Determining Optimal Dosage of High-Modulus Asphalt Binders Through Comprehensive Rheological Assessment Across Full Temperature Range
Abstract
1. Introduction
2. Objectives and Scopes
- Establish an enhanced MSCR approach to quantify the permanent deformation resistance and stress sensitivity of high-modulus binders in high temperatures and to improve dosage discriminability within the effective operating domain.
- Develop a comprehensive full-temperature-range evaluation framework for high-modulus modified binders to support dosage identification and engineering decision-making.
3. Materials and Test Methods
3.1. Materials and Sample Preparation
3.1.1. The Base Binder
3.1.2. The High-Modulus Additive
3.2. Sample Preparation
3.3. Test Methods
3.3.1. High-Temperature Performance Grade (PG) Test
3.3.2. MSCR Test
3.3.3. LAS Test
3.3.4. Asphalt Binder Cracking Device (ABCD) Test
4. Results and Discussion
4.1. High-Temperature Rheological Performance
4.1.1. High-Temperature PG Test Results
4.1.2. Effective Stress Range for the MSCR Test
4.1.3. Results of the Enhanced MSCR Test
4.2. Intermediate-Temperature Performance
LAS Test Results
4.3. Low-Temperature Performance
4.4. High-Modulus Dosage Optimization Based on Full-Temperature-Range Performance
5. Conclusions
Author Contributions
Funding
Data Availability Statement
Conflicts of Interest
References
- Chen, Y.; Wang, H.; Xu, S.; You, Z. High Modulus Asphalt Concrete: A State-of-the-Art Review. Constr. Build. Mater. 2020, 237, 117653. [Google Scholar] [CrossRef]
- Zou, X.; Sha, A.; Jiang, W.; Huang, X. Modification Mechanism of High Modulus Asphalt Binders and Mixtures Performance Evaluation. Constr. Build. Mater. 2015, 90, 53–58. [Google Scholar] [CrossRef]
- Ullah, A.; Wen, H.P.; Ullah, Z.; Ali, B.; Khan, D. Evaluation of High Modulus Asphalts in China, France, and USA for Durable Road Infrastructure, a Theoretical Approach. Constr. Build. Mater. 2024, 432, 136622. [Google Scholar] [CrossRef]
- Geng, H.; Clopotel, C.S.; Bahia, H.U. Effects of High Modulus Asphalt Binders on Performance of Typical Asphalt Pavement Structures. Constr. Build. Mater. 2013, 44, 207–213. [Google Scholar] [CrossRef]
- Komba, J.; Anochie-Boateng, J.; O’Connell, J.; Verhaeghe, B. Long-Term Pavement Performance Monitoring and the Revision of Performance Criteria for High Modulus Asphalt in South Africa. In Proceedings of the Roles of Accelerated Pavement Testing in Pavement Sustainability; Aguiar-Moya, J.P., Vargas-Nordcbeck, A., Leiva-Villacorta, F., Loría-Salazar, L.G., Eds.; Springer International Publishing: Cham, Switzerland, 2016; pp. 177–194. [Google Scholar]
- Du, S.W.; Liu, C.F. Performance Evaluation of High Modulus Asphalt Mixture with Button Rock Asphalt. Adv. Mater. Res. 2012, 549, 558–562. [Google Scholar] [CrossRef]
- Moreno-Navarro, F.; Sol-Sánchez, M.; Rubio-Gámez, M.C.; Segarra-Martínez, M. The Use of Additives for the Improvement of the Mechanical Behavior of High Modulus Asphalt Mixes. Constr. Build. Mater. 2014, 70, 65–70. [Google Scholar] [CrossRef]
