Dispersion Mechanism of Styrene–Butadiene Rubber Powder Modified by Itaconic Acid and Its Toughening Effect on Oil Well Cement
Abstract
:1. Introduction
2. Experimental Section
2.1. Materials
2.2. Preparation of Three Latex Powders
2.3. Characterization of Latex Powder
2.3.1. Absorbance of the Latex Powder
2.3.2. Particle Size of the Latex Powder
2.3.3. Zeta Potential of the Latex Powder
2.4. Measurements of Cement Paste with Latex
2.4.1. Fluidity of Cement Paste
2.4.2. Isothermal Heat Flow Calorimetry
2.4.3. Triaxial Mechanical Test
2.4.4. Compressive Strength
2.5. Reaction Mechanism of Latex Powder
2.5.1. X-ray Diffraction Tests
2.5.2. Adsorption Measurement
2.5.3. Scanning Electron Microscope (SEM) Tests
3. Results and Discussion
3.1. Dispersion State Analysis of SISBR Latex Powder
3.2. Influence of SISBR Latex on Cement Slurry
3.2.1. Fluidity
3.2.2. Optical Microstructure of Cement Slurry
3.3. Effects of SISBR Latex Powders on Cement Hydration
3.3.1. Hydration Kinetics
3.3.2. X-ray Diffraction Analysis
3.3.3. Adsorption Behavior of SISBR Latex Powders on Cement Surface
3.4. Effects of SISBR Latex on Mechanical Property of Cement
3.4.1. Effects of SISBR Latex on Compressive Strength of Cement
3.4.2. Effects of SISBR Latex on Toughness of Cement
3.4.3. Effects of SISBR Latex on Microstructure of Cement Stone
4. Conclusions
Author Contributions
Funding
Institutional Review Board Statement
Informed Consent Statement
Data Availability Statement
Conflicts of Interest
References
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Chemical Compositions (wt.%) | |||||||
---|---|---|---|---|---|---|---|
CaO | SiO2 | Fe2O3 | SO3 | Al2O3 | MgO | K2O | Others |
69.68 | 15.13 | 6.45 | 3.39 | 2.34 | 0.92 | 0.79 | 1.3 |
Latex Samples | IA Dosage (%) in Latex | Elastic Modulus (GPa) |
---|---|---|
SBR | 0 | 8.34 |
SISBR-1 | 1 | 5.9 |
SISBR-3 | 3 | 3.16 |
SISBR-5 | 5 | 8.4 |
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Xing, Y.; Hu, M.; Cao, C.; Yu, J.; Zhao, J.; Zheng, H.; Guo, J. Dispersion Mechanism of Styrene–Butadiene Rubber Powder Modified by Itaconic Acid and Its Toughening Effect on Oil Well Cement. Materials 2022, 15, 8345. https://doi.org/10.3390/ma15238345
Xing Y, Hu M, Cao C, Yu J, Zhao J, Zheng H, Guo J. Dispersion Mechanism of Styrene–Butadiene Rubber Powder Modified by Itaconic Acid and Its Toughening Effect on Oil Well Cement. Materials. 2022; 15(23):8345. https://doi.org/10.3390/ma15238345
Chicago/Turabian StyleXing, Yubing, Miaomiao Hu, Chengzhang Cao, Jiayu Yu, Jiaqi Zhao, Hongbing Zheng, and Jintang Guo. 2022. "Dispersion Mechanism of Styrene–Butadiene Rubber Powder Modified by Itaconic Acid and Its Toughening Effect on Oil Well Cement" Materials 15, no. 23: 8345. https://doi.org/10.3390/ma15238345