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16 pages, 20415 KB  
Article
Flow-Line-Reducing Tetrahedral Metal Effect Pigments for Injection Molding: A Yield-Rate-Improved Particle Manufacturing Method Based on Soft UVImprint Lithography
by Nils Maximilian Demski, Holger Seidlitz, Felix Kuke, Oliver Niklas Dorn, Janina Zoglauer, Tobias Hückstaedt, Paul Hans Kamm, Francisco García-Moreno, Noah Kremp, Christian Dreyer and Dirk Oberschmidt
Polymers 2025, 17(19), 2708; https://doi.org/10.3390/polym17192708 - 8 Oct 2025
Abstract
This publication presents an improved manufacturing method for tetrahedral metal effect pigment particles that demonstrates reduced flowlines in injection-molded polymer components compared with conventional platelet-shaped pigment particles. The previously published cold forming process for tetrahedral particles, made entirely from aluminum, faced manufacturing challenges, [...] Read more.
This publication presents an improved manufacturing method for tetrahedral metal effect pigment particles that demonstrates reduced flowlines in injection-molded polymer components compared with conventional platelet-shaped pigment particles. The previously published cold forming process for tetrahedral particles, made entirely from aluminum, faced manufacturing challenges, resulting in a high reject rate due to particle adhesion to the micro-structured mold roller. In contrast, this study introduces a new manufacturing method for tetrahedral particles, now consisting of metallized UV-cured thermoset polymer. These particles, dispersed in amorphous matrix thermoplastics, have shown to maintain their shape during the injection molding process. The manufacturing technique for these novel particles is based on UV imprint lithography, omitting the reject rates compared with the previously presented cold rolling process of tetrahedral full aluminum particles. Thus, the novel manufacturing technique for tetrahedral pigment particles shows increased potential for automation through roll-to-roll manufacturing in the future. Full article
(This article belongs to the Special Issue 3D Printing and Molding Study in Polymeric Materials, 2nd Edition)
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21 pages, 6377 KB  
Article
Fatigue Strength Study of WAAM-Fabricated Shafts with Stacked Steel Ring Substrates Using Advanced Modeling
by Pham Son Minh, Quang Tri Truong and Van-Minh Nguyen
Metals 2025, 15(10), 1110; https://doi.org/10.3390/met15101110 - 6 Oct 2025
Viewed by 41
Abstract
This study investigates the fatigue performance of 3D-printed metal shafts fabricated via Wire Arc Additive Manufacturing (WAAM) with stacked steel ring substrates under rotating bending (ISO 1143:2021). A Taguchi L25 orthogonal array was used to analyze five process parameters: ring diameter, current intensity, [...] Read more.
This study investigates the fatigue performance of 3D-printed metal shafts fabricated via Wire Arc Additive Manufacturing (WAAM) with stacked steel ring substrates under rotating bending (ISO 1143:2021). A Taguchi L25 orthogonal array was used to analyze five process parameters: ring diameter, current intensity, torch speed, ring thickness, and contact tip to workpiece distance (CTWD). Analysis of Variance (ANOVA) identified ring diameter as the dominant factor, significantly enhancing fatigue life at 14.0 mm by reducing stress concentrations. Current intensity (125 A) and torch speed (550 mm/min) further improve weld quality and microstructure, while ring thickness (1.0 mm) and CTWD (1.5 mm) have minor effects. A linear regression model (R2 = 0.9603) accurately predicts fatigue life, with optimal settings yielding 299,730 cycles. The stacked-ring configuration enables intricate structures like cooling channels, ideal for aerospace and automotive applications. The 3.5% unexplained variance suggests parameter interactions, warranting further investigation into shielding gas effects and multiaxial loading to broaden material and loading applicability. Full article
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19 pages, 3238 KB  
Article
Vacuum Diffusion Bonding Process Optimization for the Lap Shear Strength of 7B04 Aluminum Alloy Joints with a 7075 Aluminum Alloy Powder Interlayer Using the Response Surface Method
by Ning Wang, Lansheng Xie and Minghe Chen
Metals 2025, 15(10), 1109; https://doi.org/10.3390/met15101109 - 6 Oct 2025
Viewed by 111
Abstract
The high-strength aluminum alloy 7B04 used in aircraft structures poses challenges in welding. In this study, 7075 aluminum alloy powder is used as an interlayer to strengthen the vacuum diffusion bonding (DB) joint of 7B04 aluminum alloy. Surface treatments with plasma activation before [...] Read more.
