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Keywords = cylindrical anisotropy

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14 pages, 3233 KiB  
Article
Influence of Printing Parameters on Microstructure and Mechanical Properties of EOS NickelAlloy HX Produced via Laser Powder Bed Fusion
by Piotr Maj, Konstanty Jonak, Rafał Molak, Ryszard Sitek and Jarosław Mizera
Appl. Sci. 2025, 15(14), 8011; https://doi.org/10.3390/app15148011 - 18 Jul 2025
Viewed by 271
Abstract
The research investigated the influence of laser powder bed fusion (LPBF) parameters for NickelAlloy HX, a nickel-based superalloy, to achieve high-density components with superior mechanical properties. A systematic approach was employed, involving printing 40 cylindrical specimens with varying energy densities (50–240 J/mm3 [...] Read more.
The research investigated the influence of laser powder bed fusion (LPBF) parameters for NickelAlloy HX, a nickel-based superalloy, to achieve high-density components with superior mechanical properties. A systematic approach was employed, involving printing 40 cylindrical specimens with varying energy densities (50–240 J/mm3) to evaluate porosity, hardness, and anisotropy. Results revealed that energy density significantly influences relative density, with optimal parameters identified at 111 J/mm3 (900 mm/s scan speed, 120 W laser power). Microstructural examination revealed columnar grains aligned with the build direction in as-printed samples. The findings highlight the trade-offs between density, hardness, and microstructure in the additive manufacturing of nickel-based superalloys, providing actionable insights for industrial applications requiring specific property profiles. Full article
(This article belongs to the Special Issue The Applications of Laser-Based Manufacturing for Material Science)
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18 pages, 5103 KiB  
Article
Elastic Wave Propagation Through Cylinders with Fluid-Filled Fractures Using the Discontinuous Galerkin Method
by Ana L. Ramos-Barreto, Jonas D. De Basabe and Raul U. Silva-Avalos
Mathematics 2025, 13(10), 1572; https://doi.org/10.3390/math13101572 - 10 May 2025
Viewed by 384
Abstract
Accurately modeling fractures in wave-propagation simulations is challenging due to their small scale relative to other features. While equivalent-media models can approximate fracture-induced anisotropy, they fail to capture their discrete influence on wave propagation. To address this limitation, the Interior-Penalty Discontinuous Galerkin Method [...] Read more.
Accurately modeling fractures in wave-propagation simulations is challenging due to their small scale relative to other features. While equivalent-media models can approximate fracture-induced anisotropy, they fail to capture their discrete influence on wave propagation. To address this limitation, the Interior-Penalty Discontinuous Galerkin Method (IP-DGM) can be adapted to incorporate the Linear-Slip Model (LSM) to represent fractures explicitly. In this study, we apply IP-DGM to elastic wave propagation in fractured cylindrical domains using realistic fracture compliances obtained from laboratory experiments (using ultrasonic-pulse transmission) to simulate the effects of fluid-filled fractures. We analyze how fracture spacing and fluid type influence P- and S-wave behavior, focusing on amplitude attenuation and wave-front delays. Our numerical results align with experimental and theoretical predictions, demonstrating that higher-density fluids enhance wave transmission, reducing the impedance contrast and improving coupling across fracture surfaces. These findings highlight the capability of IP-DGM to accurately model wave propagation in realistic fractured and saturated media, providing a valuable tool for seismic monitoring in fractured reservoirs and other applications where fluid-filled fractures are prevalent. Full article
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18 pages, 13825 KiB  
Article
Effect of Load Vector Orientation on Uniaxial Compressive Strength of 3D Photoresin
by Evgenii Kozhevnikov, Mikhail Turbakov, Evgenii Riabokon, Zakhar Ivanov, Andrei Golosov, Arina Panteleeva and Yan Savitsky
J. Manuf. Mater. Process. 2025, 9(1), 23; https://doi.org/10.3390/jmmp9010023 - 14 Jan 2025
Cited by 1 | Viewed by 1022
Abstract
Rapid prototyping has a wide range of applications across various fields, both in industry and for private use. It enables the production of individual parts in a short time, independent of supply chains, which is particularly important in remote locations. Among all 3D [...] Read more.
