Rheological, Microstructural, and Physicochemical Characterization of Pasta Fortified with Carrot Pomace: A Comparative Study of Wheat Types and Carrot Varieties
Abstract
1. Introduction
2. Materials and Methods
2.1. Materials
2.2. Hydration Capacity
2.3. Proximate Composition and Mineral Content
2.4. Total Polyphenol Content (TPC)
2.5. Total Yellow Pigments (TYPs)
2.6. Rheological Behavior
2.7. Texture Analysis
2.7.1. Dough Texture
2.7.2. Fracturability of Uncooked Pasta
2.7.3. Cooked Pasta Texture
2.8. Cooking Behavior
2.9. Color
2.10. Microstructure and Surface Structure
2.11. Sensory Properties
2.12. Statistics and Experimental Design
3. Results and Discussions
3.1. The Influence of the Type of Flour, the Addition Level, and the Type of Carrot Pomace on the Properties of Wheat Flour, Dough, and Pasta
3.2. Optimization of Flour Type and Carrot Pomace Dose
3.3. Characterization of the Optimal Samples
3.3.1. Rheological Properties of Dough
3.3.2. Chemical Composition and Bioactive Compounds
3.3.3. Physical and Structural Properties
3.3.4. Sensory Profile
3.3.5. Correlations and Principal Component Analysis
4. Conclusions
Supplementary Materials
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Acknowledgments
Conflicts of Interest
References
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| Factor | HC (%) | G* (Pa) | Jmax (Pa·s) | Dough Hardness (N) | Chroma (adim.) | CL (%) | Fracturability (N) | Chewiness (N) | TYPs (mg/kg) | Fiber (%) |
|---|---|---|---|---|---|---|---|---|---|---|
| p-Value | ||||||||||
| Model | <0.01 | <0.01 | <0.01 | <0.01 | <0.01 | <0.01 | <0.01 | <0.01 | <0.01 | <0.01 |
| A | <0.01 | <0.01 | <0.01 | <0.01 | <0.01 | <0.01 | 0.01 | 0.36 | <0.01 | 0.01 |
| B | <0.01 | <0.01 | <0.01 | <0.01 | <0.01 | <0.01 | <0.01 | <0.01 | <0.01 | <0.01 |
| C | <0.01 | <0.01 | <0.01 | <0.01 | <0.01 | 0.01 | <0.01 | <0.01 | <0.01 | <0.01 |
| AB | <0.01 | <0.01 | <0.01 | 0.01 | <0.01 | 0.61 | 0.12 | 0.93 | <0.01 | 0.04 |
| AC | <0.01 | <0.01 | <0.01 | <0.01 | <0.01 | 0.01 | <0.01 | <0.01 | <0.01 | 0.11 |
| BC | <0.01 | <0.01 | <0.01 | 0.97 | <0.01 | 0.07 | 0.31 | 0.01 | <0.01 | 0.01 |
| R2 | 0.98 | 0.84 | 0.84 | 0.89 | 0.91 | 0.84 | 0.85 | 0.75 | 0.90 | 0.88 |
| Adj-R2 | 0.97 | 0.82 | 0.82 | 0.88 | 0.90 | 0.82 | 0.83 | 0.71 | 0.89 | 0.86 |
| Pred.-R2 | 0.97 | 0.77 | 0.78 | 0.84 | 0.88 | 0.79 | 0.80 | 0.65 | 0.86 | 0.83 |
| CV (%) | 3.23 | 18.31 | 24.85 | 10.45 | 2.24 | 9.96 | 9.53 | 9.28 | 8.80 | 17.14 |
