Search Results (18)

Based on finite element simulation analysis, laminated ceramic tool materials with different structures were designed and the effect of laminated structure on tool state was investigated. Residual stresses in ceramic tool materials increase with the number of layers and layer–thickness ratio. Based on the simulation results, SiAlON-SiC-SiCw/SiAlON-Al₂O₃ ceramic tool materials (SCWAs) were prepared using the spark plasma sintering process, and the influence of residual stress on the mechanical properties and microstructure of laminated ceramic tool materials was studied. The mechanical properties of ceramic materials were significantly improved under the effect of residual stresses. The fracture toughness of SCWA4 with 7 layers and a layer–thickness ratio of 6 was 6.02 ± 0.19 MPa·m^1/2, and the front and side flexural strengths were 602 ± 19 MPa and 595 ± 17 MPa, 36.3% and 39.0% higher than homogeneous SiAlON ceramics, respectively. Full article

Sialon ceramic tool material has become one of the most ideal materials for the high-speed cutting of superalloy materials. However, studies on the geometric structure of sialon ceramic solid end mill is lacking at the present. In this work, the geometric structure of sialon ceramic end mills was designed for difficult-to-machine nickel-based superalloy materials. The cutting force and heat, flank wear and machined surface quality were analyzed to study the effect of the main parameters on tool performance. The results showed that the end mill experienced severe flank wear and chipping, which were the leading cause of its failure during high-speed cutting. The cutting force and temperature decreased gradually with the increase in the helix angle. With the increase in the rake angle, the flank wear and the quality of the machined surface of the specimen first decreased and then increased. With the increase in the relief angle, the cutting temperature of the ceramic end mill gradually decreased, and the cutting force and the machined surface roughness showed an initial decrease and then increased. When the helix angle, rake angle and relief angle were 35°, −15° and 12°, respectively, the sialon ceramic end mill exhibited the best cutting performance and obtained better machined surface quality in the nickel-based superalloys. Full article

DLC coatings have low adhesive bond strength with the substrate and a high level of residual stresses. This paper is devoted to researching a complex of characteristics of a DLC-Si coating deposited on samples of SiAlON ceramics with intermediate coatings (CrAlSi)N pre-formed to improve the adhesive bond strength employing vacuum-plasma spraying. DLC-Si coatings were formed by chemical vapor deposition in a gas mixture of acetylene, argon, and tetramethylsilane supplied through a multichannel gas purge system controlling the tetramethylsilane volume by 1, 4, 7, and 10%. The SiAlON samples with deposited (CrAlSi)N/DLC-Si coatings with different silicon content in the DLC layer were subjected to XPS and EDX analyses. Tribological tests were carried out under conditions of high-temperature heating at 800C. The nanohardness and elasticity modulus of the rational (CrAlSi)N/DLC-Si coating with Si-content of 4.1% wt. were 26 ± 1.5 GPa and 238 ± 6 GPa, correspondingly. The rational composition of (CrAlSi)N/DLC-Si coating was deposited on cutters made of SiAlON ceramics and tested in high-speed machining of aircraft nickel-chromium alloy compared to uncoated and DLC-coated samples. The average operating time (wear resistance) of (CrAlSi)N/DLC-Si(4.1% wt.)-coated end mills before reaching the accepted failure criterion was 15.5 min when it was 10.5 min for the original cutters. Full article

Silicon alumina nitride (SiAlON) and alumina toughened zirconia (ATZ) ceramics are applied for ceramic cutting tools to machine, e.g., cast iron, nickel base alloys and other difficult-to-machine materials. The state of the art technology for manufacturing of the cutting tool geometry is grinding. Laser processing of ceramics is already studied in terms of ablation rate and roughness evaluation with the application of dental implant manufacturing. In the present study, laser machining of the mentioned ceramics is explored with a laser beam source of 1064 nm wavelength and 10 ps pulse duration (FWHM). The angle dependent energy specific removal rate is described in a model and the optimal pulse fluence for the different materials and the irradiation angles can be derived. For processing at irradiation angle of up to 75° no decrease of the relative absorption could be observed. For ATZ, lowest surface roughness is determined for both, orthogonal and quasi-tangential processing angle. For SiAlON, the roughness decreases constantly for higher tilt angles. A significant difference in the material answer with change of the sample composition can be detected and the results show the potential of further developing SiAlON ceramics towards machineability for laser ablation. Full article

