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Keywords = Near Solidus Forming

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14 pages, 3997 KB  
Article
Investigation of Die Design Influence on Required Forces in Near-Solidus Forging of Complex Components
by John Damilola Sunday, Alberto Murillo-Marrodán, Eduardo García and Carl Slater
J. Manuf. Mater. Process. 2025, 9(7), 245; https://doi.org/10.3390/jmmp9070245 - 21 Jul 2025
Viewed by 730
Abstract
This study investigates the influence of die design parameters on forging forces and thermomechanical responses during near-solidus forging (NSF) of complex steel components. Finite element simulations using Forge NxT analyzed six die configurations varying geometry orientation, gating system design (conical, cylindrical, curvilinear), and [...] Read more.
This study investigates the influence of die design parameters on forging forces and thermomechanical responses during near-solidus forging (NSF) of complex steel components. Finite element simulations using Forge NxT analyzed six die configurations varying geometry orientation, gating system design (conical, cylindrical, curvilinear), and draft angles (20° and 30°), with 42CrMo4E steel modeled at 1360 °C. Key responses including punch and lateral forces, temperature distribution, strain localization, and die stress were evaluated to assess design effects. Results showed that the gating system geometry critically controls material flow and load requirements. The conical gating design with a 30° draft angle yielded the lowest punch (141.54 t) and lateral (149.44 t) forces, alongside uniform temperature and strain distributions, which improve product quality by minimizing defects and incomplete filling. Lower lateral forces also reduce die opening risk, enhancing die life. In contrast, the base case with a 20° draft angle exhibited higher forces and uneven strain, increasing die stress and compromising part quality. These findings highlight the importance of selecting appropriate gating systems and draft angles to reduce forming loads, increase die life, and improve uniform material flow, contributing to better understanding of die design in NSF of complex steel components. Full article
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21 pages, 5639 KB  
Review
The Formation Mechanisms of np-Fe in Lunar Regolith: A Review
by Mingchao Xiong, Yanxue Wu, Wenqing Yao, Zilei Chen, Yingying Yu, Xia Li, Pan Yan, Xiongyao Li and Xiaojia Zeng
Materials 2024, 17(23), 5866; https://doi.org/10.3390/ma17235866 - 29 Nov 2024
Cited by 2 | Viewed by 2203
Abstract
Nanophase iron (np-Fe) is widely distributed on the surface of lunar soil particles, forming as a result of space weathering. These np-Fe particles contribute to the reddening and darkening of the visible to near-infrared spectra of weathered lunar material and serve as critical [...] Read more.
Nanophase iron (np-Fe) is widely distributed on the surface of lunar soil particles, forming as a result of space weathering. These np-Fe particles contribute to the reddening and darkening of the visible to near-infrared spectra of weathered lunar material and serve as critical indicators for assessing the maturity of lunar soil. (1) This article reviews the proposed formation mechanisms of np-Fe particles from studies of Apollo and Luna soils, including the thermal reduction of iron melts, vapor deposition caused by micrometeorite impacts, and hydrogen reduction due to solar wind exposure. (2) Additionally, recent findings from the analysis of Chang’E-5 lunar soil are highlighted, revealing new mechanisms such as sub-solidus decomposition of olivine, impact-driven disproportionation, and FeO eutectic reactions. (3) Experimental studies simulating space weathering through laser and ion irradiation are also discussed and compared. Despite extensive research, a definitive understanding of np-Fe particle formation remains elusive. Previous lunar soil samples have been collected from the near side of the Moon. This year, the Chang’E-6 mission has successfully returned the first-ever lunar soil samples from the far side. These samples are expected to exhibit unique space weathering characteristics, providing new insights into the formation mechanisms of np-Fe in lunar soil. Full article
(This article belongs to the Section Advanced Nanomaterials and Nanotechnology)
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15 pages, 10883 KB  
Article
Comprehensive Analysis of Microstructure and Hot Deformation Behavior of Al-Cu-Y-Mg-Cr-Zr-Ti-Fe-Si Alloy
by Sayed M. Amer, Maria V. Glavatskikh, Ruslan Yu. Barkov, Alexander Yu. Churyumov, Irina S. Loginova, Maxim G. Khomutov and Andrey V. Pozdniakov
Metals 2023, 13(11), 1853; https://doi.org/10.3390/met13111853 - 5 Nov 2023
Cited by 3 | Viewed by 2383
Abstract
Low sensitivity to hot cracking is very important not only for casting but also for ingots of wrought alloys. Doping of Al-Cu-(Mg) alloys by eutectic forming elements provides an increasing resistance to hot cracking susceptibility, but it also leads to a decrease in [...] Read more.
