Microstructure and Properties of TiN/TiCN/Al2O3/TiN Coating Enhanced by High-Current Pulsed Electron Beam
Abstract
:1. Introduction
2. Materials and Methods
2.1. Preparation of Substrate and Coating
2.2. HCPEB Treatment
2.3. Characterization
3. Results and Discussion
3.1. Physical Phase Analysis
3.2. Microstructure Analysis
3.3. Mechanical Properties
4. Conclusions
- (1)
- After HCPEB treatment, the diffraction peak of the coating is widened and strengthened due to the formation of grain refinement and crystal defects. In addition, the stress state inside the coating also changes, and the diffraction peak shifts to a higher angle in different degrees compared with the original coating.
- (2)
- After HCPEB treatment, the surface of the coating has a typical melt-pit appearance, and the nanoscale grain appears. In addition, the surface roughness of the coating decreases after irradiation, reaching its minimum at 15 pulses. The thickness of the coating decreases with the increase of pulse time.
- (3)
- HCPEB treatment can effectively improve the surface microhardness of TiN/TiCN/Al2O3/TiN coating. The microhardness of the coating increases first and then decreases with the number of pulses, reaching a peak at 15 pulses.
- (4)
- HCPEB treatment can improve the friction and wear properties of TiN/TiCN/Al2O3/TiN coating. The wear mechanism of the original coating is mainly abrasive wear, the friction coefficient decreases after HCPEB irradiation, and the wear morphology is mainly adhesive wear. Among them, the coating wear performance after 15 pulses is the best.
- (5)
- It is proved that HCPEB treatment can change the internal structure and improve the hardness and wear resistance of the coating. This work presents the possibility of a new technology for the preparation of high-performance multilayer coatings, and also provides a new technological innovation and application prospect for the coating industry.
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
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Ge, F.; Xia, Z.; Yuan, H.; Guo, S.; Hu, Z.; Guan, J.; Cai, J.; Guan, Q.; Lyu, P. Microstructure and Properties of TiN/TiCN/Al2O3/TiN Coating Enhanced by High-Current Pulsed Electron Beam. Coatings 2024, 14, 378. https://doi.org/10.3390/coatings14040378
Ge F, Xia Z, Yuan H, Guo S, Hu Z, Guan J, Cai J, Guan Q, Lyu P. Microstructure and Properties of TiN/TiCN/Al2O3/TiN Coating Enhanced by High-Current Pulsed Electron Beam. Coatings. 2024; 14(4):378. https://doi.org/10.3390/coatings14040378
Chicago/Turabian StyleGe, Feiyu, Ziteng Xia, Haoming Yuan, Siyang Guo, Zhijun Hu, Jintong Guan, Jie Cai, Qingfeng Guan, and Peng Lyu. 2024. "Microstructure and Properties of TiN/TiCN/Al2O3/TiN Coating Enhanced by High-Current Pulsed Electron Beam" Coatings 14, no. 4: 378. https://doi.org/10.3390/coatings14040378
APA StyleGe, F., Xia, Z., Yuan, H., Guo, S., Hu, Z., Guan, J., Cai, J., Guan, Q., & Lyu, P. (2024). Microstructure and Properties of TiN/TiCN/Al2O3/TiN Coating Enhanced by High-Current Pulsed Electron Beam. Coatings, 14(4), 378. https://doi.org/10.3390/coatings14040378