Rapid prototyping has a wide range of applications across various fields, both in industry and for private use. It enables the production of individual parts in a short time, independent of supply chains, which is particularly important in remote locations. Among all 3D printing technologies, stereolithography using photo resins is the most accessible and offers the highest printing quality. However, the strength properties of parts made from photo resins remain a critical concern. In this study, we conducted experimental research to investigate the effect of load vector orientation under uniaxial compression on the elastic and mechanical properties of 3D-printed cylindrical samples. The results revealed that samples with layers oriented at 60° to the load vector exhibited the highest strength, while those with layers at 30° to the load vector showed the lowest strength. Samples with layers aligned parallel or perpendicular to the load vector demonstrated similar strength properties. Under quasi-elastic loading, samples with layers parallel to the load vector exhibited the highest Young’s modulus and the lowest Poisson’s ratio. Conversely, samples with layers oriented at 30° to the load vector displayed the highest Poisson’s ratio. Microstructural analysis revealed that the anisotropy in the mechanical properties of the 3D-printed samples is attributed to the layered, heterogeneous structure of the photoresin, which exhibits varying degrees of polymerization along the printing axes. The upper part of each layer, with a lower degree of polymerization, contributes to the ductile behavior of the samples under shear stresses. In contrast, the lower part of the layer, with a higher degree of polymerization, leads to brittle behavior in the samples. Full article
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15 pages, 4295 KiB  
Article
Local Stress in Cylindrically Curved Lipid Membrane: Insights into Local Versus Global Lateral Fluidity Models
by Konstantin V. Pinigin
Biomolecules 2024, 14(11), 1471; https://doi.org/10.3390/biom14111471 - 19 Nov 2024
Cited by 1 | Viewed by 1303
Abstract
Lipid membranes, which are fundamental to cellular function, undergo various mechanical deformations. Accurate modeling of these processes necessitates a thorough understanding of membrane elasticity. The lateral shear modulus, a critical parameter describing membrane resistance to lateral stresses, remains elusive due to the membrane’s [...] Read more.
Lipid membranes, which are fundamental to cellular function, undergo various mechanical deformations. Accurate modeling of these processes necessitates a thorough understanding of membrane elasticity. The lateral shear modulus, a critical parameter describing membrane resistance to lateral stresses, remains elusive due to the membrane’s fluid nature. Two contrasting hypotheses, local fluidity and global fluidity, have been proposed. While the former suggests a zero local lateral shear modulus anywhere within lipid monolayers, the latter posits that only the integral of this modulus over the monolayer thickness vanishes. These differing models lead to distinct estimations of other elastic moduli and affect the modeling of biological processes, such as membrane fusion/fission and membrane-mediated interactions. Notably, they predict distinct local stress distributions in cylindrically curved membranes. The local fluidity model proposes isotropic local lateral stress, whereas the global fluidity model predicts anisotropy due to anisotropic local lateral stretching of lipid monolayers. Using molecular dynamics simulations, this study directly investigates these models by analyzing local stress in a cylindrically curved membrane. The results conclusively demonstrate the existence of static local lateral shear stress and anisotropy in local lateral stress within the monolayers of the cylindrical membrane, strongly supporting the global fluidity model. These findings have significant implications for the calculation of surface elastic moduli and offer novel insights into the fundamental principles governing lipid membrane elasticity. Full article
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17 pages, 3768 KiB  
Article
A Study on Yield Criteria Influence on Anisotropic Behavior and Fracture Prediction in Deep Drawing SECC Steel Cylindrical Cups
by Quy-Huy Trieu, The-Thanh Luyen, Duc-Toan Nguyen and Ngoc-Tam Bui
Materials 2024, 17(12), 2872; https://doi.org/10.3390/ma17122872 - 12 Jun 2024
Cited by 3 | Viewed by 1515
Abstract
The deep drawing process, a pivotal technique in sheet metal forming, frequently encounters challenges such as anisotropy-induced defects. This study comprehensively investigates the influence of various yield criteria on the anisotropic behavior and fracture prediction in SECC steel cylindrical cups. It integrates Hill’48R, [...] Read more.