| Sample | Type of Values | F1Ba | F1Be | F1Ni | F1Si | F2Ba | F2Be | F2Ni | F2Si |
|---|---|---|---|---|---|---|---|---|---|
| Flour type-protein content (%) | - | F1 | F1 | F1 | F1 | F2 | F2 | F2 | F2 |
| Dose (%) | - | 6.34 | 9.25 | 8.30 | 7.71 | 8.12 | 9.06 | 10.36 | 11.17 |
| Carrot variety | - | Baltimore | Belgrado | Niagara | Sirkana | Baltimore | Belgrado | Niagara | Sirkana |
| HC (%) | predicted | 75.30 ± 2.37 Ay | 83.67 ± 2.37 Bx | 87.02 ± 2.37 Ax | 88.25 ± 2.37 Ax | 75.94 ± 2.37 Ay | 65.86 ± 2.37 Azw | 63.07 ± 2.37 Aw | 71.52 ± 2.37 Ayz |
| experimental | 74.87 ± 0.33 Ae | 88.25 ± 0.07 Aa | 83.18 ± 0.19 Ac | 81.00 ± 0.08 Ab | 69.54 ± 0.33 Be | 66.76 ± 0.30 Af | 65.18 ± 0.23 Ag | 74.76 ± 0.23 Ad | |
| G* (kPa) | predicted | 591.69 ± 83.29 Axy | 437.86 ± 83.29 Ay | 546.33 ± 83.29 Axy | 461.80 ± 83.29 Ay | 514.98 ± 83.29 Axy | 422.05 ± 83.29 Ay | 505.28 ± 83.29 Axy | 714.86 ± 83.29 Ax |
| experimental | 524.65 ± 2.75 Abcd | 469.80 ± 12.20 Acde | 535.60 ± 13.40 Abd | 456.80 ± 21.00 Ade | 511.02 ± 25.87 Abcd | 418.40 ± 4.00 Ae | 557.35 ± 13.95 Ab | 766.35 ± 60.35 Aa | |
| Jmax (Pa·s) | predicted | 3.80 ± 0.99 Axy | 2.25 ± 0.99 Ay | 2.59 ± 0.99 Ay | 3.33 ± 0.99 Axy | 3.92 ± 0.99 Axy | 5.39 ± 0.99 Ax | 2.33 ± 0.99 Ay | 1.73 ± 0.99 Ay |
| experimental | 3.46 ± 0.29 Abc | 2.24 ± 0.94 Ade | 2.75 ± 0.05 Acd | 3.48 ± 0.24 Abd | 3.81 ± 0.38 Ab | 5.40 ± 0.11 Aa | 2.08 ± 0.25 Ade | 1.64 ± 0.49 Ae | |
| Dough hardness (N) | predicted | 37.04 ± 3.40 Axyz | 39.67 ± 3.40 Axy | 44.49 ± 3.40 Ay | 35.76 ± 3.40 Axyz | 30.60 ± 3.40 Ayz | 28.28 ± 3.40 Az | 31.91 ± 3.40 Ayz | 32.74 ± 3.40 Ayz |
| experimental | 39.00 ± 1.28 Aabc | 41.22 ± 4.39 Aab | 44.71 ± 1.81 Aa | 38.82 ± 4.64 Aabc | 27.49 ± 3.76 Ad | 29.52 ± 4.25 Acd | 25.35 ± 1.85 Bd | 33.20 ± 4.91 Abcd | |
| Chroma (adim.) | predicted | 23.39 ± 0.50 Ax | 22.99 ± 0.50 Axy | 22.03 ± 0.50Bxy | 23.26 ± 0.50 Axy | 20.13 ± 0.50Bz | 19.95 ± 0.50 Az | 21.86 ± 0.50 By | 22.80 ± 0.50 Axy |
| experimental | 21.30 ± 0.05 Bd | 20.03 ± 1.03 Bf | 24.91 ± 0.61 Aa | 22.72 ± 0.19 Abc | 22.15 ± 0.20 Ac | 20.36 ± 0.04 Ae | 23.21 ± 0.29 Ab | 22.28 ± 0.07 Ae | |
| CL (%) | predicted | 6.82 ± 0.67 Axy | 7.58 ± 0.67 Axy | 7.65 ± 0.67 Axy | 7.71 ± 0.67 Axy | 6.10 ± 0.67 Ay | 6.38 ± 0.67 Axy | 8.12 ± 0.67 Ax | 7.02 ± 0.67 Axy |
| experimental | 6.45 ± 0.23 Ab | 7.82 ± 0.36 Aa | 7.72 ± 0.64 Aa | 7.72 ± 0.33 Aa | 7.38 ± 0.00 Aa | 7.64 ± 0.34 Aa | 7.94 ± 0.03 Aa | 7.82 ± 0.00 Aa | |
