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Article

Influence of Alpha/Gamma-Stabilizing Elements on the Hot Deformation Behaviour of Ferritic Stainless Steel

by
Andrés Núñez
1,2,*,
Irene Collado
1,
Marta Muratori
1,
Andrés Ruiz
1,
Juan F. Almagro
1 and
David L. Sales
2,*
1
Laboratory & Research Section, Technical Department, Acerinox Europa S.A.U., 11379 Palmones, Spain
2
Department of Materials Science and Metallurgical Engineering and Inorganic Chemistry, Algeciras School of Engineering and Technology, University of Cádiz, INNANOMAT, IMEYMAT, Ramón Puyol Ave., 11202 Algeciras, Spain
*
Authors to whom correspondence should be addressed.
J. Manuf. Mater. Process. 2025, 9(8), 265; https://doi.org/10.3390/jmmp9080265
Submission received: 4 July 2025 / Revised: 29 July 2025 / Accepted: 4 August 2025 / Published: 6 August 2025

Abstract

This study investigates the hot deformation behaviour and microstructural evolution of two AISI 430 ferritic stainless steel variants: 0A (basic) and 1C (modified). These variants primarily differ in chemical composition, with 0A containing higher austenite-stabilizing elements (C, N) compared to 1C, which features lower interstitial content and slightly higher Si and Cr. This research aimed to optimize hot rolling conditions for enhanced forming properties. Uniaxial hot compression tests were conducted using a Gleeble thermo-mechanical system between 850 and 990 C at a strain rate of 3.3 s1, simulating industrial finishing mill conditions. Analysis of flow curves, coupled with detailed microstructural characterization using electron backscatter diffraction, revealed distinct dynamic restoration mechanisms influencing each material’s response. Thermodynamic simulations confirmed significant austenite formation in both materials within the tested temperature range, notably affecting their deformation behaviour despite their initial ferritic state. Material 0A consistently exhibited a strong tendency towards dynamic recrystallization (DRX) across a wider temperature range, particularly at 850 C. DRX led to a microstructure with a high concentration of low-angle grain boundaries and sharp deformation textures, actively reorienting grains towards energetically favourable configurations. However, under this condition, DRX did not fully complete the recrystallization process. In contrast, material 1C showed greater activity of both dynamic recovery and DRX, leading to a much more advanced state of grain refinement and recrystallization compared to 0A. This indicates that the composition of 1C helps mitigate the strong influence of the deformation temperature on the crystallographic texture, leading to a weaker texture overall than 0A.
Keywords: FSS; hot deformation; DRX; DRV; LAGBs; crystallographic texture; EBSD; Gleeble simulation FSS; hot deformation; DRX; DRV; LAGBs; crystallographic texture; EBSD; Gleeble simulation

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MDPI and ACS Style

Núñez, A.; Collado, I.; Muratori, M.; Ruiz, A.; Almagro, J.F.; Sales, D.L. Influence of Alpha/Gamma-Stabilizing Elements on the Hot Deformation Behaviour of Ferritic Stainless Steel. J. Manuf. Mater. Process. 2025, 9, 265. https://doi.org/10.3390/jmmp9080265

AMA Style

Núñez A, Collado I, Muratori M, Ruiz A, Almagro JF, Sales DL. Influence of Alpha/Gamma-Stabilizing Elements on the Hot Deformation Behaviour of Ferritic Stainless Steel. Journal of Manufacturing and Materials Processing. 2025; 9(8):265. https://doi.org/10.3390/jmmp9080265

Chicago/Turabian Style

Núñez, Andrés, Irene Collado, Marta Muratori, Andrés Ruiz, Juan F. Almagro, and David L. Sales. 2025. "Influence of Alpha/Gamma-Stabilizing Elements on the Hot Deformation Behaviour of Ferritic Stainless Steel" Journal of Manufacturing and Materials Processing 9, no. 8: 265. https://doi.org/10.3390/jmmp9080265

APA Style

Núñez, A., Collado, I., Muratori, M., Ruiz, A., Almagro, J. F., & Sales, D. L. (2025). Influence of Alpha/Gamma-Stabilizing Elements on the Hot Deformation Behaviour of Ferritic Stainless Steel. Journal of Manufacturing and Materials Processing, 9(8), 265. https://doi.org/10.3390/jmmp9080265

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