The high-strength aluminum alloy 7B04 used in aircraft structures poses challenges in welding. In this study, 7075 aluminum alloy powder is used as an interlayer to strengthen the vacuum diffusion bonding (DB) joint of 7B04 aluminum alloy. Surface treatments with plasma activation before DB can effectively increase the bonding rate and lap shear strength (LSS) of the joint. The effects of DB temperature, pressure, and holding time on the joint LSS were analyzed by developing a quadratic regression model based on the response surface method (RSM). The model’s determination coefficient reached 99.52%, with a relative error of about 5%, making it suitable for 7B04 aluminum alloy DB process parameters optimization and joint performance prediction. Two sets of process parameters (505 °C-5.7 h-4.5 MPa and 515 °C-7.5 h-4.4 MPa) were acquired using the satisfaction function optimization method. Experimental results confirmed that the error between measured and predicted LSS is approximately 5%, and a higher LSS of 174 MPa was achieved at 515 °C-7.5 h-4.4 MPa. Full article
(This article belongs to the Section Welding and Joining)
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17 pages, 10273 KB  
Article
Deep Learning-Based Approach for Automatic Defect Detection in Complex Structures Using PAUT Data
by Kseniia Barshok, Jung-In Choi and Jaesun Lee
Sensors 2025, 25(19), 6128; https://doi.org/10.3390/s25196128 - 3 Oct 2025
Viewed by 334
Abstract
This paper presents a comprehensive study on automated defect detection in complex structures using phased array ultrasonic testing data, focusing on both traditional signal processing and advanced deep learning methods. As a non-AI baseline, the well-known signal-to-noise ratio algorithm was improved by introducing [...] Read more.
This paper presents a comprehensive study on automated defect detection in complex structures using phased array ultrasonic testing data, focusing on both traditional signal processing and advanced deep learning methods. As a non-AI baseline, the well-known signal-to-noise ratio algorithm was improved by introducing automatic depth gate calculation using derivative analysis and eliminated the need for manual parameter tuning. Even though this method demonstrates robust flaw indication, it faces difficulties for automatic defect detection in highly noisy data or in cases with large pore zones. Considering this, multiple DL architectures—including fully connected networks, convolutional neural networks, and a novel Convolutional Attention Temporal Transformer for Sequences—are developed and trained on diverse datasets comprising simulated CIVA data and real-world data files from welded and composite specimens. Experimental results show that while the FCN architecture is limited in its ability to model dependencies, the CNN achieves a strong performance with a test accuracy of 94.9%, effectively capturing local features from PAUT signals. The CATT-S model, which integrates a convolutional feature extractor with a self-attention mechanism, consistently outperforms the other baselines by effectively modeling both fine-grained signal morphology and long-range inter-beam dependencies. Achieving a remarkable accuracy of 99.4% and a strong F1-score of 0.905 on experimental data, this integrated approach demonstrates significant practical potential for improving the reliability and efficiency of NDT in complex, heterogeneous materials. Full article
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16 pages, 6351 KB  
Article
The Role of La–Ti–Al–O Complex Inclusions in Microstructure Refinement and Toughness Enhancement of the Coarse-Grained Heat-Affected Zone in High-Heat-Input Welding
by Qiuming Wang, Jiangli He, Qingfeng Wang and Riping Liu
Metals 2025, 15(10), 1105; https://doi.org/10.3390/met15101105 - 3 Oct 2025
Viewed by 167
Abstract
The low-temperature impact properties of high-heat-input steels, particularly low-carbon Nb–Ti steel, are significantly influenced by the coarse-grained heat-affected zone (CGHAZ) in welded joints. The microstructure predominantly consists of granular bainitic ferrite (GBF), ferrite side plate (FSP), degenerate pearlite (DP), coarse plate-like ferrite (PF), [...] Read more.