| Fracturability (N) | predicted | 52.28 ± 4.59 Axy | 60.66 ± 4.59 Ax | 50.75 ± 4.59 Axyz | 38.98 ± 4.59 Az | 44.77 ± 4.59 Ayz | 52.18 ± 4.59 Axy | 52.77 ± 4.59 Axy | 57.37 ± 4.59 Axy |
| experimental | 58.54 ± 1.66 Aa | 60.48 ± 7.30 Aa | 49.98 ± 5.11 Aabc | 40.83 ± 6.05 Ac | 45.13 ± 0.76 Abc | 48.37 ± 2.68 Aabc | 54.82 ± 4.54 Aab | 58.48 ± 4.20 Aa | |
| Masticability (N) | predicted | 24.15 ± 2.16 Axy | 24.52 ± 2.16 Axy | 20.81 ± 2.16 Axy | 21.79 ± 2.16 Axy | 19.62 ± 2.16 Ay | 19.00 ± 2.16 Ay | 24.88 ± 2.16 Axy | 26.59 ± 2.16 Ax |
| experimental | 22.97 ± 1.09 Aab | 21.97 ± 1.65 Aab | 20.56 ± 0.28 Abc | 20.26 ± 0.28 Abc | 18.00 ± 0.54 Ac | 19.30 ± 1.04 Abc | 23.15 ± 0.91 Aab | 24.93 ± 2.95 Aa | |
| TYPs (mg/kg) | predicted | 0.30 ± 0.03 Ay | 0.29 ± 0.03 Ay | 0.36 ± 0.03 Ay | 0.35 ± 0.03 Ay | 0.29 ± 0.03 Ay | 0.33 ± 0.03 Ay | 0.53 ± 0.03 Ax | 0.49 ± 0.03 Ax |
| experimental | 0.27 ± 0.01 Ae | 0.34 ± 0.00 Ac | 0.36 ± 0.01 Ab | 0.35 ± 0.00 Ac | 0.30 ± 0.00 Ad | 0.34 ± 0.00 Ac | 0.51 ± 0.00 Aa | 0.50 ± 0.00 Aa | |
| Crude fiber (%) | predicted | 0.77 ± 0.17 Az | 0.89 ± 0.17 Ayz | 1.03 ± 0.17 Ayz | 1.20 ± 0.17 Axyz | 1.05 ± 0.17 Ayz | 1.10 ± 0.17 Ayz | 1.29 ± 0.17 Axy | 1.66 ± 0.17 Ax |
| experimental | 0.81 ± 0.01 Ad | 0.93 ± 0.02 Ad | 1.09 ± 0.02 Ac | 1.18 ± 0.03 Ac | 1.11 ± 0.03 Ac | 1.17 ± 0.02 Ac | 1.40 ± 0.08 Ab | 1.65 ± 0.10 Aa |
| Sample | Protein (% d.w.) | Lipid (% d.w.) | Ash (% d.w.) | Crude Fiber (% d.w.) | Carbohydrates (% d.w.) | Energetic Value (kcal/100 g) | TPC (mg GAE/100 g d.w.) |
|---|---|---|---|---|---|---|---|
| F1 | 14.57 ± 0.03 b | 0.78 ± 0.04 d | 0.95 ± 0.03 f | 0.64 ± 0.03 e | 83.05 ± 0.14 d | 357.26 ± 0.04 b | 15.25 ± 0.09 a |
| F1Ba | 14.02 ± 0.03 c | 0.75 ± 0.03 d | 1.32 ± 0.02 c | 0.90 ± 0.01 d | 83.01 ± 0.03 d | 355.74 ± 0.13 c | 11.16 ± 0.04 f |
| F1Be | 12.72 ± 0.02 d | 0.88 ± 0.02 c | 1.60 ± 0.02 a | 1.04 ± 0.02 d | 83.76 ± 0.04 c | 354.33 ± 0.05 d | 10.72 ± 0.23 g |
| F1Ni | 14.52 ± 0.03 b | 0.74 ± 0.01 d | 1.43 ± 0.02 b | 1.22 ± 0.02 c | 82.08 ± 0.08 e | 353.21 ± 0.16 f | 12.39 ± 0.07 d |
| F1Si | 14.69 ± 0.02 a | 0.72 ± 0.04 d | 1.48 ± 0.01 b | 1.31 ± 0.03 c | 81.79 ± 0.05 f | 353.36 ± 0.17 ef | 10.28 ± 0.08 h |
| F2 | 12.13 ± 0.02 g | 1.19 ± 0.02 b | 0.54 ± 0.02 g | 0.63 ± 0.02 e | 85.51 ± 0.00 a | 358.94 ± 0.02 a | 14.80 ± 0.04 b |
| F2Ba | 12.43 ± 0.03 e | 0.50 ± 0.03 e | 1.11 ± 0.02 e | 1.22 ± 0.03 c | 84.73 ± 0.10 b | 354.00 ± 0.01 d | 11.11 ± 0.04 f |
| F2Be | 12.24 ± 0.03 f | 1.40 ± 0.04 a | 1.25 ± 0.02 d | 1.30 ± 0.02 c | 83.81 ± 0.02 c | 358.93 ± 0.35 a | 11.96 ± 0.10 e |