The deep drawing process, a pivotal technique in sheet metal forming, frequently encounters challenges such as anisotropy-induced defects. This study comprehensively investigates the influence of various yield criteria on the anisotropic behavior and fracture prediction in SECC steel cylindrical cups. It integrates Hill’48R, Hill’48S, and von Mises yield criteria in conjunction with Swift’s hardening law to evaluate material behavior under complex stress states. Experimental and numerical simulations assess the anisotropy effects across multiple orientations (0°, 45°, and 90°), revealing intricate relationships between stress criteria and material response. The findings indicate significant discrepancies between isotropic and anisotropic models in predicting fracture heights, emphasizing the importance of selecting appropriate yield criteria. Notably, the von Mises criterion results in lower fracture heights, suggesting higher susceptibility to fractures, while the Hill’48R model aligns closely with experimental data, validated through variations in punch corner radius and blank holder force parameters, with a maximum deviation of 3.23%. Hill’48S displays moderate plastic deformation characteristics. Full article
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21 pages, 5683 KiB  
Article
An Enhanced Approach for High-Strain Plasticity in Flat Anisotropic Specimens with Progressively Distorting Neck Sections
by Giuseppe Mirone, Raffaele Barbagallo, Giuseppe Bua, Pietro Licignano and Michele Maria Tedesco
Metals 2024, 14(5), 578; https://doi.org/10.3390/met14050578 - 14 May 2024
Cited by 2 | Viewed by 1613
Abstract
Characterizing the behavior of ductile metals at high strains is essential in various fields. In the case of thin sheets, rectangular cross-section specimens are used to characterize these materials, typically by tensile tests. Unlike cylindrical specimens, flat ones pose additional challenges for the [...] Read more.
Characterizing the behavior of ductile metals at high strains is essential in various fields. In the case of thin sheets, rectangular cross-section specimens are used to characterize these materials, typically by tensile tests. Unlike cylindrical specimens, flat ones pose additional challenges for the hardening characterization at high strains, especially in the post-necking phase, which, for many high-strength steels, may cover most of the plastic strain range. After the onset of global necking, the rectangular cross-sections tend to distort with respect to their original shape, as their edges progressively curve and bulge inward. The localized necking occurring after the global one in thinner specimens, further distorts the necked zone. Additionally, sheet metals usually exhibit anisotropic characteristics that affect the derivation of the stress–strain curve and need to be dealt with. No exact method exists for the stress–strain characterization of ductile thin sheets at high strains from tensile tests. Although several approximate methods are available in the literature, they either discard the post-necking range or require highly advanced and complex experimental setups not suitable for industrial applications (e.g., 3D DIC). Then, this work proposes a relatively simple methodology for the experimental characterization of anisotropic thin sheet metals through tensile tests on rectangular cross-section specimens that delivers the true stress–strain curve of the material, extended over the necking range and up to fracture, accurately assessing the anisotropy and the distortion of the neck section. The proposed methodology, employing a standard single-camera experimental setup, is illustrated here, referring to four different steels for automotive applications with reference to a single material orientation; it is intended as representative of the repeated procedure involving tensile tests along 3 or more material directions in order to describe the whole anisotropic plastic response. A detailed comparison between the novel methodology and four other common approaches is carried out, highlighting the differences and the enhanced capabilities of the novel one proposed. Full article
(This article belongs to the Special Issue Feature Papers in Structural Integrity of Metals)
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18 pages, 5616 KiB  
Article
Study of Anisotropic Behavior in Sheet Metal Forming
by Haibo Wang, Qiang Niu and Yu Yan
Materials 2024, 17(9), 2031; https://doi.org/10.3390/ma17092031 - 26 Apr 2024
Cited by 2 | Viewed by 2162
Abstract
Since sheet metal exhibits significant anisotropy in processing and forming, which has a significant impact on its performance during processing, forming, and use, we explore the anisotropic behavior of materials in the forming process of sheet metal. The ability of the Yld2000-2d criterion [...] Read more.