This work characterises the structure and mechanical properties, such as adhesion, of two different chemical vapour deposition (CVD) coatings deposited onto silicon aluminium oxynitride (Si₃N₄ + Al₂O₃ + Y₂O₃) round (RNGN) milling cutter tooling inserts. These inserts are often known by the trade abbreviation “SiAlON”. Wear was produced on the inserts using unidirectional sliding (pin-on-disc type) and scratch testing. Two coatings were investigated: a multilayer CVD coating (Coating A) with a composition of TiN + TiCN + Al₂O₃ and a bilayer coating (Coating B) with a composition of Al₂O₃ + TiN. Microstructural analysis was conducted after wear testing and Coating B demonstrated high stability when subjected to high alternating shear and tensile stresses, high abrasion resistance and very high adhesion to the SiAlON ceramic insert substrate when compared to Coating A. Coating A demonstrated a low capacity to distribute alternating shear and tensile stresses during the pin-on-disc and scratch testing, which led to failure. The scratch and pin-on-disc results from this study correlate highly with completed machining insert wear analysis that has used Coating A and Coating B SiAlON inserts to machine aged Inconel 718. Full article

A kind of multiscale β-sialon grain-reinforced Al₂O₃ matrix composite ceramic tool material, named ASN, was prepared and studied. For the ASN, β-sialon (molecular formula: Si₄Al₂O₂N₆) was synthesized in situ by a hot-pressing and solid-solution reaction process. A total of six samples were prepared at varying sintering temperatures and holding times under vacuum conditions. The solid solution reaction mechanism of β-sialon, the phase composition, mechanical properties, microstructure, and strengthening and toughening mechanisms of the composite ASN were investigated. As a result, within the experimental parameters, an optimal ASN tool material was obtained under a pressure of 32 MPa and at a temperature of 1550 °C for 20 min. The tested mechanical properties of the optimal sample were as follows: flexural strength 997 ± 59 MPa, fracture toughness 6.4 ± 0.3 MPa·m^1/2, Vickers hardness 18.2 ± 0.4 GPa, and relative density 98.1 ± 0.2%. According to crystal defect theory, the solid solution reaction mechanism of in-situ-synthesized β-sialon in an Al₂O₃ matrix involves a double mechanism of unequivalence (or hetero-valence) and interstitial filling. The multiscale β-sialon grains mainly consisted of four grains, which were elongated β-sialon grains with a diameter of 0.3–0.4 μm and an aspect ratio of 6–9, elongated β-sialon grains with a diameter of 70 nm and an aspect ratio of 10, β-sialon whiskers with a diameter of 0.2 μm and an aspect ratio of 12–15, and intragranular β-sialon whiskers with a diameter of 70 nm. The mechanical properties were improved due to strengthening and toughening mechanisms, such as mixed structure mode (intergranular and transgranular), elongated grain pullout, interface bonding, crack reflection, pinning, and bridging. Full article

SiAlON is one of the problematic and least previously studied but prospective cutting ceramics suitable for most responsible machining tasks, such as cutting sophisticated shapes of aircraft gas turbine engine parts made of chrome–nickel alloys (Inconel 718 type) with increased mechanical and thermal loads (semi-finishing). Industrially produced SiAlON cutting inserts are replete with numerous defects (stress concentrators). When external loads are applied, the wear pattern is difficult to predict. The destruction of the cutting edge, such as the tearing out of entire conglomerates, can occur at any time. The complex approach of additional diamond grinding, lapping, and polishing combined with an advanced double-layer (CrAlSi)N/DLC coating was proposed here for the first time to minimize it. The criterion of failure was chosen to be 0.4 mm. The developed tri-nitride coating sub-layer plays a role of improving the main DLC coating adhesion. The microhardness of the DLC coating was 28 ± 2 GPa, and the average coefficient of friction during high-temperature heating (up to 800 °C) was ~0.4. The average durability of the insert after additional diamond grinding, lapping, polishing, and coating was 12.5 min. That is superior to industrial cutting inserts and those subjected to (CrAlSi)N/DLC coating by 1.8 and 1.25 times, respectively. Full article

