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Keywords = thermoplastic face sheets

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18 pages, 4550 KB  
Article
Effect of Annealing on High Temperature Tensile Performance of 3D Printed Polyamide Carbon Fiber: A Comparative Study
by Theodor Florian Zach and Mircea Cristian Dudescu
J. Compos. Sci. 2025, 9(11), 624; https://doi.org/10.3390/jcs9110624 - 10 Nov 2025
Viewed by 1151
Abstract
Fused filament fabrication of thermoplastic composites, despite its recyclability, increased strength, and efficiency, faces structural limitations under elevated temperatures. The literature on heat treatments for improving the thermal resilience of accessible 3D printed composites is limited. Therefore, this study comprehensively presents the efficacy [...] Read more.
Fused filament fabrication of thermoplastic composites, despite its recyclability, increased strength, and efficiency, faces structural limitations under elevated temperatures. The literature on heat treatments for improving the thermal resilience of accessible 3D printed composites is limited. Therefore, this study comprehensively presents the efficacy of annealing on carbon fiber reinforced polyamide (PAHT-CF). The methodology includes uniaxial tensile testing of 200 samples across a wide temperature range (25–150 °C) and five different infill orientations, annealed as per the Technical Data Sheet (80 °C, 12 h). Scanning electron microscopy (SEM) of the fracture surfaces revealed the microstructural changes responsible for the improved properties after annealing. At 25 °C, annealing led to a 50% strength increase (63.88 MPa) and a 70% lower strain (2.65%). At 150 °C, the material maintained a 17.5% strength advantage (23.62 MPa) and a 17.5% reduction in strain (12.67%). The 0°, 90°, and 0/90° orientations exhibited the highest improvements, while the remainder displayed lower strengths and higher deformation beyond the glass transition temperature (70 °C). Overall, annealed PAHT-CF demonstrates high-temperature resilience, comparable to previously analyzed materials like carbon fiber reinforced polyether–ether–ketone (PEEK-CF). This makes it a potentially accessible alternative for the aerospace and automotive sectors. However, practical applications must consider the trade-off between its enhanced mechanical properties and the increased lead time from annealing. Full article
(This article belongs to the Special Issue Polymer Composites and Fibers, 3rd Edition)
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15 pages, 6728 KB  
Article
Flexural Analysis of Additively Manufactured Continuous Fiber-Reinforced Honeycomb Sandwich Structures
by Rafael Guerra Silva, Esteban Gonzalez, Andres Inostroza and Gustavo Morales Pavez
J. Manuf. Mater. Process. 2024, 8(5), 226; https://doi.org/10.3390/jmmp8050226 - 10 Oct 2024
Cited by 6 | Viewed by 2535
Abstract
This study explores the flexural behavior of continuous fiber-reinforced composite sandwich structures built entirely using material extrusion additive manufacturing. The continuous fiber additive manufacturing system used in this study works sequentially, thus enabling the addition of fiber reinforcement just in the face sheets, [...] Read more.
This study explores the flexural behavior of continuous fiber-reinforced composite sandwich structures built entirely using material extrusion additive manufacturing. The continuous fiber additive manufacturing system used in this study works sequentially, thus enabling the addition of fiber reinforcement just in the face sheets, where it is most effective. Three-point bending tests were carried out on sandwich panel specimens built using thermoplastic reinforced with continuous glass fiber to quantify the effect of fiber reinforcement and infill density in the flexural properties and failure mode. Sandwich structures containing continuous fiber reinforcement had higher flexural strength and rigidity than unreinforced sandwiches. On the other hand, an increase in the lattice core density did not improve the flexural strength and rigidity. The elastic modulus of fiber-reinforced 3D-printed sandwich panels exceeded the predictions of the analytical models; the equivalent homogeneous model had the best performance, with a 15% relative error. However, analytical models could not correctly predict the failure mode: wrinkle failure occurs at 75% and 30% of the critical load in fiber-reinforced sandwiches with low- and high-density cores, respectively. Furthermore, no model is currently available to predict interlayer debonding between the matrix and the thermoplastic coating of fiber layers. Divergences between analytical models and experimental results could be attributed to the simplifications in the models that do not consider defects inherent to additive manufacturing, such as air gaps and poor interlaminar bonding. Full article
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15 pages, 5135 KB  
Article
Low-Cost Surface Enhanced Raman Scattering for Bio-Probes
by Blessing Adewumi, Martin Feldman, Debsmita Biswas, Dongmei Cao, Li Jiang and Naga Korivi
Solids 2022, 3(2), 188-202; https://doi.org/10.3390/solids3020013 - 7 Apr 2022
Cited by 2 | Viewed by 3962
Abstract
Raman Spectroscopy is a well-known method for identifying molecules by their spectroscopic “fingerprint”. In Surface Enhanced Raman Scattering (SERS), the presence of nanometallic surfaces in contact with the molecules enormously enhances the spectroscopic signal. Raman enhancing surfaces are often fabricated lithographically or chemically, [...] Read more.