Since sheet metal exhibits significant anisotropy in processing and forming, which has a significant impact on its performance during processing, forming, and use, we explore the anisotropic behavior of materials in the forming process of sheet metal. The ability of the Yld2000-2d criterion to describe anisotropic behavior is analyzed, and its accuracy for characterization of the anisotropic behavior of metal plates is improved, based on which anisotropic behavior is predicted in three-dimensional space. Theoretical and experimental results on the anisotropy of sheet metal are compared, and two materials, 5754O aluminum alloy and DP980 steel plate, are tested and analyzed, and the anisotropic behaviors, such as three-point bending and cylindrical deep-drawing, are well predicted. Full article
(This article belongs to the Section Metals and Alloys)
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14 pages, 3166 KiB  
Article
Mathematical Modeling of Multi-Phenomena Anisotropic Systems: Ejection of Primary Aerosols during the Fast Pyrolysis of Biomass
by Mario A. Sánchez, Juan C. Maya, Farid Chejne, Brennan Pecha and Adriana M. Quinchía-Figueroa
Mathematics 2024, 12(6), 925; https://doi.org/10.3390/math12060925 - 21 Mar 2024
Cited by 2 | Viewed by 1578
Abstract
This study introduces a novel particle model for biomass fast pyrolysis, incorporating an anisotropic cylindrical particle to address mass and energy transport coupled with aerosol ejection, which previous models have overlooked. The main contribution lies in developing a model that considers aerosol generation [...] Read more.
This study introduces a novel particle model for biomass fast pyrolysis, incorporating an anisotropic cylindrical particle to address mass and energy transport coupled with aerosol ejection, which previous models have overlooked. The main contribution lies in developing a model that considers aerosol generation in anisotropic cylindrical particles for the first time, addressing bubbling dynamics and bursting within the liquid phase. The population balance equation describes bubble dynamics and aerosol formation, capturing phenomena like nucleation, growth, coalescence, and bursting. The model employs the method of moments with bubble volume as an internal variable, substantially reducing computational costs by eliminating dependence on this variable. Results highlight the significant impact of anisotropy and particle size on aerosol ejection: smaller, less elongated particles experience faster heating, quicker conversion, and the increased accumulation of the liquid intermediate phase. Specifically, 1 mm diameter particles yield higher concentrations of metaplast and bio-oil aerosols, exceeding 15%, compared to concentrations below 11% for 3 mm particles. This model provides insights into aerosol structure (volume, surface area), aiding in understanding aerosol reactivity at the reactor scale. Full article
(This article belongs to the Special Issue Computational Mathematics and Mathematical Modelling)
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9 pages, 2034 KiB  
Article
The Effect of Magnetoelastic Anisotropy on the Magnetization Processes in Rapidly Quenched Amorphous Nanowires
by Cristian Rotarescu, Sorin Corodeanu, Costică Hlenschi, George Stoian, Horia Chiriac, Nicoleta Lupu and Tibor-Adrian Óvári
Materials 2024, 17(5), 1141; https://doi.org/10.3390/ma17051141 - 29 Feb 2024
Viewed by 1029
Abstract
In this paper, we report for the first time on the theoretical and experimental investigation of Fe77.5Si7.5B15 amorphous glass-coated nanowires by analyzing samples with the same diameters in both cases. The hysteresis curves, the dependence of the switching [...] Read more.