α-SiAlON is commonly used to machine superalloys owing to its desirable thermal and structural properties. α-SiAlON is among the crystalline forms of SiAlON and has more favorable properties than β-SiAlON. However, it becomes fragile during the machining of hard-to-cut materials due to its low fracture toughness and machinability. Recent research efforts focus on improving the thermal and structural properties of α-SiAlON using suitable dopants, nano-sized precursors, and the addition of metallic/ceramic reinforcement particles. The present study presents a material-by-design approach to designing and developing ceramic and metal-particle-reinforced Ca-α-SiAlON composites with properties tailored for the cutting tool applications. The mean-field homogenization theories and effective medium approximations implemented in an in-house code are used to effectively optimize the thermal and structural properties of the Ca-α-SiAlON composite by varying essential parameters such as inclusion material, volume fraction, porosity, particulate size, and thermal interface resistance. Individual properties of the matrix and reinforcements are considered in the computations of effective properties such as thermal conductivity, thermal expansion coefficient, modulus of elasticity, and fracture toughness. The main objective of the study is to enhance the thermal conductivity and fracture toughness of Ca-α-SiAlON, while lowering its thermal expansion coefficient. At the same time, the elastic modulus and hardness/strength must be maintained within an acceptable range. As a validation, Ni/Ca-α-SiAlON and SiC/Ca-α-SiAlON composites are synthesized from the nano-sized precursors, CaO dopant, and Ni/SiC microparticles via spark plasma sintering (SPS) process. The thermal conductivity, coefficient of thermal expansion, and elastic modulus of the composites are measured and compared with the computational predictions. The computational predictions are found to be comparable to that of the experimental measurements. Moreover, the studies show that WC, SiC, and Cr can be suitable reinforcement materials for enhancing the thermal and structural properties of Ca-α-SiAlON material for the cutting tool inserts. Full article

Nickel-based alloys, referred to as the most difficult-to-cut materials, pose a great challenge to cutting tool materials due to their excellent high-temperature properties. Ceramic tools have the potential to improve the machinability of these alloys with the advance of toughening mechanisms. In this work, the wear mechanisms of SiC whisker-reinforced alumina and Sialon when high-speed turning Inconel 718 alloy under dry cutting condition were investigated. The results showed that the wear process of Al₂O₃-SiC_w WG300 was dominated by the notch wear, while the flank wear characterized by ridges and grooves perpendicular to the cutting edge was the main wear mode for Sialon SX9. A Ti−enriched belt was found at the boundary of the wear band for both ceramic tools. The SEM inspection and EDS analysis for this belt suggested the trace of diffusion between the workpiece material and tool matrix. As for the notch formation, the periodically adhesive action of the workpiece material at the depth-of-cut line combined with the thermal shock resistance of ceramic tools were considered to account for its formation. In addition, the oxidation of the workpiece material at the depth-of-cut line played a positive role in reducing the adhesive affinity and consequent notch wear. Full article

This research aimed at an increase in wear resistance of round cutting plates manufactured with SiAlON dielectric ceramics through deposition of wear-resistant coatings. To increase effectiveness of the coatings, their adhesion was improved by the removal of defective surface layers from the cutting plates before the deposition. As the depth of caverns and grooves appearing on the cutting plates due to manufacturing by diamond grinding reached 5 µm, a concentrated beam of fast argon atoms was used for the removal of defective layers with a thickness exceeding the depth of caverns and grooves. At the equal angles of incidence to the front and back surfaces of the cutting wedge amounting to 45 degrees, two-hour-long etching of rotating cutting plates provided removal of defective layers with thickness of ~10 µm from the surfaces. After the removal, the cutting edge radius of the plates diminished from 20 to 10 µm, which indicates the cutting plates’ sharpening. Wear-resistant TiAlN coatings deposited after the etching significantly improve the processing stability and increase wear resistance of the cutting plates by not less than 1.7 times. Full article

The machining of nickel-based super alloys is challenging, owing to the generation of high cutting temperatures, as well as difficulty in maintaining dimensional accuracy and minimizing surface roughness, which compels the use of cutting fluids for reducing these issues due to efficient cooling/lubrication strategies. The present work investigates the comparative performance of four cooling/lubrication techniques: dry cutting, wet, minimum quantity lubricant (MQL) and compressed-air modes in turning Nitronic 60 steel using a new-generation SiAlON ceramic inserts. Several machinability parameters were analyzed for performance evaluation. For this purpose, 16 cycles of turning trials were performed based on Taguchi’s L₁₆ orthogonal array experimental design by varying cutting conditions and lubrication modes. MQL exhibits beneficial effects as compared to the other lubrication conditions concerning low cutting force, improved surface finish, decreased cutting temperature, longer tool life, and lower white layer thickness on machined surface. Burr formation on the saw-tooth chip surface, as well as friction, greatly influenced the tool flank wear due to improper cooling and poor lubrication approach in dry, wet, and compressed-air-cooled machining environments in comparison to MQL-machining. From an economical perspective, the tool life in MQL machining improved by 11%, 72%, and 138% in the comparison with flooded, compressed-air, and dry conditions, respectively. The results of the study demonstrate that using the MQL system can help with heat extraction capability, and provide some promising outcomes. Full article