The low-temperature impact properties of high-heat-input steels, particularly low-carbon Nb–Ti steel, are significantly influenced by the coarse-grained heat-affected zone (CGHAZ) in welded joints. The microstructure predominantly consists of granular bainitic ferrite (GBF), ferrite side plate (FSP), degenerate pearlite (DP), coarse plate-like ferrite (PF), and limited acicular ferrite (AF). This study investigates the effect of lanthanum (La) addition to Nb–Ti steel, leading to the formation of composite inclusions with a LaAlO3·TiN core surrounded by MnS/MnC precipitates. Unlike conventional Al2O3·MnS inclusions in Nb–Ti steel, these La-modified inclusions promote enhanced AF nucleation. This not only refines prior austenite grains but also reduces detrimental microstructural constituents such as GBF and FSP. As a result, the impact energy at −40 °C significantly improves from 23 J (Nb–Ti steel) to 137 J (Nb–Ti–La steel). Moreover, the inclusions exhibit an increase in size but a decrease in number density. The Nb–Ti–La variant demonstrates a higher AF volume fraction and increased AF density within the CGHAZ. The refined grain structure, along with an increased proportion of high-angle grain boundaries, effectively impedes secondary crack propagation. These microstructural modifications contribute to a substantial improvement in the low-temperature impact toughness of welded joints. Full article
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15 pages, 4711 KB  
Article
Experimental and Numerical Study of Laser Beam Welding of PBT-G30 for Electronic Housings in Automotive Applications
by Luiz R. R. Silva, Paulo D. P. Nunes, Eduardo A. S. Marques, Ricardo J. C. Carbas and Lucas F. M. da Silva
Polymers 2025, 17(19), 2662; https://doi.org/10.3390/polym17192662 - 1 Oct 2025
Viewed by 281
Abstract
This study investigates the application of laser spot welding to join protective housing components in the automotive electronics industry. The PBT GF 30 components were joined using two primary configurations: a purely overlapping joint and a top-overlap joint, both autogenous (i.e., without filler [...] Read more.
This study investigates the application of laser spot welding to join protective housing components in the automotive electronics industry. The PBT GF 30 components were joined using two primary configurations: a purely overlapping joint and a top-overlap joint, both autogenous (i.e., without filler material). To complement the experimental analysis, a numerical model, previously validated for a simpler joint configuration, was adapted and applied to configurations beyond the overlapping and top-overlap joint, more representative of practical automotive industry components. The results demonstrated that butt-overlap joints exhibited significantly higher strength (85% increase) than purely overlapping joints. This enhancement is attributed to the combined effect of normal and shear stresses in the top-overlap configuration, whereas purely overlapping joints rely solely on shear stress. The validated numerical model accurately predicted the experimental results, including displacement and force values. While minor deviations were observed, the numerical model’s predictions converged within the average experimental values and standard deviation, demonstrating that such a model can be used to precisely design laser-welded joints for similar applications. Full article
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17 pages, 6517 KB  
Article
Investigation of Process and Properties of Cu-Mn-Al Alloy Cladding Deposited on 27SiMn Steel via Cold Metal Transfer
by Jin Peng, Shihua Xie, Junhai Xia, Xingxing Wang, Zenglei Ni, Pei Wang and Nannan Chen
Crystals 2025, 15(10), 858; https://doi.org/10.3390/cryst15100858 - 30 Sep 2025
Viewed by 197
Abstract
This study systematically investigates the effects of welding current on the macro-morphology, microstructure, mechanical properties, and corrosion resistance of Cu-Mn-Al alloy coatings deposited on 27SiMn steel substrates using Cold Metal Transfer (CMT) technology. The 27SiMn steel is widely applied in coal mining, geology, [...] Read more.