- Ye, F.; Xiao, B.; Liu, F.; Ding, X.; Peng, P.; Ma, T.; Xu, G. A Piezoelectric Sensing and Machine Learning Integrated Method for Modulus Inversion and Structural Strength Prediction in Asphalt Pavements. Adv. Eng. Inform. 2026, 69, 103956. [Google Scholar] [CrossRef]
- Ding, X.; Huang, F.; Rath, P.; Ye, Z.; Buttlar, W.G.; Ma, T. Comparative Fracture Resistance Assessment of Rubber-Modified Asphalt Mortar Based on Meso-and Macro-Mechanical Analysis. Int. J. Pavement Eng. 2023, 24, 2265032. [Google Scholar] [CrossRef]
- Ma, X.; Zhang, C.; Li, R.; Zheng, L.; Xu, J. Effect of Temperature and Humidity Environment on the Microstructure and Physicochemical Properties of SBS Modified Asphalt. Case Stud. Constr. Mater. 2025, 22, e04192. [Google Scholar] [CrossRef]
- Sun, J.; Huang, W.; Wang, X.; Zhang, B.; Zhang, Z.; Rahman, A.; Huang, Y.; Luo, S. Epoxy Steel Slag Asphalt Mixture: Achieving Breakthrough in Pavement Performance and Efficient Waste Resource Utilization. Chem. Eng. J. 2025, 520, 166262. [Google Scholar] [CrossRef]
- Peng, Y.; Li, S.; Xu, X.; Chen, R.; Cao, A.; Lan, J.; Jiang, X.; Sreeram, A. Functionalized Recycling of Waste Polypropylene into Low-Carbon Asphalt Modifier Towards Circularity: From Mechanochemical Preparation to Structural and Performance Evaluations. Chem. Eng. J. 2026, 529, 172719. [Google Scholar] [CrossRef]
- Du, Y.; Xu, J.; Wang, Z.; Ma, C.; Deng, H. Characterization and mechanism of road performance of fiber-reinforced high modulus asphalt mixture. J. Cent. S. Univ. Sci. Technol. 2024, 55, 3898–3908. [Google Scholar]
- Jia, Y.; Li, W.; Wei, J. Research of High Modulus Asphalt Aging Performance Based on Mechanics of Rheological Properties. Mater. Rep. 2016, 30, 406–411, 415. [Google Scholar]
- Ma, T.; Ding, X.; Zhang, D.; Huang, X.; Chen, J. Experimental Study of Recycled Asphalt Concrete Modified by High-Modulus Agent. Constr. Build. Mater. 2016, 128, 128–135. [Google Scholar] [CrossRef]
- Cheng, L.; Zhang, L.; Lei, Y.; Ma, Y.; Yan, C. Effect of the Laboratory Short-Term Aging Temperature on the Chemical and Rheological Characteristics of High Modulus Asphalts. Constr. Build. Mater. 2022, 314, 125569. [Google Scholar] [CrossRef]
- Wang, C.; Wang, H.; Zhao, L.; Cao, D. Experimental Study on Rheological Characteristics and Performance of High Modulus Asphalt Binder with Different Modifiers. Constr. Build. Mater. 2017, 155, 26–36. [Google Scholar] [CrossRef]
- Jafari, M.; Babazadeh, A. Evaluation of Polyphosphoric Acid-Modified Binders Using Multiple Stress Creep and Recovery and Linear Amplitude Sweep Tests. Road Mater. Pavement Des. 2016, 17, 859–876. [Google Scholar] [CrossRef]
- Chen, Y.; Zheng, W.; Gao, R.; Tebaldi, G.; Hossiney, N. Evaluation of Test Methods for Fracture Resistance of High Modulus Asphalt Binders from Rheological and Mechanical Perspectives. Constr. Build. Mater. 2022, 329, 127216. [Google Scholar] [CrossRef]