Low sensitivity to hot cracking is very important not only for casting but also for ingots of wrought alloys. Doping of Al-Cu-(Mg) alloys by eutectic forming elements provides an increasing resistance to hot cracking susceptibility, but it also leads to a decrease in plasticity. The quasi-binary alloys based on an Al-Cu-REM system with an atomic ratio of Cu/REM = 4 have a high solidus temperature, narrow solidification range and fine microstructure. The detailed investigation of microstructure, precipitation and hot deformation behavior, and mechanical properties of novel Al-Cu-Y-Mg-Cr-Zr-Ti-Fe-Si alloy was performed in this study. The fine Al8Cu4Y, needle-shaped Al11Cu2Y2Si2, compact primary (Al,Ti)84Cu6.4Y4.3Cr5.3 and Q (Al8Cu2Mg8Si6) phases were identified in the as-cast microstructure. Near-spherical coarse Al3(Zr,Y) and fine Al45Cr7 precipitates with a size of 60 nm and 10 nm were formed after 3 h of solution treatment at 580 °C. S′(Al2CuMg) precipitates with an average diameter of 140 nm, thickness of 6 nm and calculated volume fraction of 0.033 strengthened 36 HV during aging at 210 °C for 3 h. Three-dimensional hot processing maps demonstrated an excellent and stable deformation behavior at 440–540 °C and strain rates of 0.01–10 s−1. The rolled sheets had a good combination of yield strength (313 MPa) and plasticity (10.8%) in the recrystallized at 580 °C, with water quenched and aged at 210 °C for a 3 h state. The main calculated effect in the yield strength was contributed by Al45Cr7 precipitates. Full article
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12 pages, 3424 KB  
Perspective
Do Pegmatites Crystallise Fast? A Perspective from Petrologically-Constrained Isotopic Dating
by Daniil V. Popov
Geosciences 2023, 13(10), 297; https://doi.org/10.3390/geosciences13100297 - 2 Oct 2023
Cited by 2 | Viewed by 3127
Abstract
Most recent studies consider the formation of individual pegmatite bodies to be a fast process with estimated crystal growth rates reaching a walloping 10 m/day. This opinion is presumably underpinned by the traditional way of thinking of them as the end products of [...] Read more.
Most recent studies consider the formation of individual pegmatite bodies to be a fast process with estimated crystal growth rates reaching a walloping 10 m/day. This opinion is presumably underpinned by the traditional way of thinking of them as the end products of magmatic fractionation. Indeed, modelling has shown that if a pegmatite-forming substance with a temperature near granitic solidus intrudes into a much colder host rock, as recorded in some outcrops, it must cool rapidly. From here, a conclusion is made that the crystallisation must likewise be rapid. However, this view is challenged by several studies that published isotopic dates supported by petrological characterisation of the analysed materials, which suggested or can be used to suggest that some minerals in pegmatites grew over millions of years. Surprisingly, such in-depth work on the geochronology of individual pegmatite bodies is relatively uncommon, so it is early to make generalisations. Here, I highlight some of the existing evidence with the aim to stimulate further research into the timescales of pegmatite crystallisation, including the use of petrologically constrained isotopic dating. Full article
(This article belongs to the Section Geochemistry)
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19 pages, 4461 KB  
Article
A Preliminary Study of New Experimental Low-Cost Fe–P-Based and Mn–Fe–P-Based Brazing Filler Metals for Brazing of Non-Alloy and Low-Alloy Steels
by Matija Zorc, Borut Zorc, Jožef Medved and Aleš Nagode
Metals 2023, 13(9), 1513; https://doi.org/10.3390/met13091513 - 24 Aug 2023
Cited by 2 | Viewed by 1720
Abstract
Seventeen new experimental filler metals from eight different alloy systems based on Fe–P–X and Mn–Fe–P–X (X = B, C, Si in various combinations) were created and experimented with. DSC analyses were performed to determine the solidus and liquidus temperatures and the melting ranges. [...] Read more.