This study systematically investigates the effects of welding current on the macro-morphology, microstructure, mechanical properties, and corrosion resistance of Cu-Mn-Al alloy coatings deposited on 27SiMn steel substrates using Cold Metal Transfer (CMT) technology. The 27SiMn steel is widely applied in coal mining, geology, and engineering equipment due to its high strength and toughness, but its poor corrosion and wear resistance significantly limits service life. To address this issue, a Cu-Mn-Al alloy (high-manganese aluminum bronze) was selected as a cladding material because of its superior combination of mechanical strength, toughness, and excellent corrosion resistance in saline and marine environments. Compared with conventional cladding processes, CMT technology enables low-heat-input deposition, reduces dilution from the substrate, and promotes defect-free coating formation. To the best of our knowledge, this is the first report on the fabrication of Cu-Mn-Al coatings on 27SiMn steel using CMT, aiming to optimize process parameters and establish the relationship between welding current, phase evolution, and coating performance. The experimental results demonstrate that the cladding layer width increases progressively with welding current, whereas the layer height remains relatively stable at approximately 3 mm. At welding currents of 120 A and 150 A, the cladding layer primarily consists of α-Cu, κII, β-Cu3Al, and α-Cu + κIII phases. At higher welding currents (180 A and 210 A), the α-Cu + κIII phase disappears, accompanied by the formation of petal-shaped κI phase. The peak shear strength (509.49 MPa) is achieved at 120 A, while the maximum average hardness (253 HV) is obtained at 150 A. The 120 A cladding layer demonstrates optimal corrosion resistance. These findings provide new insights into the application of CMT in fabricating Cu-Mn-Al protective coatings on steel and offer theoretical guidance for extending the service life of 27SiMn steel components in aggressive environments. Full article
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19 pages, 25806 KB  
Article
Optimizing the Y Content of Welding Wire for TIG Welding of Sand-Cast Mg-Y-RE-Zr Alloy
by Yikai Gong, Guangling Wei, Xin Tong, Guonan Liu, Yingxin Wang and Wenjiang Ding
Materials 2025, 18(19), 4549; https://doi.org/10.3390/ma18194549 - 30 Sep 2025
Viewed by 229
Abstract
The widespread application of WE43 (Mg-4Y-2Nd-1Gd-0.5Zr) alloy castings in aerospace components is hindered by the frequent formation of defects such as cracks, pores, and especially yttria inclusions. These defects necessitate subsequent welding. However, using homologous WE43 filler wires often exacerbates these issues, leading [...] Read more.
The widespread application of WE43 (Mg-4Y-2Nd-1Gd-0.5Zr) alloy castings in aerospace components is hindered by the frequent formation of defects such as cracks, pores, and especially yttria inclusions. These defects necessitate subsequent welding. However, using homologous WE43 filler wires often exacerbates these issues, leading to high crack susceptibility and reintroduction of inclusions. Herein, we propose a novel strategy of tailoring Y content in filler wires to achieve high-quality welded joint of WE43 sand castings. Systematic investigations reveal that reducing Y content to 2 wt.% (WE23) effectively suppresses oxide inclusion formation and significantly enhances the integrity of the joint. The fusion zone microstructure evolves distinctly with varying Y levels: grain size initially increases, peaking at 24 μm with WE43 wire, then decreases with further Y addition. Moreover, eutectic compounds transition from a semi-continuous to a continuous network structure with increasing Y content, deteriorating mechanical performance. Notably, joints welded with WE23 filler exhibit minimal performance loss, with ultimate tensile strength, yield strength, and elongation reaching 93.0%, 98.0%, and 97.4% of the sand-cast base metal, respectively. The underlying strengthening mechanisms and solute-second phase relationships are elucidated, highlighting the efficacy of optimizing Y content in welding wire design. This study provides valuable insights toward defect-free welding of high-performance Mg-RE alloy castings. Full article
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14 pages, 4473 KB  
Article
Research on Microstructure and Corrosion Behavior of Aluminum Alloy Laser-Welded Joints Assisted by Ultrasonic Vibration
by Di Bai, Ao Li, Jia Liu, Yan Shi, Hong Zhang and Li Yang
Micromachines 2025, 16(10), 1118; https://doi.org/10.3390/mi16101118 - 29 Sep 2025
Viewed by 205
Abstract
Laser welding of 6061 aluminum alloy often results in coarse microstructures and inferior corrosion resistance due to rapid solidification. This study introduces ultrasonic vibration as an auxiliary technique to address these limitations. The paper systematically investigates the influence of laser weld ultrasonic assistance [...] Read more.