- Zhang, Z.; Zheng, W.; Gui, Z.; Tang, Z.; Li, N.; Xu, Y. Rheological properties and modification mechanism of high-modulus asphalt modified with polymer composite modifiers. J. Mater. Sci. Eng. 2023, 41, 51–57. [Google Scholar] [CrossRef]
- Ma, L. Research on Design and Properties of High Modulus Modified Asphalt. Master’s Dissertation, Southeast University, Nanjing, China, 2019. [Google Scholar]
- Fang, S.; Xiong, Z.; Sun, C.; Hong, J. Research on temperature-viscoelastic properties of high modulus asphalt mixture. New Build. Mater. 2020, 47, 78–82. [Google Scholar]
- Issa, M.A.; Goli, A.; Revelli, V.; Ali, A.; Mehta, Y. Influence of Softening Agents on Low and Intermediate Temperature Cracking Properties of Highly Polymer Modified Asphalt Binders. Constr. Build. Mater. 2025, 490, 142404. [Google Scholar] [CrossRef]
- Sha, D.; Li, G.; Wang, F.; Tang, M.; Liu, Y. Establishment and Evaluation of Constitutive Model of High Modulus Asphalt at Low Temperature Based on BBR Test. Mater. Rep. 2025, 39, 131–137. [Google Scholar]
- Xiao, Q.; Ren, X.; Li, M.; Dong, S.; Chen, X. Rheological Properties of High Modulus Asphalt Binder. Highway 2022, 67, 20–28. [Google Scholar]
- Guo, Y.; Xu, L.; Wu, L.; Shen, X. High-temperature performance evaluation of modified asphalt based on the MSCR test. J. Build. Mater. 2018, 21, 154–158. [Google Scholar] [CrossRef]
- Wang, H.; Yang, J.; Shi, X.; Chen, X. Evaluation of High Temperature Performance Optimization for High Modulus Modified Asphalt. Highway 2015, 60, 174–179. [Google Scholar]
- AASHTO T315-15; Standard Test Method for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer (DSR). AASHTO: Washington, DC, USA, 2010.
- AASHTO T 350; Standard Method of Test for Multiple Stress Creep Recovery (MSCR) Test of Asphalt Binder Using a Dynamic Shear Rheometer (DSR). AASHTO: Washington, DC, USA, 2014.
- Bahia, H.; Tabatabaee, H.; Mandal, T.; Faheem, A. Field Evaluation of Wisconsin Modified Binder Selection Guidelines-Phase II; Wisconsin Highway Research Program: Madison, WI, USA, 2013. [Google Scholar]
- United States Department of Transportation. US DOT Public Access Plan Website. 2015. Available online: https://ntl.bts.gov/ntl/public-access (accessed on 3 December 2025).
- AASHTO T 391-20; Standard Method of Test for Estimating Fatigue Resistance of Asphalt Binders Using the Linear Amplitude Sweep. AASHTO: Washington, DC, USA, 2020.
- AASHTO T 387-19; Standard Method of Test for Determining the Cracking Temperature of Asphalt Binder Using the Asphalt Binder Cracking Device (ABCD). AASHTO: Washington, DC, USA, 2023.
- Li, S. Multiscale Research on High-Temperature Creep Behaviour of Asphalt Mixture. Doctoral Dissertation, Southeast University, Nanjing, China, 2022. [Google Scholar]
- AASHTO MP 19-10; Standard Specification for Performance-Graded Asphalt Binder Using Multiple Stress Creep Recovery (MSCR) Test. AASHTO: Washington, DC, USA, 2010.
