Creep Damage Characteristics of Fiber-Reinforced Alkali-Activated Slag Concrete: Effect of Age and Stress
Abstract
1. Introduction
2. Materials and Specimens
2.1. Materials and Mix Design
2.2. Mix Design and Specimen Preparation
2.3. Specimen Preparation and Curing
3. Creep Damage Testing: Specimens and Loading Protocol
3.1. Creep Specimens
3.2. Testing Equipment and Loading Protocol
3.3. Concrete Damage Detection Using Ultrasonic Method
4. Results of the Experimental Program
4.1. Mechanical Properties
4.2. Creep Processing
4.3. Creep Strain
5. Influence of Fibers on Concrete Creep Damage
5.1. Mechanical Properties After Short-Term Sustained Loading
5.2. Poisson’s Ratio
5.3. Non-Destructive Ultrasonic Test Results
6. Conclusions
- The stress-dependent response to short-term sustained loading reveals a damage threshold mechanism in alkali-activated matrices, where microcrack propagation transitions from beneficial densification at low stress levels (0.3 to 0.4) to destructive coalescence at higher intensities. This delineation establishes that creep damage is intrinsically governed by the competition between internal structure stabilization and fracture kinetics, offering a predictive framework for safe stress limits in structural design.
- Fiber reinforcement functions as a microstructural regulator rather than a mere mechanical enhancer, effectively constraining microcrack growth and delaying macrocrack formation by redistributing localized stresses. However, the nonlinear attenuation of this protective effect with increasing fiber content underscores a critical optimization principle: maximal damage mitigation requires balancing fiber dosage against interfacial saturation thresholds to maintain crack-arresting efficiency.
- Ultrasonic velocity degradation and Poisson’s ratio evolution collectively demonstrate that creep damage accumulation is predominantly driven by the loss of matrix cohesion under sustained loads, with fibers mitigating lateral expansion by preserving interfacial integrity. This mechanistic perspective redefines creep resistance in alkali-activated systems as a dynamic process of microcrack confinement, directly linking material composition to long-term dimensional stability and structural resilience.
Author Contributions
Funding
Data Availability Statement
Conflicts of Interest