Laser welding of 6061 aluminum alloy often results in coarse microstructures and inferior corrosion resistance due to rapid solidification. This study introduces ultrasonic vibration as an auxiliary technique to address these limitations. The paper systematically investigates the influence of laser weld ultrasonic assistance on the microstructure and corrosion behavior of a 6061-T6 aluminum alloy welded joint. The results demonstrate that ultrasonic assistance refined the grain structure and reduced the corrosion current density by 19.1% compared to conventional laser welding, achieving 73.6% of the base metal’s corrosion resistance. The enhancement is attributed to ultrasonic-induced acoustic streaming and cavitation, which promote equiaxed grain formation and impede corrosive penetration. The enhancement is attributed to ultrasonic-induced acoustic streaming and cavitation, which promote equiaxed grain formation and impede corrosive penetration. Under the ultrasonic effect, the number of dimples in the weld fracture increased and the depth was significant, which enhanced the tensile strength of the 6061 Aluminum alloy weld. This work provides a reliable and efficient strategy for producing high-performance aluminum alloy welded structures in industrial applications. Full article
(This article belongs to the Special Issue Optical and Laser Material Processing, 2nd Edition)
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21 pages, 3956 KB  
Article
Optimization of Parameters in Multi-Spot Projection Welding of Thin Aluminized Steel Sheets
by Alexandru Vladut Oprea, Robert Catalin Ciocoiu, George Constantin, Carmen Catalina Rusu and Ionelia Voiculescu
Appl. Sci. 2025, 15(19), 10530; https://doi.org/10.3390/app151910530 - 29 Sep 2025
Viewed by 260
Abstract
Welding is a technological variant of the electric resistance spot-welding process in which the machined protrusion on the surface is heated and rapidly deformed, and the small molten zone formed at the interface is then forged to form the weld spot. The paper [...] Read more.
Welding is a technological variant of the electric resistance spot-welding process in which the machined protrusion on the surface is heated and rapidly deformed, and the small molten zone formed at the interface is then forged to form the weld spot. The paper analyses the effects of projection welding parameter values for thin, low-carbon aluminized steel sheets. Two sets of 16 welded samples having three or five protrusions were performed and analyzed using the Taguchi method. The microstructural aspects were analyzed in cross sections made through the welded points, highlighting the expulsion or accumulated effects of the Al-Si alloy protective layer and the formation of intermetallic compounds. To estimate the effect of welding parameters, the samples were subjected to tensile strength tests, and the fracture mode was evaluated. It was found that the values of the breaking forces were close for the two types of samples analyzed, for identical values of the welding regime parameters, but the elongation at break was double in the case of samples with five protrusions. The breaking force increased from 10.9 kN for samples with three protrusions to 11.4 kN for samples with five protrusions, for the same values of welding parameters. Full article
(This article belongs to the Topic Welding Experiment and Simulation)
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20 pages, 8746 KB  
Article
Fatigue Performance of Q500qENH Weathering Steel Welded Joints at Low Temperature
by Lei Kang, Xuanming Shi, Tao Lan, Xiaowei Zhang, Chen Xue, Xiaopeng Wang, Zhengfei Hu and Qinyuan Liu
Materials 2025, 18(19), 4515; https://doi.org/10.3390/ma18194515 - 28 Sep 2025
Viewed by 266
Abstract
A systematic study was conducted on the fatigue performance of Q500qENH weathering steel welded joints under low-temperature conditions of −40 °C in this paper. Low-temperature fatigue tests were conducted on V-groove butt joints and cross-shaped welded joints and S-N curves with a 95% [...] Read more.