Seventeen new experimental filler metals from eight different alloy systems based on Fe–P–X and Mn–Fe–P–X (X = B, C, Si in various combinations) were created and experimented with. DSC analyses were performed to determine the solidus and liquidus temperatures and the melting ranges. Hardness measurements of the alloys were performed in the as-cast state. The alloys contain primary and eutectic intermetallic compounds that make them very hard with average hardness values ranging from 590 HV10 to 876 HV10. The wettability was determined at 1000 °C, 1040 °C and 1080 °C on C22 non-alloy steel and 15CrNiS6 low-alloy steel in Ar 4.6 and 78 vol% H2-22 vol% N2 atmospheres. The results show good wettability at T = 1080 °C in both atmospheres, as the contact angles were mostly ≤30°. Thirteen alloys exhibit very good wettability with average contact angles of ≤15.5°. Nine alloys exhibit excellent wettability with their average contact angles being ≤10°. Wettability improves at higher temperatures. The liquid alloys are reactive to solid steels and form a diffusion joint. Diffusion of P, B, C, and Si from the filler metal into the base material dealloys the composition of the melt near the joint interface. For the same reason, a continuous layer of solid solution forms on the joint interface. When brazing with filler metals rich in carbon, strong carburisation of steels can be observed near the joint. Full article
(This article belongs to the Section Welding and Joining)
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12 pages, 4032 KB  
Article
A Preliminary Study on the Quality of Joining AISI 316 and AISI 3415 Steel by the Near Solidus Forming Process
by Gorka Plata, Olaia Gordo-Burgoa, Jokin Lozares, Andrea Sánchez, Asier Bakedano, Iñaki Hurtado and Carl Slater
Metals 2023, 13(7), 1230; https://doi.org/10.3390/met13071230 - 4 Jul 2023
Viewed by 1438
Abstract
In this study, the Near Solidus Forming (NSF) process, which falls under the umbrella of semi-solid processes, was utilized to coforge an AISI 316 tube and an AISI 3415 rod into an as-forged valve geometry. The billet used for the process was kept [...] Read more.
In this study, the Near Solidus Forming (NSF) process, which falls under the umbrella of semi-solid processes, was utilized to coforge an AISI 316 tube and an AISI 3415 rod into an as-forged valve geometry. The billet used for the process was kept as large as possible to increase the contact surface area between the two materials. The process was carried out at 1360 °C in a single stroke, almost completely filling the geometry. No joining was observed in areas where low strains were expected, but in regions with medium to high strains, cross-diffusion of 2–7 μm was observed. The presence of small oxide particles was also observed in the joint due to the bimetallic billet shape. Full article
(This article belongs to the Special Issue Advances in Semi-solid Forming)
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14 pages, 6612 KB  
Article
Preliminary Study on the Capability of the Novel Near Solidus Forming (NSF) Technology to Manufacture Complex Steel Components
by Gorka Plata, Jokin Lozares, Andrea Sánchez, Iñaki Hurtado and Carl Slater
Materials 2020, 13(20), 4682; https://doi.org/10.3390/ma13204682 - 21 Oct 2020
Cited by 7 | Viewed by 2651
Abstract
The benefits of the novel Near Solidus Forming (NSF) process has shown previously in its ability to produce steel components with comparable as-forged mechanical properties but with a cost reduction of 10–15%. This study further pushes the NSF technology to produce parts that [...] Read more.
The benefits of the novel Near Solidus Forming (NSF) process has shown previously in its ability to produce steel components with comparable as-forged mechanical properties but with a cost reduction of 10–15%. This study further pushes the NSF technology to produce parts that are conventionally difficult to produce via conventional methods. A 2.7 kg 42CrMo4 steel grade component was manufactured into a complex geometry using only a 400t press. Different manufacturing parameters were evaluated to show their influence on the process and final component. A combination of X-ray fluorescence (XRF), optical microscopy and SEM analysis of the microstructure was also conducted revealing the deformation pattern of the material and shedding some light on how the material evolves during the process. The successful forging of these components shows the capability to produce previously deemed difficult geometries, with much a lower specification forging press, in a single deformation. Full article
(This article belongs to the Special Issue Forging Processes of Materials)
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15 pages, 5804 KB  
Article
Near Solidus Forming (NSF): Semi-Solid Steel Forming at High Solid Content to Obtain As-Forged Properties
by Jokin Lozares, Gorka Plata, Iñaki Hurtado, Andrea Sánchez and Iñigo Loizaga
Metals 2020, 10(2), 198; https://doi.org/10.3390/met10020198 - 30 Jan 2020
Cited by 15 | Viewed by 4035
Abstract
Near solidus forming (NSF) of steels is a novel process under the umbrella of semi-solid forming technologies midway between classical hot forging and semi-solid technologies. This article presents the work done at Mondragon Unibertsitatea to develop this technology and demonstrates the great potential [...] Read more.
Near solidus forming (NSF) of steels is a novel process under the umbrella of semi-solid forming technologies midway between classical hot forging and semi-solid technologies. This article presents the work done at Mondragon Unibertsitatea to develop this technology and demonstrates the great potential of the NSF process. The study proves the capability of the process to reduce raw material consumption by 20%, reduce forming loads from 2100 t to 300 t, and reduce forming steps from three to one, to obtain as-forged mechanical properties, as well as the excellent repeatability of the process. The work demonstrates that manufacturing commercial steel components in a single step using several off-the-shelf alloys is possible thanks to the flowing pattern of the material, which enables near-net shaping. In the first part of the article, a general overview of the semi-automated near solidus forming cell, together with a description of the NSF manufacturing trials, is provided, followed by the presentation and discussion of the results for the selected steel alloys. Full article
(This article belongs to the Special Issue Net-Shape Die Casting of Semi-solid Alloys)
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