- Wang, J.; Jiang, J.; Wang, G.; Niu, X.; Wang, L.; Jin, Y.; Ma, Z.; Dong, Q.; Ni, F. Investigation of Thermal Cracking Resistance in Modified Asphalt with Plasticizers: Rheological and Micromechanical Insights. Constr. Build. Mater. 2025, 497, 143894. [Google Scholar] [CrossRef]
- Rahbar-Rastegar, R.; Sias Daniel, J.; Reinke, G. Comparison of Asphalt Binder and Mixture Cracking Parameters. Road Mater. Pavement Des. 2017, 18, 211–233. [Google Scholar] [CrossRef]
- Aurilio, M.; Tavassoti, P.; Elwardany, M.; Baaj, H. Characterization of Styrene-Butadiene-Styrene (SBS)-Modified Asphalt Binders Using the Bending Beam Rheometer and the Asphalt Binder Cracking Device. Can. J. Civ. Eng. 2023, 50, 681–687. [Google Scholar] [CrossRef]












| Technical Indicators | Test Results | Technical Specifications |
|---|---|---|
| Penetration (25 °C)/0.1 mm | 53.7 | 40~60 |
| Softening point/°C | 75.3 | ≥60 |
| Ductility (5 °C)/cm | 31.5 | ≥20 |
| Viscosity (135 °C)/Pa·s | 1.55 | ≤3 |
| Technical Indicators | Test Results | Technical Specifications |
|---|---|---|
| Apparent relative density | 2.711 | ≥2.5 |
| Density | 1.08 | 1~1.1 |
| Water content/% | 0.4 | ≥1 |
| Hydrophilicity coefficient/% | 0.56 | <1 |
| Plasticity index | 2.6 | <4 |
| Dosage (%) | Binder Condition | Critical Temperature (℃) | High-Temperature PG (℃) |
|---|---|---|---|
| 0 | Unaged | 90.3 | 76 |
| RTFO | 80.0 | ||
| 17 | Unaged | 93.9 | 88 |
| RTFO | 91.9 | ||
| 22 | Unaged | 94.8 | 94 |
| RTFO | 94.2 | ||
| 28 | Unaged | 95.6 | 94 |
| RTFO | 96.5 |
| Temperature (℃) | Effective Stress Levels (kPa) | |||
|---|---|---|---|---|
| 0% | 17% | 22% | 28% | |
| 76 | 0.1/3.2/6.4 | 0.1/3.2/6.4 | 0.1/3.2 | 0.1 |
| 82 | 0.1/3.2/6.4 | 0.1/3.2/6.4 | 0.1/3.2 | 0.1/3.2 |
| 88 | 0.1/3.2/6.4 | 0.1/3.2/6.4 | 0.1/3.2/6.4 | 0.1/3.2 |
| 94 | 0.1/3.2/6.4 | 0.1/3.2/6.4 | 0.1/3.2/6.4 | 0.1/3.2 |
| Dosage (%) | C0 | C1 | C2 | A | B | α |
|---|---|---|---|---|---|---|
| 0 | 1 | 0.057 | 0.507 | 2.98 × 105 | 3.051 | 1.526 |
| 17 | 1 | 0.103 | 0.419 | 2.11 × 106 | 4.089 | 2.044 |
| 22 | 1 | 0.100 | 0.421 | 2.85 × 106 | 4.080 | 2.040 |
| 28 | 1 | 0.103 | 0.452 | 5.48 × 105 | 4.037 | 2.018 |
Disclaimer/Publisher’s Note: The statements, opinions and data contained in all publications are solely those of the individual author(s) and contributor(s) and not of MDPI and/or the editor(s). MDPI and/or the editor(s) disclaim responsibility for any injury to people or property resulting from any ideas, methods, instructions or products referred to in the content. |
© 2026 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license.
Share and Cite
Wang, Y.; Ye, B.; Wang, Q.; Bai, Q.; Jiang, J. Determining Optimal Dosage of High-Modulus Asphalt Binders Through Comprehensive Rheological Assessment Across Full Temperature Range. Materials 2026, 19, 1155. https://doi.org/10.3390/ma19061155
Wang Y, Ye B, Wang Q, Bai Q, Jiang J. Determining Optimal Dosage of High-Modulus Asphalt Binders Through Comprehensive Rheological Assessment Across Full Temperature Range. Materials. 2026; 19(6):1155. https://doi.org/10.3390/ma19061155
Chicago/Turabian StyleWang, Yijun, Bolan Ye, Qisheng Wang, Qifeng Bai, and Jiwang Jiang. 2026. "Determining Optimal Dosage of High-Modulus Asphalt Binders Through Comprehensive Rheological Assessment Across Full Temperature Range" Materials 19, no. 6: 1155. https://doi.org/10.3390/ma19061155
APA StyleWang, Y., Ye, B., Wang, Q., Bai, Q., & Jiang, J. (2026). Determining Optimal Dosage of High-Modulus Asphalt Binders Through Comprehensive Rheological Assessment Across Full Temperature Range. Materials, 19(6), 1155. https://doi.org/10.3390/ma19061155

