High-Power Ultrasonic Synthesis and Magnetic-Field-Assisted Arrangement of Nanosized Crystallites of Cobalt-Containing Layered Double Hydroxides
Abstract
:1. Introduction
2. Materials and Methods
3. Results and Discussion
4. Conclusions
Author Contributions
Funding
Acknowledgments
Conflicts of Interest
References
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LDH Composition | a (Å) | c (Å) | d (Å) | |
---|---|---|---|---|
Co2Al–NO3 | Conventional co-precipitation followed by 4-h crystallization in a water bath | 3.063 | 26.732 | 8.911 |
Co2Al–NO3 (sonication-assisted crystallization) | 2 min | 3.049 | 26.585 | 8.862 |
5 min | 3.071 | 26.579 | 8.860 | |
10 min | 3.054 | 26.513 | 8.838 | |
Co2Al–CO3 | Standard anion-exchange (7 days) | 3.072 | 22.878 | 7.626 |
Sonication-assisted exchange (7 min) | 3.070 | 22.831 | 7.610 |
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Salak, A.N.; Vieira, D.E.L.; Lukienko, I.M.; Shapovalov, Y.O.; Fedorchenko, A.V.; Fertman, E.L.; Pashkevich, Y.G.; Babkin, R.Y.; Shilin, A.D.; Rubanik, V.V.; et al. High-Power Ultrasonic Synthesis and Magnetic-Field-Assisted Arrangement of Nanosized Crystallites of Cobalt-Containing Layered Double Hydroxides. ChemEngineering 2019, 3, 62. https://doi.org/10.3390/chemengineering3030062
Salak AN, Vieira DEL, Lukienko IM, Shapovalov YO, Fedorchenko AV, Fertman EL, Pashkevich YG, Babkin RY, Shilin AD, Rubanik VV, et al. High-Power Ultrasonic Synthesis and Magnetic-Field-Assisted Arrangement of Nanosized Crystallites of Cobalt-Containing Layered Double Hydroxides. ChemEngineering. 2019; 3(3):62. https://doi.org/10.3390/chemengineering3030062
Chicago/Turabian StyleSalak, Andrei N., Daniel E. L. Vieira, Irina M. Lukienko, Yuriy O. Shapovalov, Alexey V. Fedorchenko, Elena L. Fertman, Yurii G. Pashkevich, Roman Yu. Babkin, Aleksandr D. Shilin, Vasili V. Rubanik, and et al. 2019. "High-Power Ultrasonic Synthesis and Magnetic-Field-Assisted Arrangement of Nanosized Crystallites of Cobalt-Containing Layered Double Hydroxides" ChemEngineering 3, no. 3: 62. https://doi.org/10.3390/chemengineering3030062