References
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| Materials | Item | Unit (wt) | Value |
|---|---|---|---|
| GGBFS | SiO2 | % | 27.42 |
| Al2O3 | % | 18.44 | |
| Fe2O3 | % | 0.34 | |
| CaO | % | 36.96 | |
| MgO | % | 8.74 | |
| Na2O | % | 0.61 | |
| K2O | % | 0.42 | |
| SO3 | % | 2.48 | |
| P2O5 | % | 0.02 | |
| TiO2 | % | 0.74 | |
| LOI | % | 2.1 | |
| Sodium silicate solution | H2O | % | 56.9 |
| Si2O | % | 29.8 | |
| Na2O | % | 13.2 | |
| Fe | % | 0.02 | |
| Baume | Baumé degree | 50 | |
| Density | g/ | 1.539 | |
| PP fiber | Length | mm | 12 |
| Diameter | μm | 60 | |
| Density | g/ | 0.91 | |
| Tensile strength | MPa | 650 | |
| Elastic modulus | MPa | 4500 |
| Items | Mass |
|---|---|
| Fine aggregate | 1110.65 |
| GGBFS | 666.39 |
| Sodium hydroxide solution | 93.29 |
| Sodium silicate solution | 479.80 |
| Water | 146.61 |
| Water reducer | 4.51 |
| Water/binder | 0.40 |
| Groups | ID | Age (Days) | Stress Ratio (%) | Fiber Volume (%) |
|---|---|---|---|---|
| Damage | 07G50TF00 | 7 | 50 | 0 |
| 07G50TF05 | 5 | |||
| 07G50TF10 | 10 | |||
| 07G60TF00 | 60 | 0 | ||
| 07G60TF05 | 5 | |||
| 07G60TF10 | 10 | |||
| 07G70TF00 | 70 | 0 | ||
| 07G70TF05 | 5 | |||
| 07G70TF10 | 10 | |||
| 07G80TF00 | 80 | 0 | ||
| 07G80TF05 | 5 | |||
| 07G80TF10 | 10 | |||
| 14G50TF00 | 14 | 50 | 0 | |
| 14G50TF05 | 5 | |||
| 14G50TF10 | 10 | |||
| 14G60TF00 | 60 | 0 | ||
| 14G60TF05 | 5 | |||
| 14G60TF10 | 10 | |||
| 14G70TF00 | 70 | 0 | ||
| 14G70TF05 | 5 | |||
| 14G70TF10 | 10 | |||
| 14G80TF00 | 80 | 0 | ||
| 14G80TF05 | 5 | |||
| 14G80TF10 | 10 | |||
| 28G50TF00 | 28 | 50 | 0 | |
| 28G50TF05 | 5 | |||
| 28G50TF10 | 10 | |||
| 28G60TF00 | 60 | 0 | ||
| 28G60TF05 | 5 | |||
| 28G60TF10 | 10 | |||
| 28G70TF00 | 70 | 0 | ||
| 28G70TF05 | 5 | |||
| 28G70TF10 | 10 | |||
| 28G80TF00 | 80 | 0 | ||
| 28G80TF05 | 5 | |||
| 28G80TF10 | 10 |
| Groups | ID | Age (Days) | Stress Ratio (%) | Fiber Volume (%) |
|---|---|---|---|---|
| Controlled | 07G30CF00 | 7 | 30 | 0 |
| 07G30CF05 | 5 | |||
| 07G30CF10 | 10 | |||
| 07G40CF00 | 40 | 0 | ||
| 07G40CF05 | 5 | |||
| 07G40CF10 | 10 | |||
| 14G30CF00 | 14 | 30 | 0 | |
| 14G30CF05 | 5 | |||
| 14G30CF10 | 10 | |||
| 14G40CF00 | 40 | 0 | ||
| 14G40CF05 | 5 | |||
| 14G40CF10 | 10 | |||
| 28G30CF00 | 28 | 30 | 0 | |
| 28G30CF05 | 5 | |||
| 28G30CF10 | 10 | |||