A systematic study was conducted on the fatigue performance of Q500qENH weathering steel welded joints under low-temperature conditions of −40 °C in this paper. Low-temperature fatigue tests were conducted on V-groove butt joints and cross-shaped welded joints and S-N curves with a 95% reliability level were obtained. A comparative analysis with the Eurocode 3 reveals that low-temperature conditions lead to a regular increase in the design fatigue strength for both types of welded joints. Fracture surface morphology was examined using scanning electron microscopy, and combined with fracture characteristic analysis, the fatigue fracture mechanisms of welded joints under low-temperature conditions were elucidated. Based on linear elastic fracture mechanics theory, a numerical simulation approach was employed to investigate the fatigue crack propagation behavior of welded joints. The results indicate that introducing an elliptical surface initial crack with a semi-major axis length of 0.4 mm in the model effectively predicts the fatigue life and crack growth patterns of both joint types. A parametric analysis was conducted on key influencing factors, including the initial crack size, initial crack location, and initial crack angle. The results reveal that these factors exert varying degrees of influence on the fatigue life and crack propagation paths of welded joints. Among them, the position of the initial crack along the length direction of the fillet weld has the most significant impact on the fatigue life of cross-shaped welded joints. Full article
(This article belongs to the Section Metals and Alloys)
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12 pages, 1923 KB  
Article
Microwave Resonant Probe-Based Defect Detection for Butt Fusion Joints in High-Density Polyethylene Pipes
by Jinping Pan, Chaoming Zhu and Lianjiang Tan
Polymers 2025, 17(19), 2617; https://doi.org/10.3390/polym17192617 - 27 Sep 2025
Viewed by 236
Abstract
With the widespread use of high-density polyethylene (HDPE) pipes in various industrial and municipal applications, ensuring the structural integrity of their joints is crucial. This paper presents a novel defect detection method based on a microwave resonant probe, designed to perform efficient and [...] Read more.
With the widespread use of high-density polyethylene (HDPE) pipes in various industrial and municipal applications, ensuring the structural integrity of their joints is crucial. This paper presents a novel defect detection method based on a microwave resonant probe, designed to perform efficient and non-destructive evaluation of butt fusion joints in HDPE pipes. The experimental setup integrates a microwave antenna and resonant cavity to record real-time variations in resonance frequency and S21 magnitude while scanning the pipe surface. This method effectively detects common defects, including cracks, holes, and inclusions, within the butt fusion joints. The results show that the microwave resonant probe exhibits high sensitivity in detecting HDPE pipe defects. It can identify different sizes of cracks and holes, and can distinguish between talc powder and sand particles. This technique offers a promising solution for pipeline health monitoring, particularly for evaluating the quality of welded joints in non-metallic materials. Full article
(This article belongs to the Special Issue Advanced Joining Technologies for Polymers and Polymer Composites)
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22 pages, 5246 KB  
Article
Improving Health and Safety in Welding Through Remote Human–Robot Collaboration
by Shahram Sheikhi, Sharath P. Subadra, Robert Langer, Lucas Christoph Ebel, Eduard Mayer, Patrick Zuther and Jochen Maaß
Processes 2025, 13(9), 3017; https://doi.org/10.3390/pr13093017 - 21 Sep 2025
Viewed by 527
Abstract
Welding is an essential process across various industries; however, it exposes workers to dangerous fumes, extreme heat and physical stress, which pose considerable health and safety hazards. To tackle these issues, this article introduces the creation of a remote-controlled human–robot welding system aimed [...] Read more.
Welding is an essential process across various industries; however, it exposes workers to dangerous fumes, extreme heat and physical stress, which pose considerable health and safety hazards. To tackle these issues, this article introduces the creation of a remote-controlled human–robot welding system aimed at safeguarding workers while ensuring the quality of the welds. The system monitors a welder’s torch movements through a stereoscopic sensor and accurately reproduces them with a robotic arm, facilitating real-time remote welding. Operated by a student, it effectively welded standardized sheet metals in overhead positions while adhering to critical quality standards. The weld geometry met ISO 5817 requirements, tensile strength surpassed the base material specifications, and bending and hardness assessments verified the durability and integrity of the welds. When utilized in hazardous settings, the system showcases its capability to produce high-quality welds while significantly enhancing worker safety, underscoring its potential for real-world industrial applications. Full article
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15 pages, 1401 KB  
Article
Kinetics of Luteolin Extraction from Peanut Shells and Reseda luteola for Potential Applications as a Biofunctional Ingredient
by Efstratios Episkopou, Dimitrios Tsimogiannis, Maria Giannakourou and Petros Taoukis
Processes 2025, 13(9), 3009; https://doi.org/10.3390/pr13093009 - 21 Sep 2025
Viewed by 331
Abstract
This study investigates the extraction kinetics of luteolin, a bioactive flavonoid with recognized antioxidant and health-promoting properties, from the aerial parts of Reseda luteola (dyer’s weld), with emphasis on its industrial potential. A comparative analysis with peanut shells (Arachis hypogea) identified [...] Read more.