In this paper, we report for the first time on the theoretical and experimental investigation of Fe77.5Si7.5B15 amorphous glass-coated nanowires by analyzing samples with the same diameters in both cases. The hysteresis curves, the dependence of the switching field values on nanowire dimensions, and the effect of the magnetoelastic anisotropy on the magnetization processes were analyzed and interpreted to explain the magnetization reversal in highly magnetostrictive amorphous nanowires prepared in cylindrical shape by rapid quenching from the melt. All the measured samples were found to be magnetically bistable, being characterized by rectangular hysteresis loops. The most important feature of the study is the inclusion of the magnetoelastic anisotropy term that originates in the specific production process of these amorphous nanowires. The results show that the switching field decreases when the nanowire diameter increases and this effect is due to the reduction in anisotropy and in the intrinsic mechanical stresses. Moreover, the obtained results reveal the importance of factors such as geometry and magnetoelastic anisotropy for the experimental design of cylindrical amorphous nanowires for multiple applications in miniaturized devices, like micro and nanosensors. Full article
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17 pages, 7115 KiB  
Article
Elastoplastic Solution of Cylindrical Cavity Expansion in Unsaturated Offshore Island Soil Considering Anisotropy
by Jifei Cui, Yanhao Jin, Yingjie Jing and Yu Lu
J. Mar. Sci. Eng. 2024, 12(2), 308; https://doi.org/10.3390/jmse12020308 - 9 Feb 2024
Cited by 11 | Viewed by 1288
Abstract
An elastoplastic analysis scheme for the cylindrical cavity expansion in offshore islands unsaturated soils considering anisotropy is established. The hydraulic properties and anisotropy caused by stress of unsaturated soils are coupled in an elastoplastic constitutive matrix for unsaturated soil to obtain the governing [...] Read more.
An elastoplastic analysis scheme for the cylindrical cavity expansion in offshore islands unsaturated soils considering anisotropy is established. The hydraulic properties and anisotropy caused by stress of unsaturated soils are coupled in an elastoplastic constitutive matrix for unsaturated soil to obtain the governing equations for the cylindrical cavity expansion problem, with an analytical solution that utilizes the original hydro-mechanical state of the soil as the initial conditions. Through a comparative analysis with other analytical solutions, the effectiveness of the new solution is verified. Moreover, the swelling response of the cylindrical cavity expansion in unsaturated soils is examined by systematically analyzing different parameters of the surrounding soil. The findings reveal that the development and rate of anisotropy in normal consolidated soil and over-consolidated soil exert a significant impact on the soil’s mechanical characteristics. Nevertheless, the alteration in the model constant h has little effect on the soil’s mechanical characteristics. The analytical solution introduces anisotropy and broadens the expansion theory of unsaturated soils to yield a more comprehensive theoretical framework for the comprehensive analysis of offshore islands’ unsaturated soils. Full article
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12 pages, 1751 KiB  
Article
3D Magnetization Textures: Toroidal Magnetic Hopfion Stability in Cylindrical Samples
by Konstantin Guslienko
Nanomaterials 2024, 14(1), 125; https://doi.org/10.3390/nano14010125 - 4 Jan 2024
Cited by 7 | Viewed by 2450
Abstract
Topologically non-trivial magnetization configurations in ferromagnetic materials on the nanoscale, such as hopfions, skyrmions, and vortices, have attracted considerable attention of researchers during the last few years. In this article, by applying the theory of micromagnetism, I demonstrate that the toroidal hopfion magnetization [...] Read more.