| 28G40CF00 | 40 | 0 | ||
| 28G40CF05 | 5 | |||
| 28G40CF10 | 10 |
| Age (Days) | Fiber Volume (%) | Peak Strain (με) | Peak Stress (MPa) | Elastic Modulus (GPa) |
|---|---|---|---|---|
| 7 | 0.0 | 2715 (52) | 51.8 (0.93) | 24.1 (0.32) |
| 0.5 | 2762 (55) | 55.4 (0.87) | 25.2 (0.33) | |
| 1.0 | 2776 (53) | 57.5 (0.92) | 26.3 (0.32) | |
| 14 | 0.0 | 2672 (29) | 58.2 (0.92) | 28.1 (0.28) |
| 0.5 | 2719 (29) | 62.4 (0.87) | 29.2 (0.25) | |
| 1.0 | 2731 (27) | 64.4 (0.88) | 30.2 (0.32) | |
| 28 | 0.0 | 2692 (25) | 65.2 (0.88) | 31.7 (0.28) |
| 0.5 | 2664 (23) | 70.2(0.85) | 33.9 (0.22) | |
| 1.0 | 2638 (23) | 73.0 (0.86) | 34.9 (0.24) |
| Specimen | Initial Strain ε1 (με) | Final Strain ε2 (με) | Irreversible Strain εi (με) | Irreversible Ratio |
|---|---|---|---|---|
| 07G30CF00 | 636 (12) | 709 (14) | 60 (3) | 9.5% |
| 07G30CF05 | 622 (11) | 692 (13) | 59 (3) | 9.5% |
| 07G30CF10 | 609 (10) | 676 (12) | 56 (3) | 9.3% |
| 07G40CF00 | 868 (15) | 1006 (18) | 85 (4) | 9.8% |
| 07G40CF05 | 846 (14) | 980 (17) | 81 (4) | 9.5% |
| 07G40CF10 | 829 (13) | 958 (16) | 79 (4) | 9.5% |
| 07G50TF00 | 1033 (18) | 1254 (22) | 129 (6) | 12.5% |
| 07G50TF05 | 1003 (17) | 1216 (21) | 119 (6) | 11.9% |
| 07G50TF10 | 975 (16) | 1179 (20) | 116 (6) | 11.9% |
| 07G60TF00 | 1240 (22) | 1747 (30) | 196 (9) | 15.8% |
| 07G60TF05 | 1212 (21) | 1705 (29) | 190 (9) | 15.7% |
| 07G60TF10 | 1185 (20) | 1660 (28) | 180 (8) | 15.3% |
| 07G70TF00 | 1381 (25) | 1908 (33) | 294 (13) | 21.3% |
| 07G70TF05 | 1349 (24) | 1856 (32) | 279 (12) | 20.8% |
| 07G70TF10 | 1318 (23) | 1804 (31) | 271 (12) | 20.7% |
| 14G30CF00 | 619 (12) | 695 (14) | 55 (3) | 8.9% |
| 14G30CF05 | 598 (11) | 672 (13) | 51 (3) | 8.6% |
| 14G30CF10 | 685 (13) | 879 (16) | 59 (3) | 8.6% |
| 14G40CF00 | 841 (14) | 961 (17) | 79 (4) | 9.4% |
| 14G40CF05 | 816 (13) | 933 (16) | 76 (4) | 9.4% |
| 14G40CF10 | 802 (13) | 915 (15) | 74 (4) | 9.2% |
| 14G50TF00 | 1208 (21) | 1426 (25) | 143 (7) | 11.9% |
| 14G50TF05 | 1172 (20) | 1383 (24) | 129 (6) | 11.0% |
| 14G50TF10 | 1158 (20) | 1361 (24) | 125 (6) | 10.9% |
| 14G60TF00 | 1307 (23) | 1621 (28) | 203 (9) | 15.5% |
| 14G60TF05 | 1272 (22) | 1578 (27) | 185 (8) | 14.6% |
| 14G60TF10 | 1250 (22) | 1544 (26) | 178 (8) | 14.2% |
| 14G70TF00 | 1408 (25) | 1880 (32) | 295 (13) | 21.0% |