Sustainable manufacturing has received great attention in the last few decades for obtaining high quality products with minimal costs and minimal negative impacts on environment. Sustainable machining is one of the main sustainable manufacturing branches, which is concerned with improving environmental conditions, reducing power consumption, and minimizing machining costs. In the current study, the performance of three sustainable machining techniques, namely dry, compressed air cooling, and minimum quantity lubrication, is compared with conventional flood machining during the turning of austenitic stainless steel (Nitronic 60). This alloy is widely used in aerospace engine components, medical applications, gas power industries, and nuclear power systems due to its superior mechanical and thermal properties. Machining was performed using SiAlON ceramic tool with four different cutting speeds, feeds and a constant depth of cut. Consequently, various chip characteristics such as chip morphology, chip thickness, saw tooth distance and chip segmentation frequency were analyzed with both optical and scanning electron microscopes. Performance assessment was performed under the investigated cutting conditions. Our results show that the tool life under MQL machining are 138%, 72%, and 11% greater than dry, compressed air, and flooded conditions, respectively. The use of SiAlON ceramic tool results is more economically viable under the MQL environment as the overall machining cost per component is lower ($0.27) as compared to dry ($0.36), compressed air ($0.31), and flooded ($0.29) machining conditions. The minimum quantity lubrication technique outperformed the other investigated techniques in terms of eco-friendly aspects, economic feasibility, and technical viability to improve sustainability. Full article

Nickel-based superalloys are attractive to many industrial sectors (automotive, military, energy, aerospace, etc.). However, their physical properties make them difficult to machining using traditional tools. Therefore, new materials for the machining of Ni-based alloys are required. Ceramic-based composites could act as a tool to replace the current materials. The incentives for this paper are to provide an overview of existing ceramic composites and draw some conclusions that will help in solving the problem of choosing materials for the processing of Ni-based superalloys. Despite the diversity of ceramic composites in this work, the possibility of using the SiAlON ceramic for Ni-based alloy machining is highlighted. Full article

Productivity in the manufacture of aircrafts components, especially engine components, must increase along with more sustainable conditions. Regarding machining, a solution is proposed to increase the cutting speed, but engines are made with very difficult-to-cut alloys. In this work, a comparison between two cutting tool materials, namely (a) cemented carbide and (b) SiAlON ceramics, for milling rough operations in Inconel^® 718 in aged condition was carried out. Furthermore, both the influence of coatings in cemented carbide milling tools and the cutting speed in the ceramic tools were analysed. All tools were tested until the end of their useful life. The cost performance ratio was used to compare the productivity of the tested tools. Despite the results showing higher durability of the coated carbide tool, the ceramic tools presented a better behavior in terms of productivity at higher speed. Therefore, ceramic tools should be used for higher productivity demands, while coated carbide tools for low speed-high volume material removal. Full article

The study is devoted to the development and testing of technological principles for the manufacture of solid end mills from ceramics based on a powder composition of α-SiAlON, β-SiAlON, and TiN additives, including spark plasma sintering powder composition, diamond sharpening of sintered ceramic blanks for shaping the cutting part of mills and deposition of anti-friction Si-containing diamond-like carbon (DLC) coatings in the final stage. A rational relationship between the components of the powder composition at spark plasma sintering was established. The influence of optimum temperature, which is the most critical sintering parameter, on ceramic samples’ basic physical and mechanical properties was investigated. DLC coatings’ role in changing the surface properties of ceramics based on SiAlON, such as microrelief, friction coefficient, et cetera, was studied. A comparative analysis of the efficiency of two tool options, such as developed samples of experimental mills made of SiAlON/TiN and commercial samples ceramic mills based on SiAlON, doped with stabilizing additives containing Yb when processing nickel alloys (NiCr20TiAl alloy was used as an example). DLC coatings’ contribution to the quantitative indicators of the durability of ceramic mills and the surface quality of machined products made of nickel alloy is shown. Full article