Topologically non-trivial magnetization configurations in ferromagnetic materials on the nanoscale, such as hopfions, skyrmions, and vortices, have attracted considerable attention of researchers during the last few years. In this article, by applying the theory of micromagnetism, I demonstrate that the toroidal hopfion magnetization configuration is a metastable state of a thick cylindrical ferromagnetic nanodot or a nanowire of a finite radius. The existence of this state is a result of the competition among exchange, magnetostatic, and magnetic anisotropy energies. The Dzyaloshinskii–Moriya exchange interaction and surface magnetic anisotropy are of second importance for the hopfion stabilization. The toroidal hopfion metastable magnetization configuration may be reached in the process of remagnetizing the sample by applying an external magnetic field along the cylindrical axis. Full article
(This article belongs to the Special Issue Magnetism and Magnetic Properties of Nanomaterials)
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15 pages, 4388 KiB  
Article
Three-Dimensional Printer-Assisted Electrospinning for Fabricating Intricate Biological Tissue Mimics
by Komal Raje, Keisuke Ohashi and Satoshi Fujita
Nanomaterials 2023, 13(22), 2913; https://doi.org/10.3390/nano13222913 - 8 Nov 2023
Cited by 3 | Viewed by 1758
Abstract
Although regenerative medicine necessitates advanced three-dimensional (3D) scaffolds for organ and tissue applications, creating intricate structures across scales, from nano- to meso-like biological tissues, remains a challenge. Electrospinning of nanofibers offers promise due to its capacity to craft not only the dimensions and [...] Read more.
Although regenerative medicine necessitates advanced three-dimensional (3D) scaffolds for organ and tissue applications, creating intricate structures across scales, from nano- to meso-like biological tissues, remains a challenge. Electrospinning of nanofibers offers promise due to its capacity to craft not only the dimensions and surfaces of individual fibers but also intricate attributes, such as anisotropy and porosity, across various materials. In this study, we used a 3D printer to design a mold with polylactic acid for gel modeling. This gel template, which was mounted on a metal wire, facilitated microfiber electrospinning. After spinning, these structures were treated with EDTA to remove the template and were then cleansed and dried, resulting in 3D microfibrous (3DMF) structures, with average fiber diameters of approximately 1 µm on the outer and inner surfaces. Notably, these structures matched their intended design dimensions without distortion or shrinkage, demonstrating the adaptability of this method for various template sizes. The cylindrical structures showed high elasticity and stretchability with an elastic modulus of 6.23 MPa. Furthermore, our method successfully mimicked complex biological tissue structures, such as the inner architecture of the voice box and the hollow partitioned structure of the heart’s tricuspid valve. Achieving specific intricate shapes required multiple spinning sessions and subsequent assemblies. In essence, our approach holds potential for crafting artificial organs and forming the foundational materials for cell culture scaffolds, addressing the challenges of crafting intricate multiscale structures. Full article
(This article belongs to the Special Issue Applications of Electrospinning-Based 3D Architecture Nanomaterials)
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12 pages, 3679 KiB  
Article
Magnetic Bimerons in Cylindrical Nanotubes
by David Galvez, Mario Castro, Guilherme Bittencourt, Vagson Carvalho and Sebastian Allende
Nanomaterials 2023, 13(21), 2841; https://doi.org/10.3390/nano13212841 - 26 Oct 2023
Cited by 2 | Viewed by 1874
Abstract
This work presents the analysis of the stability of magnetic bimerons in a cylindrical nanotube. Through micromagnetic simulations, we study the influence of magnetic and geometrical parameters on the bimeron existence and size. The obtained results allow us to present diagram states showing [...] Read more.
This work presents the analysis of the stability of magnetic bimerons in a cylindrical nanotube. Through micromagnetic simulations, we study the influence of magnetic and geometrical parameters on the bimeron existence and size. The obtained results allow us to present diagram states showing the stability region of a bimeron as a function of the nanotube’s height and radius for different anisotropy and Dzyaloshinskii–Moriya interaction strengths. We also obtain two other magnetic states in the range of parameters where the bimeron is not stable: helicoidal and saturated states. Full article
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15 pages, 6053 KiB  
Article
Effect of Process Variables on Interface Friction Characteristics in Strip Drawing of AA 5182 Alloy and Its Formability in Warm Deep Drawing
by Archit Shrivastava and Ravi Kumar Digavalli
J. Manuf. Mater. Process. 2023, 7(5), 175; https://doi.org/10.3390/jmmp7050175 - 29 Sep 2023
Cited by 3 | Viewed by 1970
Abstract
Warm forming is widely used to enhance the formability of aluminum alloy sheets. In warm deep drawing, the process variables significantly affect frictional characteristics at the tool–blank interface. It has been a conventional approach to use a constant value of friction coefficients in [...] Read more.
