Antimicrobial Efficacy of Low Concentration PVP-Silver Nanoparticles Deposited on DBD Plasma-Treated Polyamide 6,6 Fabric
Abstract
:1. Introduction
2. Materials and Methods
3. Results
3.1. FTIR–ATR Analyses of Untreated and Plasma-Treated PA66 Samples
3.2. Reflectance Spectroscopy
3.3. SEM and EDS Analysis
3.4. XPS Analysis
3.5. Antibacterial Activity
4. Discussion
5. Conclusions
Author Contributions
Funding
Acknowledgments
Conflicts of Interest
References
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Samples | C (at %) | O (at %) | N (at %) | Ag (at %) | O/C Ratio | N/C Ratio |
---|---|---|---|---|---|---|
Spray | 80.5 | 11.0 | 8.5 | ND | 0.14 | 0.11 |
Spray DBD | 79.5 | 13.0 | 7.5 | ND | 0.16 | 0.09 |
Ex. 30 | 77.9 | 11.8 | 10.3 | ND | 0.15 | 0.13 |
Ex. 30 DBD | 77.0 | 12.5 | 9.0 | 1.5 | 0.16 | 0.12 |
Ex. 70 | 80.1 | 11.0 | 8.9 | ND | 0.14 | 0.11 |
Ex. 70 DBD | 79.9 | 11.6 | 8.2 | 0.3 | 0.15 | 0.10 |
Samples | Ag3d | C1s | O1s | N1s | ||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|
367.8 eV | 374.6 eV | 285.0 eV | 286.1 eV | 286.4 eV | 287.8 eV | 288.0 eV | 531.2 eV | 531.4 eV | 532.9 eV | 399.7 eV | 401.6 eV | |
Spray No DBD | – | – | 71.5 | 13.4 | – | 15.0 | – | 74.3 | – | 25.7 | 95.6 | 4.4 |
Spray DBD | – | – | 67.6 | – | 16.9 | 15.5 | – | – | 55.9 | 44.1 | 91.4 | 8.6 |
Ex. 30 No DBD | – | – | 70.0 | 15.1 | – | 14.9 | – | 73.6 | – | 26.3 | 93.3 | 6.7 |
Ex. 30 DBD | 52.2 | 47.8 | 67.2 | – | 16.5 | – | 16.3 | – | 71.4 | 28.6 | 93.4 | 6.6 |
Ex. 70 No DBD | – | – | 71.4 | 13.5 | – | 15.1 | – | 73.9 | – | 26.1 | 88.9 | 11.1 |
Ex. 70 DBD | 57.7 | 42.3 | 68.9 | – | 15.4 | – | 15.7 | – | 71.7 | 28.3 | 89.5 | 10.5 |
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Ribeiro, A.I.; Senturk, D.; Silva, K.K.; Modic, M.; Cvelbar, U.; Dinescu, G.; Mitu, B.; Nikiforov, A.; Leys, C.; Kuchakova, I.; et al. Antimicrobial Efficacy of Low Concentration PVP-Silver Nanoparticles Deposited on DBD Plasma-Treated Polyamide 6,6 Fabric. Coatings 2019, 9, 581. https://doi.org/10.3390/coatings9090581
Ribeiro AI, Senturk D, Silva KK, Modic M, Cvelbar U, Dinescu G, Mitu B, Nikiforov A, Leys C, Kuchakova I, et al. Antimicrobial Efficacy of Low Concentration PVP-Silver Nanoparticles Deposited on DBD Plasma-Treated Polyamide 6,6 Fabric. Coatings. 2019; 9(9):581. https://doi.org/10.3390/coatings9090581
Chicago/Turabian StyleRibeiro, Ana Isabel, Dilara Senturk, Késia Karina Silva, Martina Modic, Uros Cvelbar, Gheorghe Dinescu, Bogdana Mitu, Anton Nikiforov, Christophe Leys, Irina Kuchakova, and et al. 2019. "Antimicrobial Efficacy of Low Concentration PVP-Silver Nanoparticles Deposited on DBD Plasma-Treated Polyamide 6,6 Fabric" Coatings 9, no. 9: 581. https://doi.org/10.3390/coatings9090581