| F2Ni | 12.39 ± 0.03 e | 0.52 ± 0.03 e | 1.61 ± 0.01 a | 1.56 ± 0.09 b | 83.91 ± 0.02 c | 351.61 ± 0.20 g | 10.97 ± 0.08 fg |
| F2Si | 12.40 ± 0.03 e | 0.51 ± 0.04 e | 1.44 ± 0.01 b | 1.83 ± 0.11 a | 83.81 ± 0.03 c | 353.88 ± 0.32 de | 13.24 ± 0.09 c |
| Sample | Cooking Behavior | Uncooked Pasta Color | Cooked Pasta Color | ||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|
| OCT (min) | CL (%) | WA (%) | L* (adim.) | a* (adim.) | b* (adim.) | H (adim.) | L* (adim.) | a* (adim.) | b* (adim.) | H (adim.) | |
| F1 | 12.50 ± 0.00 b | 5.00 ± 0.30 c | 130.77 ± 7.71 c | 71.71 ± 0.39 b | 0.06 ± 0.05 d | 17.64 ± 0.17 f | 89.82 ± 0.14 a | 78.06 ± 1.27 a | −1.35 ± 0.28 h | 14.59 ± 0.32 h | 95.28 ± 1.00 a |
| F1Ba | 12.25 ± 0.25 bc | 6.45 ± 0.23 b | 133.36 ± 9.53 c | 75.83 ± 0.72 a | 0.41 ± 0.09 cd | 21.30 ± 0.05 cd | 88.89 ± 0.24 ab | 66.64 ± 0.44 e | 1.70 ± 0.21 ef | 21.87 ± 0.28 f | 85.57 ± 0.49 c |
| F1Be | 12.00 ± 0.00 c | 7.82 ± 0.36 a | 128.27 ± 1.30 c | 66.30 ± 0.84 cd | 0.66 ± 0.24 c | 20.02 ± 1.03 e | 88.13 ± 0.65 bc | 72.65 ± 0.24 c | 2.84 ± 0.08 d | 26.67 ± 0.23 cd | 83.93 ± 0.13 d |
| F1Ni | 12.50 ± 0.00 b | 7.72 ± 0.64 a | 133.41 ± 0.25 c | 71.15 ± 2.78 b | 1.88 ± 0.24 a | 24.83 ± 0.63 a | 85.67 ± 0.65 de | 72.38 ± 0.98 c | 1.99 ± 0.20 e | 25.63 ± 0.05 e | 85.57 ± 0.44 c |
| F1Si | 12.00 ± 0.00 c | 7.72 ± 0.33 a | 133.28 ± 3.21 c | 68.98 ± 0.56 bc | 1.91 ± 0.02 a | 22.64 ± 0.19 b | 85.19 ± 0.05 e | 72.40 ± 0.15 c | 1.52 ± 0.11 f | 26.53 ± 0.44 cd | 86.72 ± 0.17 c |
| F2 | 13.25 ± 0.25 a | 4.36 ± 0.06 c | 168.54 ± 8.43 a | 65.80 ± 0.31 d | 0.52 ± 0.10 cd | 16.07 ± 0.04 g | 88.16 ± 0.34 b | 75.52 ± 0.20 b | 0.18 ± 0.01 g | 19.95 ± 0.18 g | 89.49 ± 0.02 b |
| F2Ba | 13.25 ± 0.25 a | 7.38 ± 0.00 a | 125.15 ± 2.42 c | 63.98 ± 0.65 d | 2.10 ± 0.25 a | 22.05 ± 0.18 bc | 84.57 ± 0.60 e | 68.68 ± 0.18 d | 3.81 ± 0.06 ab | 27.46 ± 0.04 b | 82.11 ± 0.12 e |
| F2Be | 12.00 ± 0.00 c | 7.64 ± 0.34 a | 123.87 ± 1.28 c | 64.55 ± 0.42 d | 1.90 ± 0.05 a | 20.27 ± 0.04 de | 84.66 ± 0.12 e | 67.32 ± 0.47 de | 3.27 ± 0.09 cd | 26.11 ± 0.43 d | 82.87 ± 0.08 de |
| F2Ni | 12.50 ± 0.00 b | 7.94 ± 0.03 a | 135.01 ± 6.78 c | 63.58 ± 0.27 d | 1.28 ± 0.33 b | 23.17 ± 0.28 b | 86.85 ± 0.78 cd | 68.38 ± 0.22 d | 3.36 ± 0.22 bc | 27.18 ± 0.16 bc | 82.96 ± 0.41 de |
| F2Si | 12.00 ± 0.00 c | 7.82 ± 0.00 a | 150.83 ± 0.55 b | 63.96 ± 0.54 d | 1.22 ± 0.01 b | 22.24 ± 0.07 bc | 86.85 ± 0.01 cd | 67.81 ± 0.17 de | 3.95 ± 0.11 a | 29.01 ± 0.10 a | 82.25 ± 0.19 e |