| 14G70TF05 | 1373 (24) | 1829 (31) | 278 (12) | 20.2% |
| 14G70TF10 | 1346 (24) | 1784 (30) | 270 (12) | 19.9% |
| 28G30CF00 | 615 (12) | 688 (14) | 52 (3) | 8.5% |
| 28G30CF05 | 602 (11) | 672 (13) | 47 (3) | 7.7% |
| 28G30CF10 | 589 (11) | 656 (12) | 44 (3) | 7.6% |
| 28G40CF00 | 820 (14) | 924 (16) | 68 (4) | 8.3% |
| 28G40CF05 | 803 (13) | 904 (16) | 64 (4) | 8.0% |
| 28G40CF10 | 780 (13) | 875 (15) | 60 (4) | 7.8% |
| 28G50TF00 | 1074 (19) | 1325 (23) | 111 (5) | 10.3% |
| 28G50TF05 | 1042 (18) | 1283 (22) | 107 (5) | 10.3% |
| 28G50TF10 | 1019 (18) | 1248 (22) | 102 (5) | 10.1% |
| 28G60TF00 | 1304 (23) | 1604 (28) | 182 (8) | 13.9% |
| 28G60TF05 | 1273 (22) | 1563 (27) | 167 (8) | 13.1% |
| 28G60TF10 | 1237 (22) | 1510 (26) | 160 (8) | 12.9% |
| 28G70TF00 | 1379 (25) | 1734 (30) | 254 (11) | 18.4% |
| 28G70TF05 | 1350 (24) | 1690 (29) | 247 (11) | 18.3% |
| 28G70TF10 | 1316 (24) | 1638 (28) | 237 (10) | 17.9% |
| Specimen | Creep Strain (με) | Creep Coefficient | Specimen | Creep Strain (με) | Creep Coefficient | Specimen | Creep Strain (με) | Creep Coefficient |
|---|---|---|---|---|---|---|---|---|
| 07G30CF00 | 73 (4) | 0.11 | 14G30CF00 | 76 (4) | 0.12 | 28G30CF00 | 73 (4) | 0.12 |
| 07G30CF05 | 70 (4) | 0.11 | 14G30CF05 | 74 (4) | 0.12 | 28G30CF05 | 70 (4) | 0.12 |
| 07G30CF10 | 67 (4) | 0.11 | 14G30CF10 | 94 (5) | 0.12 | 28G30CF10 | 67 (4) | 0.11 |
| 07G40CF00 | 138 (7) | 0.16 | 14G40CF00 | 120 (6) | 0.14 | 28G40CF00 | 104 (5) | 0.13 |
| 07G40CF05 | 134 (7) | 0.16 | 14G40CF05 | 117 (6) | 0.14 | 28G40CF05 | 101 (5) | 0.13 |
| 07G40CF10 | 129 (7) | 0.16 | 14G40CF10 | 113 (6) | 0.14 | 28G40CF10 | 95 (5) | 0.12 |
| 07G50TF00 | 221 (11) | 0.21 | 14G50TF00 | 218 (11) | 0.18 | 28G50TF00 | 251 (12) | 0.23 |
| 07G50TF05 | 213 (11) | 0.21 | 14G50TF05 | 211 (11) | 0.18 | 28G50TF05 | 241 (12) | 0.23 |
| 07G50TF10 | 204 (10) | 0.21 | 14G50TF10 | 203 (10) | 0.18 | 28G50TF10 | 229 (11) | 0.23 |
| 07G60TF00 | 507 (25) | 0.41 | 14G60TF00 | 314 (16) | 0.24 | 28G60TF00 | 300 (15) | 0.23 |
| 07G60TF05 | 493 (25) | 0.41 | 14G60TF05 | 306 (15) | 0.24 | 28G60TF05 | 290 (15) | 0.23 |
| 07G60TF10 | 475 (24) | 0.40 | 14G60TF10 | 294 (15) | 0.24 | 28G60TF10 | 273 (14) | 0.22 |
| 07G70TF00 | 527 (26) | 0.38 | 14G70TF00 | 472 (24) | 0.34 | 28G70TF00 | 355 (18) | 0.26 |
| 07G70TF05 | 507 (25) | 0.38 | 14G70TF05 | 456 (23) | 0.33 | 28G70TF05 | 340 (17) | 0.25 |
