Photocatalytic Activity of Titanium Dioxide Nanotubes Following Long-Term Aging
Abstract
:1. Introduction
2. Methodology
2.1. Material Synthesis
2.2. Aging Test Setup
2.3. Preparation of Synthetic Greywater
2.4. Sample Handling and Testing
2.4.1. Morphological Investigation
2.4.2. Methylene Blue Dye Degradation Tests
3. Results and Discussion
3.1. Morphology and Chemical Composition
3.2. Effect of Aging on the Photocatalytic Activity
4. Conclusions
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
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Chemical | Concentration in the Final Solution mg/L | Working Concentration 1:100 Preparation of 10 L Stock (g) |
---|---|---|
Ammonium Chloride | 12.2 | 12.2 |
Calcium Carbonate | 2.1 | 2.1 |
Calcium Chloride | 63.5 | 63.5 |
CAPB | 4.0 | 4.0 |
Polyquaterium-10 | 4.0 | 4.0 |
Magnesium Sulfate anhydrous | 110 | 110 |
Potassium Chloride | 7.3 | 7.3 |
Sodium hydrogen carbonate | 29.5 | 29.5 |
Sodium Chloride | 120 | 120 |
SDS | 15 | 15 |
Sodium nitrate | 4.0 | 4.0 |
Sodium Sulfate | 100 | 100 |
Yeast extract | 49.0 | 49.0 |
Testing Period | Test Duration |
---|---|
1 | After: 4 Weeks |
2 | 8 Weeks |
3 | 16 Weeks |
4 | 32 Weeks |
5 | 52 Weeks |
Material | Parameters | Layer Thickness (µm) | Tube Diameter (nm) | Wall Thickness (nm) | Aspect Ratio |
---|---|---|---|---|---|
TiO2NT-O | 70 V, 1 h | 9.99 ± 0.48 | 85–125 | 10.0 ± 2.00 | 80–117 |
TiO2NT-S | 20 V, 6 h | 1.45 ± 0.07 | 60–100 | 14 ± 2.00 | 14–24 |
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Abela, S.; Farrugia, C.; Xuereb, R.; Lia, F.; Zammit, E.; Rizzo, A.; Refalo, P.; Grech, M. Photocatalytic Activity of Titanium Dioxide Nanotubes Following Long-Term Aging. Nanomaterials 2021, 11, 2823. https://doi.org/10.3390/nano11112823
Abela S, Farrugia C, Xuereb R, Lia F, Zammit E, Rizzo A, Refalo P, Grech M. Photocatalytic Activity of Titanium Dioxide Nanotubes Following Long-Term Aging. Nanomaterials. 2021; 11(11):2823. https://doi.org/10.3390/nano11112823
Chicago/Turabian StyleAbela, Stephen, Clayton Farrugia, Ryan Xuereb, Frederick Lia, Edwin Zammit, Alex Rizzo, Paul Refalo, and Maurice Grech. 2021. "Photocatalytic Activity of Titanium Dioxide Nanotubes Following Long-Term Aging" Nanomaterials 11, no. 11: 2823. https://doi.org/10.3390/nano11112823