(3-(4-Chlorophenyl)-4,5-dihydroisoxazol-5-yl)methyl Benzenesulfonate
Round 1
Reviewer 1 Report
Khalid Bougrin and coworkers fully characterized (multinuclear NMR, ESI-MS, FT-IR, SCXRD including Hirshfeld analysis and DFT calculations) a new isoxazoline-linked sulfonate derivate, (3-(4-chlorophenyl)-4,5-dihydroisoxazol-5-yl)methylbenzene sulfonate.
After polishing the manuscript will be accepted for publication in Towards the Sustainable Synthesis of Biologically Active Molecules in Green Solvents topic of Molbank.
My problems:
1./ The packing diagrams of 5 are very important for the SCXRD analysis, but Figure 3-5 should be inserted into the SM.
2./ Table 1 is also important but move it to the SM, too.
3./ Figure 7-8 should be inserted into SM, the manuscript is long.
4./ Instead of Table 2, it would be better to have a figure overlaid with the DFT calculations and the SCXRD data. Move the Table 2 to the SM.
5./ Table 3-4 and Figure 9 put to the SM.
6./ In the SM, the ESI-MS spectrum shows only 1 decimal digit; it is not necessary to present.
Author Response
Please see the attachment.
Author Response File: 
Author Response.pdf
Round 2
Reviewer 1 Report
After the corrections, we can read the correct article.