| Sample | Chewiness (N) | Elasticity (%) | Cohesiveness (adim.) | Gumminess (N) | Firmness (N) |
|---|---|---|---|---|---|
| F1 | 10.51 ± 0.15 f | 99.98 ± 0.21 a | 0.36 ± 0.02 c | 10.53 ± 0.14 f | 27.64 ± 2.35 bc |
| F1Ba | 22.97 ± 1.09 abc | 99.95 ± 0.09 a | 0.67 ± 0.07 ab | 23.03 ± 1.08 ab | 32.90 ± 2.58 a |
| F1Be | 21.97 ± 1.65 abc | 99.84 ± 0.01 ab | 0.67 ± 0.01 ab | 21.45 ± 1.50 abc | 32.01 ± 0.53 ab |
| F1Ni | 20.56 ± 0.28 bcd | 99.84 ± 0.00 ab | 0.60 ± 0.03 b | 20.62 ± 0.28 bcd | 33.30 ± 0.90 a |
| F1Si | 20.26 ± 0.28 bcd | 99.83 ± 0.01 ab | 0.66 ± 0.04 ab | 20.34 ± 0.27 bcd | 31.70 ± 2.07 ab |
| F2 | 16.20 ± 1.10 e | 99.96 ± 0.07 a | 0.65 ± 0.03 ab | 16.23 ± 1.10 e | 25.48 ± 1.97 c |
| F2Ba | 18.00 ± 0.54 de | 99.84 ± 0.23 ab | 0.59 ± 0.04 b | 18.04 ± 0.55 de | 30.72 ± 1.37 ab |
| F2Be | 19.30 ± 1.04 cde | 99.65 ± 0.01 b | 0.61 ± 0.01 b | 19.38 ± 1.02 cde | 33.86 ± 2.00 a |
| F2Ni | 23.15 ± 0.91 ab | 99.68 ± 0.00 ab | 0.63 ± 0.04 ab | 22.68 ± 0.00 ab | 34.57 ± 0.00 a |
| F2Si | 24.93 ± 2.95 a | 99.83 ± 0.00 ab | 0.74 ± 0.06 a | 23.99 ± 2.49 a | 35.30 ± 0.43 a |
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Luca, M.I.; Ungureanu-Iuga, M.; Ciobanu, V.-G.; Batariuc, A.; Mironeasa, S. Rheological, Microstructural, and Physicochemical Characterization of Pasta Fortified with Carrot Pomace: A Comparative Study of Wheat Types and Carrot Varieties. Foods 2026, 15, 2201. https://doi.org/10.3390/foods15122201
Luca MI, Ungureanu-Iuga M, Ciobanu V-G, Batariuc A, Mironeasa S. Rheological, Microstructural, and Physicochemical Characterization of Pasta Fortified with Carrot Pomace: A Comparative Study of Wheat Types and Carrot Varieties. Foods. 2026; 15(12):2201. https://doi.org/10.3390/foods15122201
Chicago/Turabian StyleLuca, Marian Ilie, Mădălina Ungureanu-Iuga, Viorela-Gabriela Ciobanu, Ana Batariuc, and Silvia Mironeasa. 2026. "Rheological, Microstructural, and Physicochemical Characterization of Pasta Fortified with Carrot Pomace: A Comparative Study of Wheat Types and Carrot Varieties" Foods 15, no. 12: 2201. https://doi.org/10.3390/foods15122201
APA StyleLuca, M. I., Ungureanu-Iuga, M., Ciobanu, V.-G., Batariuc, A., & Mironeasa, S. (2026). Rheological, Microstructural, and Physicochemical Characterization of Pasta Fortified with Carrot Pomace: A Comparative Study of Wheat Types and Carrot Varieties. Foods, 15(12), 2201. https://doi.org/10.3390/foods15122201