| 07G70TF10 | 485 (24) | 0.37 | 14G70TF10 | 438 (22) | 0.32 | 28G70TF10 | 322 (16) | 0.25 |
| 07G80TF00 | 690 (35) | 0.43 | 14G80TF00 | 662 (33) | 0.38 | 28G80TF00 | 572 (29) | 0.35 |
| 07G80TF05 | 668 (33) | 0.42 | 14G80TF05 | 643 (32) | 0.38 | 28G80TF05 | 551 (28) | 0.34 |
| 07G80TF10 | 641 (32) | 0.41 | 14G80TF10 | 615 (31) | 0.37 | 28G80TF10 | 517 (26) | 0.33 |
| Specimen | Normlized Data | |||
|---|---|---|---|---|
| Peak Strain | Peak Strength | Unloading Elastic Modulus | Reloading Elastic Modulus | |
| 07G30CF00 | 1.02 | 1.04 | 1.04 | 1.00 |
| 07G30CF05 | 1.02 | 1.02 | 1.01 | 0.98 |
| 07G30CF10 | 1.02 | 1.04 | 0.99 | 0.96 |
| 07G40CF00 | 1.03 | 1.00 | 1.03 | 1.00 |
| 07G40CF05 | 1.03 | 1.00 | 1.00 | 0.98 |
| 07G40CF10 | 1.03 | 1.01 | 0.98 | 0.97 |
| 07G50TF00 | 1.05 | 0.94 | 0.99 | 0.89 |
| 07G50TF05 | 1.05 | 0.96 | 0.96 | 0.87 |
| 07G50TF10 | 1.04 | 0.98 | 0.93 | 0.85 |
| 07G60TF00 | 1.08 | 0.89 | 0.97 | 0.78 |
| 07G60TF05 | 1.07 | 0.90 | 0.95 | 0.77 |
| 07G60TF10 | 1.07 | 0.91 | 0.93 | 0.76 |
| 07G70TF00 | 1.12 | 0.86 | 0.93 | 0.72 |
| 07G70TF05 | 1.11 | 0.81 | 0.91 | 0.70 |
| 07G70TF10 | 1.10 | 0.83 | 0.88 | 0.69 |
| 14G30CF00 | 1.01 | 0.99 | 1.01 | 1.00 |
| 14G30CF05 | 1.01 | 1.03 | 0.99 | 0.97 |
| 14G30CF10 | 1.04 | 1.02 | 1.01 | 1.00 |
| 14G40CF00 | 1.02 | 0.99 | 1.01 | 1.00 |
| 14G40CF05 | 1.02 | 0.99 | 0.98 | 0.98 |
| 14G40CF10 | 1.02 | 0.99 | 0.96 | 0.97 |
| 14G50TF00 | 1.05 | 1.01 | 0.98 | 0.88 |
| 14G50TF05 | 1.04 | 0.97 | 0.95 | 0.86 |
| 14G50TF10 | 1.04 | 1.00 | 0.94 | 0.85 |
| 14G60TF00 | 1.07 | 0.89 | 0.96 | 0.78 |
| 14G60TF05 | 1.07 | 0.91 | 0.93 | 0.76 |
| 14G60TF10 | 1.06 | 0.88 | 0.91 | 0.75 |
| 14G70TF00 | 1.12 | 0.85 | 0.91 | 0.71 |
| 14G70TF05 | 1.10 | 0.82 | 0.89 | 0.70 |
| 14G70TF10 | 1.10 | 0.84 | 0.88 | 0.69 |
| 28G30CF00 | 1.00 | 1.01 | 1.00 | 0.99 |
| 28G30CF05 | 1.00 | 1.04 | 0.97 | 0.96 |
| 28G30CF10 | 0.99 | 1.00 | 0.95 | 0.94 |
| 28G40CF00 | 1.00 | 1.00 | 1.00 | 0.99 |
| 28G40CF05 | 1.00 | 1.01 | 0.98 | 0.98 |
| 28G40CF10 | 1.00 | 1.03 | 0.95 | 0.95 |
| 28G50TF00 | 1.02 | 0.98 | 0.98 | 0.88 |
| 28G50TF05 | 1.02 | 1.01 | 0.96 | 0.87 |
| 28G50TF10 | 1.02 | 0.97 | 0.93 | 0.85 |
| 28G60TF00 | 1.05 | 0.93 | 0.93 | 0.78 |
| 28G60TF05 | 1.05 | 0.92 | 0.91 | 0.76 |
| 28G60TF10 | 1.05 | 0.91 | 0.88 | 0.74 |
| 28G70TF00 | 1.08 | 0.87 | 0.89 | 0.69 |
