2020, 4(1), 31; https://doi.org/10.3390/jcs4010031 - 20 Mar 2020
Cited by 35 | Viewed by 5256
Abstract
This work reviews the effects of z-Pins used in composite laminates as through-the-thickness reinforcement to increase the composite’s properties in the out-of-plane direction. The paper presents the manufacture and microstructure of this reinforcement type while also incorporating the impact of z-Pins on the [...] Read more.
This work reviews the effects of z-Pins used in composite laminates as through-the-thickness reinforcement to increase the composite’s properties in the out-of-plane direction. The paper presents the manufacture and microstructure of this reinforcement type while also incorporating the impact of z-Pins on the mechanical properties of the composite. Mechanical properties include tensile, compression, flexure properties in static, dynamic and fatigue loads. Additionally, mode I and mode II properties in both static and fatigue loading are presented, as well as hygrothermal, impact and compression after impact properties. Full article
(This article belongs to the Special Issue Feature Papers in Journal of Composites Science in 2019)
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12 pages, 8344 KiB  
Article
In Situ Study on Fracture Behavior of Z-Pinned Carbon Fiber-Reinforced Aluminum Matrix Composite via Scanning Electron Microscope (SEM)
by Yunhe Zhang, Sian Wang, Xiwang Zhao, Fanming Wang and Gaohui Wu
Materials 2019, 12(12), 1941; https://doi.org/10.3390/ma12121941 - 17 Jun 2019
Cited by 10 | Viewed by 2958
Abstract
Inside a scanning electron microscope (SEM) chamber, we performed an in situ interlaminar shear test on a z-pinned carbon fiber-reinforced aluminum matrix composite (Cf/Al) fabricated by the pressure the infiltration method to understand its failure mechanism. Experiments show that introducing a stainless-steel z-pin [...] Read more.
Inside a scanning electron microscope (SEM) chamber, we performed an in situ interlaminar shear test on a z-pinned carbon fiber-reinforced aluminum matrix composite (Cf/Al) fabricated by the pressure the infiltration method to understand its failure mechanism. Experiments show that introducing a stainless-steel z-pin increases the interlaminar shear strength of Cf/Al composite by 148%. The increase in interlaminar shear strength is attributed to the high strength of the stainless-steel z-pin and the strong bonding between the z-pin and the matrix. When the z-pin/matrix interface failed, the z-pin can still experience large shear deformation, thereby enhancing delamination resistance. The failure mechanism of composite includes interfacial debonding, aluminum plough, z-pin shear deformation, frictional sliding, and fracture. These results in this study will help us understand the interlaminar strengthening mechanism of z-pins in the delamination of metal matrix composites. Full article
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11 pages, 4485 KiB  
Article
Microstructure and Flexural Properties of Z-Pinned Carbon Fiber-Reinforced Aluminum Matrix Composites
by Sian Wang, Yunhe Zhang, Pibo Sun, Yanhong Cui and Gaohui Wu
Materials 2019, 12(1), 174; https://doi.org/10.3390/ma12010174 - 7 Jan 2019
Cited by 21 | Viewed by 4166
Abstract
Z-pinning can significantly improve the interlaminar shear properties of carbon fiber-reinforced aluminum matrix composites (Cf/Al). However, the effect of the metal z-pin on the in-plane properties of Cf/Al is unclear. This study examines the effect of the z-pin on the flexural strength and [...] Read more.
Z-pinning can significantly improve the interlaminar shear properties of carbon fiber-reinforced aluminum matrix composites (Cf/Al). However, the effect of the metal z-pin on the in-plane properties of Cf/Al is unclear. This study examines the effect of the z-pin on the flexural strength and failure mechanism of Cf/Al composites with different volume contents and diameters of the z-pins. The introduction of a z-pin leads to the formation of a brittle phase at the z-pin/matrix interface and microstructural damage such as aluminum-rich pockets and carbon fiber waviness, thereby resulting in a reduction of the flexural strength. The three-point flexural test results show that the adding of a metal z-pin results in reducing the Cf/Al composites’ flexural strength by 2–25%. SEM imaging of the fracture surfaces revealed that a higher degree of interfacial reaction led to more cracks on the surface of the z-pin. This crack-susceptible interface layer between the z-pin and the matrix is likely the primary cause of the reduction of the flexural strength. Full article
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14 pages, 2498 KiB  
Article
Interlaminar Shear Properties of Z-Pinned Carbon Fiber Reinforced Aluminum Matrix Composites by Short-Beam Shear Test
by Sian Wang, Yunhe Zhang and Gaohui Wu
Materials 2018, 11(10), 1874; https://doi.org/10.3390/ma11101874 - 1 Oct 2018
Cited by 14 | Viewed by 5496
Abstract
This paper presents the effect of through-thickness reinforcement by steel z-pins on the interlaminar shear properties and strengthening mechanisms of carbon fiber reinforced aluminum matrix composites (Cf/Al) with a short beam shear test method. Microstructural analysis reveals that z-pins cause minor microstructural damage [...] Read more.
This paper presents the effect of through-thickness reinforcement by steel z-pins on the interlaminar shear properties and strengthening mechanisms of carbon fiber reinforced aluminum matrix composites (Cf/Al) with a short beam shear test method. Microstructural analysis reveals that z-pins cause minor microstructural damage including to fiber waviness and aluminum-rich regions, and interface reaction causes a strong interface between the stainless steel pin and the aluminum matrix. Z-pinned Cf/Al composites show reduced apparent interlaminar shear strength due to a change in the failure mode compared to unpinned specimens. The changed failure mode could result from decreased flexural strength due to microstructural damage as well as increased actual interlaminar shear strength. Fracture work is improved significantly with a z-pin diameter. The strong interface allows the deformation resistance of the steel pin to contribute to the crack bridging forces, which greatly enhances the interlaminar shear properties. Full article
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9 pages, 5001 KiB  
Article
Experimental Characterization of the Properties of Double-Lap Needled and Hybrid Joints of Carbon/Epoxy Composites
by A. Arnautov, A. Nasibullins, V. Gribniak, I. Blumbergs and M. Hauka
Materials 2015, 8(11), 7578-7586; https://doi.org/10.3390/ma8115410 - 11 Nov 2015
Cited by 28 | Viewed by 5578
Abstract
The effect of through-thickness reinforcement by thin 1 mm steel needles (z-pins) on the static tensile strength of double-lap joints of a carbon/epoxy composite was investigated. Two types of joints—z-pinned and hybrid (including glued ones)—were considered. The joints were reinforced in the overlap [...] Read more.
The effect of through-thickness reinforcement by thin 1 mm steel needles (z-pins) on the static tensile strength of double-lap joints of a carbon/epoxy composite was investigated. Two types of joints—z-pinned and hybrid (including glued ones)—were considered. The joints were reinforced in the overlap region with 9, 25, or 36 z-pins. Comparing mechanical properties of the double-lap joints with the corresponding characteristics of their unpinned counterparts, the z-pins were found to be highly effective: the strength and stiffness of the pinned joints increased up to 300% and 280%, respectively. These improvements were due to a transition in the failure mechanism from debonding of the joint in the absence of z-pins to pullout or shear rupture of z-pins or to the tensile failure of laminate adherends, depending on the volume content of the pins. Full article
(This article belongs to the Section Advanced Composites)
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