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Article

Analysis of Acoustic Absorption Coefficients and Characterization of Epoxy Adhesive Compositions Based on the Reaction Product of Bisphenol A with Epichlorohydrin Modified with Fillers

by
Izabela Miturska-Barańska
1,*,
Anna Rudawska
1,
Lydia Sobotova
2,
Miroslav Badida
2,
Ewa Olewnik-Kruszkowska
3,
Miroslav Müller
4 and
Monika Hromasová
5
1
Department of Production Computerisation and Robotisation, Faculty of Mechanical Engineering, Lublin University of Technology, Nadbystrzycka 36, 20-618 Lublin, Poland
2
Department of Business Management and Environmental Engineering, Faculty of Mechanical Engineering, Technical University of Kosice, Letná 9, 042 00 Košice, Slovakia
3
Department of Physical Chemistry and Physicochemistry of Polymers, Faculty of Chemistry, Nicolaus Copernicus University in Toruń, Gagarina 7, 87-100 Toruń, Poland
4
Department of Material Science and Manufacturing Technology, Faculty of Engineering, Czech University of Life Sciences, Kamýcká 129, 165 21 Prague, Czech Republic
5
Department of Electrical Engineering and Automation, Faculty of Engineering, Czech University of Life Sciences, Kamýcká 129, 165 21 Prague, Czech Republic
*
Author to whom correspondence should be addressed.
Materials 2024, 17(18), 4452; https://doi.org/10.3390/ma17184452
Submission received: 24 July 2024 / Revised: 20 August 2024 / Accepted: 27 August 2024 / Published: 10 September 2024

Abstract

Material development in acoustic engineering plays a significant role in various applications, such as industrial noise control. It is important and relevant to consider alternative materials capable of reducing noise levels in different frequency ranges. One commonly used material in engineering structures is epoxy adhesive compositions. Favoring the use of adhesive compositions are their main characteristics, including weight reduction in structures, corrosion resistance, relatively low manufacturing costs, and high mechanical strength. This paper aims to discuss the relationship between the mechanical properties of modified epoxy adhesives, their structure, and sound absorption efficiency. The subjects of this study were specimens of an epoxy composition in the cured state. Acoustic absorption coefficients were evaluated using a dual-microphone impedance tube, and tensile, compressive, and bending strength properties were determined using a testing machine. The impact strength of the compositions was also investigated. An analysis of the structure of the adhesives in the cured state was carried out using a scanning electron microscope. The test specimens were made from Epidian 5 epoxy resin cured with a polyamide PAC curing agent. Nanobent ZR2 aluminosilicate in an amount of 1%, CaCO3 calcium carbonate in an amount of 5%, and CWZ-22 activated carbon in an amount of 20% were used as modifiers. The conducted studies revealed that the highest tensile strength was obtained for the adhesive composition with the addition of ZR2 filler. The highest compressive strength was exhibited by the adhesive composition with the addition of CWZ-22 filler. The highest flexural strength was demonstrated by the unmodified composition. For all the tested adhesive compositions, low sound absorption values were achieved, with a maximum of approximately 0.18. From the perspective of the reduction index R, it was observed that these samples performed better in reduction than in absorption. The best values were achieved in the compositions modified with CaCO3.
Keywords: adhesive modification; epoxy composition; sound absorption test; SEM analysis adhesive modification; epoxy composition; sound absorption test; SEM analysis

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MDPI and ACS Style

Miturska-Barańska, I.; Rudawska, A.; Sobotova, L.; Badida, M.; Olewnik-Kruszkowska, E.; Müller, M.; Hromasová, M. Analysis of Acoustic Absorption Coefficients and Characterization of Epoxy Adhesive Compositions Based on the Reaction Product of Bisphenol A with Epichlorohydrin Modified with Fillers. Materials 2024, 17, 4452. https://doi.org/10.3390/ma17184452

AMA Style

Miturska-Barańska I, Rudawska A, Sobotova L, Badida M, Olewnik-Kruszkowska E, Müller M, Hromasová M. Analysis of Acoustic Absorption Coefficients and Characterization of Epoxy Adhesive Compositions Based on the Reaction Product of Bisphenol A with Epichlorohydrin Modified with Fillers. Materials. 2024; 17(18):4452. https://doi.org/10.3390/ma17184452

Chicago/Turabian Style

Miturska-Barańska, Izabela, Anna Rudawska, Lydia Sobotova, Miroslav Badida, Ewa Olewnik-Kruszkowska, Miroslav Müller, and Monika Hromasová. 2024. "Analysis of Acoustic Absorption Coefficients and Characterization of Epoxy Adhesive Compositions Based on the Reaction Product of Bisphenol A with Epichlorohydrin Modified with Fillers" Materials 17, no. 18: 4452. https://doi.org/10.3390/ma17184452

APA Style

Miturska-Barańska, I., Rudawska, A., Sobotova, L., Badida, M., Olewnik-Kruszkowska, E., Müller, M., & Hromasová, M. (2024). Analysis of Acoustic Absorption Coefficients and Characterization of Epoxy Adhesive Compositions Based on the Reaction Product of Bisphenol A with Epichlorohydrin Modified with Fillers. Materials, 17(18), 4452. https://doi.org/10.3390/ma17184452

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