Preparation, Characterisation, and Application of Bifunctional BaSO4 Sheets
Abstract
:1. Introduction
2. Materials and Methods
2.1. Materials
2.2. Sheet Preparation
2.3. Sheet Characterization
2.3.1. Scanning Electron Microscopy (SEM)
2.3.2. Dynamic Contact Angle Test
2.3.3. Determination of Solid Content
2.3.4. Determination of Wet Sheet Thickness
2.3.5. Determination of Reflectance
2.3.6. Particle Size Distribution Tests
2.3.7. Determination of Scattering Power
3. Results
3.1. Analysis of BaSO4 Particles
3.2. BaSO4 Morphology
3.3. Sheet Morphology
3.4. Mixing Time
3.5. Surfactant
3.6. Solid Content
3.7. Wet Sheet Thickness
3.8. Reflection Tests
3.9. Scattering PowerTests
3.10. Chip Detection
3.11. Repeatability Tests
3.12. Accuracy Tests
4. Conclusions
Author Contributions
Funding
Conflicts of Interest
References
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Acetone Volume (mL) | Solid Content (%) | The Surface and Flatness of Bifunctional Sheet |
---|---|---|
8 | 60.1 | uneven |
10 | 54.9 | uniform and flat |
12 | 50.5 | thin and porous |
Sheets Code | Wet Sheet Thickness (µm) | Scattering Time (s) | Scattering Diameter (cm) |
---|---|---|---|
1 | 200 | 27 | 2.3 |
2 | 250 | 20 | 2.0 |
3 | 300 | 17 | 1.9 |
4 | 350 | 14 | 1.6 |
5 | 400 | 12 | 1.3 |
6 | 450 | 11 | 1.2 |
7 | 500 | 11 | 1.2 |
Serial | Single Number (V) | Mean Single Value | Deviation |
---|---|---|---|
1 | 0.3295 | 0.3250 | 0.0045 |
2 | 0.3259 | 0.0009 | |
3 | 0.3238 | −0.0012 | |
4 | 0.3226 | −0.0024 | |
5 | 0.3230 | −0.0020 |
Chip Name | Concentration (mmol·L−1) | SD | CV (%) | |||||
---|---|---|---|---|---|---|---|---|
GLU-TiO2/CA | 8.44 | 8.81 | 8.68 | 8.19 | 8.27 | 8.47 | 0.24 | 2.8 |
GLU-BaSO4/CA | 8.23 | 8.19 | 8.61 | 8.12 | 8.54 | 8.46 | 0.20 | 2.4 |
Chip Name | Concentration (mmol·L−1) | Target Value (mmol·L−1) | Range of Target Values (mmol·L−1) | ||
---|---|---|---|---|---|
GLU-BaSO4/CA | 1.58 | 1.75 | 1.72 | 1.67 | 1.50~1.84 |
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Luo, J.; Liu, J.; Guo, X.; Liu, Y.; Jin, H.; Fan, D. Preparation, Characterisation, and Application of Bifunctional BaSO4 Sheets. Materials 2020, 13, 2903. https://doi.org/10.3390/ma13132903
Luo J, Liu J, Guo X, Liu Y, Jin H, Fan D. Preparation, Characterisation, and Application of Bifunctional BaSO4 Sheets. Materials. 2020; 13(13):2903. https://doi.org/10.3390/ma13132903
Chicago/Turabian StyleLuo, Jia, Jiaqi Liu, Xiaoyan Guo, Yuejiao Liu, Haibo Jin, and Daidi Fan. 2020. "Preparation, Characterisation, and Application of Bifunctional BaSO4 Sheets" Materials 13, no. 13: 2903. https://doi.org/10.3390/ma13132903