Raman Spectroscopy is a well-known method for identifying molecules by their spectroscopic “fingerprint”. In Surface Enhanced Raman Scattering (SERS), the presence of nanometallic surfaces in contact with the molecules enormously enhances the spectroscopic signal. Raman enhancing surfaces are often fabricated lithographically or chemically, but the throughput is low and the equipment is expensive. In this work a SERS layer was formed by the self-assembly of silver nanospheres from a hexane suspension onto an imprinted thermoplastic sheet (PET). In addition, the SERS layer was transferred and securely bonded to other surfaces. This is an important attribute for probes into solid specimen. Raman spectra were obtained with Rhodamine 6G (R6G) solution concentrations ranging from 1 mm to 1 nm. The methods described here produced robust and sensitive SERS surfaces with inexpensive equipment, readily available materials, and with no chemical or lithographic steps. These may be critical concerns to laboratories faced with diminishing funding resources. Full article
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15 pages, 8908 KB  
Technical Note
Innovation in Aircraft Cabin Interior Panels. Part II: Technical Assessment on Replacing Glass Fiber with Thermoplastic Polymers and Panels Fabricated Using Vacuum Forming Process
by Edgar Adrián Franco-Urquiza, Perla Itzel Alcántara Llanas, Victoria Rentería-Rodríguez, Raúl Samir Saleme, Rodrigo Ramírez Aguilar, Cecilia Zarate Pérez, Mauricio Torres-Arellano and Saúl Piedra
Polymers 2021, 13(19), 3258; https://doi.org/10.3390/polym13193258 - 24 Sep 2021
Cited by 9 | Viewed by 4948
Abstract
The manufacturing process of the aircraft cabin interior panels is expensive and time-consuming, and the resulting panel requires rework due to damages that occurred during their fabrication. The aircraft interior panels must meet structural requirements; hence sandwich composites of a honeycomb core covered [...] Read more.
The manufacturing process of the aircraft cabin interior panels is expensive and time-consuming, and the resulting panel requires rework due to damages that occurred during their fabrication. The aircraft interior panels must meet structural requirements; hence sandwich composites of a honeycomb core covered with two layers of pre-impregnated fiberglass skin are used. Flat sandwich composites are transformed into panels with complex shapes or geometries using the compression molding process, leading to advanced manufacturing challenges. Some aircraft interior panels are required for non-structural applications; hence sandwich composites can be substituted by cheaper alternative materials and transformed using disruptive manufacturing techniques. This paper evaluates the feasibility of replacing the honeycomb and fiberglass skin layers core with rigid polyurethane foams and thermoplastic polymers. The results show that the structural composites have higher mechanical performances than the proposed sandwich composites, but they are compatible with non-structural applications. Sandwich composite fabrication using the vacuum forming process is feasible for developing non-structural panels. This manufacturing technique is fast, easy, economical, and ecological as it uses recyclable materials. The vacuum forming also covers the entire panel, thus eliminating tapestries, paints, or finishes to the aircraft interior panels. The conclusion of the article describes the focus of future research. Full article
(This article belongs to the Special Issue Advanced Thermoplastic Polymers and Composites)
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16 pages, 4852 KB  
Article
Development of Thermoplastic Composite Reinforced Ultra-High-Performance Concrete Panels for Impact Resistance
by Reagan Smith-Gillis, Roberto Lopez-Anido, Todd S. Rushing and Eric N. Landis
Materials 2021, 14(10), 2490; https://doi.org/10.3390/ma14102490 - 12 May 2021
Cited by 8 | Viewed by 3373
Abstract
In order to improve flexural and impact performance, thin panels of steel fiber-reinforced ultra-high performance concrete (UHPC) were further reinforced with external layers of continuous fiber-reinforced thermoplastic (CFRTP) composites. CFRTP sheets were bonded to 305 × 305 × 12 mm UHPC panels using [...] Read more.
In order to improve flexural and impact performance, thin panels of steel fiber-reinforced ultra-high performance concrete (UHPC) were further reinforced with external layers of continuous fiber-reinforced thermoplastic (CFRTP) composites. CFRTP sheets were bonded to 305 × 305 × 12 mm UHPC panels using two different techniques. First, unidirectional E-glass fiber-reinforced tapes of polyethylene terephthalate glycol-modified (PETG) were arranged in layers and fused to the UHPC panels through thermoforming. Second, E-glass fiber woven fabrics were placed on the panel faces and bonded by vacuum infusion with a methyl methacrylate (MAA) polymer. Specimens were cut into four 150 mm square panels for quasi-static and low-velocity impact testing in which loads were applied at the panel centers. Under quasi-static loading, both types of thermoplastic composite reinforcements led to a 150–180% increase in both peak load capacity and toughness. Impact performance was measured in terms of both residual deformation and change in specimen compliance, and CFRTP additions were reduced both by 80% to 95%, indicating an increase in damage resistance. While both reinforcement fabrication techniques provided added performance, the thermoforming method was preferable due to its simplicity and fewer specialized tool requirements. Full article
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