| 28G70TF05 | 1.08 | 0.84 | 0.87 | 0.68 |
| 28G70TF10 | 1.07 | 0.82 | 0.85 | 0.66 |
| Specimen | 07G30CF00 | 07G30CF05 | 07G30CF10 | 07G50TF00 | 07G50TF05 | 07G50TF10 | |
|---|---|---|---|---|---|---|---|
| Point | 1 | 0.17 | 0.17 | 0.13 | 0.31 | 0.28 | 0.31 |
| 2 | 0.16 | 0.18 | 0.13 | 0.26 | 0.28 | 0.26 | |
| 3 | 0.18 | 0.16 | 0.17 | 0.27 | 0.28 | 0.29 | |
| 4 | 0.16 | 0.18 | 0.14 | 0.30 | 0.25 | 0.27 | |
| 5 | 0.15 | 0.18 | 0.16 | 0.30 | 0.28 | 0.30 | |
| 6 | 0.22 | 0.18 | 0.14 | 0.29 | 0.31 | 0.27 | |
| 7 | 0.17 | 0.16 | 0.15 | 0.30 | 0.28 | 0.25 | |
| 8 | 0.15 | 0.12 | 0.17 | 0.28 | 0.28 | 0.23 | |
| 9 | 0.14 | 0.13 | 0.11 | 0.35 | 0.30 | 0.22 | |
| Mean value | 0.16 | 0.16 | 0.15 | 0.30 | 0.28 | 0.27 | |
| Specimen | 07G70TF00 | 07G70TF05 | 07G70TF10 | 28G70TF00 | 28G70TF05 | 28G70TF10 | |
| Point | 1 | 0.61 | 0.78 | 0.68 | 0.42 | 0.49 | 0.32 |
| 2 | 0.70 | 0.72 | 0.54 | 0.43 | 0.51 | 0.44 | |
| 3 | 0.64 | 0.77 | 0.54 | 0.48 | 0.46 | 0.60 | |
| 4 | 0.70 | 0.55 | 0.66 | 0.49 | 0.56 | 0.47 | |
| 5 | 0.72 | 0.71 | 0.62 | 0.50 | 0.51 | 0.42 | |
| 6 | 0.62 | 0.57 | 0.65 | 0.54 | 0.54 | 0.52 | |
| 7 | 0.62 | 0.79 | 0.70 | 0.60 | 0.52 | 0.42 | |
| 8 | 0.69 | 0.63 | 0.61 | 0.70 | 0.54 | 0.35 | |
| 9 | 0.60 | 0.23 | 0.61 | 0.70 | 0.39 | 0.69 | |
| Mean value | 0.66 | 0.64 | 0.62 | 0.54 | 0.50 | 0.47 | |
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Share and Cite
Zhang, Z.; Wu, S.; Bian, X.; Kang, J.; Guo, J. Creep Damage Characteristics of Fiber-Reinforced Alkali-Activated Slag Concrete: Effect of Age and Stress. Materials 2026, 19, 722. https://doi.org/10.3390/ma19040722
Zhang Z, Wu S, Bian X, Kang J, Guo J. Creep Damage Characteristics of Fiber-Reinforced Alkali-Activated Slag Concrete: Effect of Age and Stress. Materials. 2026; 19(4):722. https://doi.org/10.3390/ma19040722
Chicago/Turabian StyleZhang, Ziyang, Sikai Wu, Xianggang Bian, Jianfei Kang, and Jianbo Guo. 2026. "Creep Damage Characteristics of Fiber-Reinforced Alkali-Activated Slag Concrete: Effect of Age and Stress" Materials 19, no. 4: 722. https://doi.org/10.3390/ma19040722
APA StyleZhang, Z., Wu, S., Bian, X., Kang, J., & Guo, J. (2026). Creep Damage Characteristics of Fiber-Reinforced Alkali-Activated Slag Concrete: Effect of Age and Stress. Materials, 19(4), 722. https://doi.org/10.3390/ma19040722