Warm forming is widely used to enhance the formability of aluminum alloy sheets. In warm deep drawing, the process variables significantly affect frictional characteristics at the tool–blank interface. It has been a conventional approach to use a constant value of friction coefficients in the finite element (FE) simulations. However, this can occasionally result in suboptimal accuracy of the predictions. In the present work, strip drawing tests were carried out on AA5182 aluminum alloy sheets to investigate the effect of important process variables, namely, temperature, contact pressure, and drawing speed, on the friction coefficient in the warm forming temperature range (100–250 °C) under lubricated condition. The results obtained from the strip drawing tests were used for defining the friction conditions in the simulation of warm deep drawing of cylindrical cups incorporating the variation of the friction coefficient with contact pressure and speed at different temperatures. The Barlat89 yield criterion was used to define the effect of anisotropy in the material. The Voce hardening law and Cowper–Symonds model were used to incorporate the effect of strain hardening and strain rate, respectively, in the simulation. Drawability and peak force were compared with the predictions when a constant friction coefficient was assumed. Warm deep drawing experiments were conducted to validate the predicted drawability and load–displacement curves. It is clearly observed that the accuracy of prediction of the limiting drawing ratio and peak load through simulations is improved by incorporating the effect of pressure and speed on friction coefficient as it captures the local variations of friction during warm deep drawing precisely, rather than assuming a constant average friction coefficient at all the tool–blank contact areas. Full article
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15 pages, 7102 KiB  
Article
Effects of Building Directions on Microstructure, Impurity Elements and Mechanical Properties of NiTi Alloys Fabricated by Laser Powder Bed Fusion
by Shuo Wang, Xiao Yang, Jieming Chen, Hengpei Pan, Xiaolong Zhang, Congyi Zhang, Chunhui Li, Pan Liu, Xinyao Zhang, Lingqing Gao and Zhenzhong Wang
Micromachines 2023, 14(9), 1711; https://doi.org/10.3390/mi14091711 - 31 Aug 2023
Cited by 3 | Viewed by 1827
Abstract
For NiTi alloys prepared by the Laser Powder Bed Fusion (LPBF), changes in the building directions will directly change the preferred orientation and thus directly affect the smart properties, such as superelasticity, as well as change the distribution state of defects and impurity [...] Read more.
For NiTi alloys prepared by the Laser Powder Bed Fusion (LPBF), changes in the building directions will directly change the preferred orientation and thus directly affect the smart properties, such as superelasticity, as well as change the distribution state of defects and impurity elements to affect the phase transformation behaviour, which in turn affects the smart properties at different temperatures. In this study, the relationship between impurity elements, the building directions, and functional properties; the effects of building directions on the crystallographic anisotropy; phase composition; superelastic properties; microhardness; geometrically necessary dislocation (GND) density; and impurity element content of NiTi SMAs fabricated by LPBF were systematically studied. Three building directions measured from the substrate, namely, 0°, 45° and 90°, were selected, and three sets of cylindrical samples were fabricated with the same process parameters. Along the building direction, a strong <100>//vertical direction (VD) texture was formed for all the samples. Because of the difference in transformation temperature, when tested at 15 °C, the sample with the 45° orientation possessed the highest strain recovery of 3.2%. When tested at the austenite phase transformation finish temperature (Af)+10 °C, the 90° sample had the highest strain recovery of 5.83% and a strain recovery rate of 83.3%. The sample with the 90° orientation presented the highest microhardness, which was attributed to its high dislocation density. Meanwhile, different building directions had an effect on the contents of O, C, and N impurity elements, which affected the transformation temperature by changing the Ni/Ti ratio. This study innovatively studied the impurity element content and GND densities of compressive samples with three building directions, providing theoretical guidance for LPBFed NiTi SMA structural parts. Full article
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