This study investigates the extraction kinetics of luteolin, a bioactive flavonoid with recognized antioxidant and health-promoting properties, from the aerial parts of Reseda luteola (dyer’s weld), with emphasis on its industrial potential. A comparative analysis with peanut shells (Arachis hypogea) identified R. luteola as a superior source, containing 14 ± 3 mg of LUT/g of material, approximately eight times higher than the amount in peanut shells. Luteolin occurred predominantly as luteolin-7-O-glycoside (57%) and the aglycone (35%). Methanolic semi-batch extraction at 25 °C yielded 9.6 mg LUT/g (70%) within 60 min at a solid-to-liquid ratio of 1:9, demonstrating significantly greater solvent efficiency than conventional Soxhlet or maceration techniques. Kinetic modeling, based on Fick’s second law, revealed a biphasic process with a low rate constant ratio (3:1) between the two stages, indicating the need for process optimization. These results establish R. luteola as a cost-effective and sustainable source of luteolin for dietary supplements and functional foods, while indicating the need to explore alternative solvents and advanced extraction methods to further optimize yield and efficiency. Full article
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17 pages, 14013 KB  
Article
The Effect of Welding Parameters on the Morphology and Mechanical Properties of AA6061-T6/CF-PPS Friction Stir Lap Welding Joints
by Wenhao Xu, Yongyong Lin, Qiaobo Feng, Yangjun Wang, Jie Wang, Sizhe Niu and Ming Lou
Metals 2025, 15(9), 1049; https://doi.org/10.3390/met15091049 - 20 Sep 2025
Viewed by 349
Abstract
The application of lightweight materials in the automotive industry can effectively achieve further weight reduction while maintaining overall structural strength, thereby reducing energy consumption. Currently, friction stir spot welding (FSSW) is the primary method for joining carbon fiber-reinforced polyphenylene sulfide (CF-PPS) with aluminum [...] Read more.
The application of lightweight materials in the automotive industry can effectively achieve further weight reduction while maintaining overall structural strength, thereby reducing energy consumption. Currently, friction stir spot welding (FSSW) is the primary method for joining carbon fiber-reinforced polyphenylene sulfide (CF-PPS) with aluminum alloys. This study successfully achieved the connection between 6061-T6 aluminum alloy and CF-PPS using the more operationally convenient friction stir lap welding (FSLW) technique. The primary objective of this study was to explore the potential of expanding the welding technologies available for successfully joining these two dissimilar materials. The joint morphology and strength were analyzed through metallographic observation and tensile testing, and the effects of different welding parameters on the microstructure and mechanical properties of dissimilar joints were studied. The study demonstrated that the successful connection between AA6061-T6 and CF-PPS was primarily attributable to the combined effects of mechanical interlocking and mixture bonding. The joint strength demonstrated a maximum value of 9.41 MPa when the following parameters were set: a rotation speed of 1800 rpm, a welding speed of 40 mm/min, and a plunge depth of 0.2 mm. Although low rotation speed and low welding speed cannot form an effective mechanical interlocking structure for the joint, the failed joints have different causes. When the rotation and welding speeds are fixed, changing the plunge depth cannot change the interlocking structure of the joint. A larger plunge depth will thin the weld and greatly reduce the joint strength. Full article
(This article belongs to the Special Issue New Welding Materials and Green Joint Technology—2nd Edition)
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